CN103385261A - Efficient green pesticide and production method thereof - Google Patents

Efficient green pesticide and production method thereof Download PDF

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Publication number
CN103385261A
CN103385261A CN2013103454868A CN201310345486A CN103385261A CN 103385261 A CN103385261 A CN 103385261A CN 2013103454868 A CN2013103454868 A CN 2013103454868A CN 201310345486 A CN201310345486 A CN 201310345486A CN 103385261 A CN103385261 A CN 103385261A
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China
Prior art keywords
vegetable insecticide
production method
ethanol
pesticide
auxiliary agent
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CN2013103454868A
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Chinese (zh)
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邹飞剑
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Individual
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Priority to CN2013103454868A priority Critical patent/CN103385261A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention provides an efficient green pesticide and a production method thereof. The efficient green pesticide is prepared from a vegetable insecticide and special addition agents, and is characterized in that the vegetable insecticide is prepared from 28kg-38kg of wild anise, 10kg-18kg of peppers, 14kg-20kg of celastrus angulatus, 26kg-36kg of stropanthus divericatus and 20kg-30kg of chinaberry seeds; the addition agents comprise 8kg-11kg of an emulsifying agent, 9kg-15kg of turpentine, 4kg-6kg of a penetrating agent, 0.6kg-1.5kg of a preservative and 22kg-28kg of ethanol; the weight ratio of the vegetable insecticide to the addition agents is 1 to 1. The green pesticide provided by the invention is efficient, secondary-toxin-free and residue-free, does not pollute the environment and can keep ecological balance.

Description

A kind of efficient green agricultural chemicals and production method
Technical field
The present invention relates to a kind of sterilization, the malicious agricultural chemicals that goes out, particularly a kind of efficient green agricultural chemicals and production method.
Background technology
Domestic existing sterilization and disinfection class agricultural chemicals is mostly chemical pesticide, use this type of agricultural chemicals easily to cause a large amount of the toxin remains in crops, vegetables and melon and fruit, make natural environment be subject to severe contamination, broken natural environment and the ecological balance encircled, constitute a public nuisance, directly threaten the mankind's living environment, be unfavorable for developing green agriculture and pollution-free food.
In recent years, someone developed several environment friendly agriculturals, and the insecticidal effect of this type of agricultural chemicals is better, but the effect of sterilization, the poison that goes out a little less than, apparatus expensive, cost is high, production scale is very limited, and is difficult to promote and implements.
Summary of the invention
The objective of the invention is to provide a kind of green agriculture chemicals of noresidue that can control fruit tree, thin dish, melon and fruit and can eat the agricultural product crop disease and insect raw, it does not contain the residuals harmful to animal, is a kind of environment-friendly type, high efficiency, without secondary toxicity, noresidue, free from environmental pollution, public nuisance-free agricultural chemicals one Greep pesticide wiith no residue that can keep ecological balance and the production method of this agricultural chemicals.
The technical solution adopted in the present invention is: Greep pesticide wiith no residue, and it is formulated by vegetable insecticide and special assistant, its formula is: wild anistree 28-38kg, Chinese prickly ash 10-18kg, Celastrus angulatus 14-20kg, stropanthus divericatus 26-36kg, chinaberry 20-30kg.
Auxiliary agent comprises emulsifier, turpentine oil, bleeding agent, preservative and ethanol, and the proportion scale of auxiliary agent is emulsifier 8-11kg, turpentine oil 9-15kg, bleeding agent 4-6kg, preservative 0.6-1.5kg, ethanol 22-28kg.Vegetable insecticide is 1: 1 with the weight batching ratio of auxiliary agent.
The production method of Greep pesticide wiith no residue:
1, get wild anise, Chinese prickly ash, Celastrus angulatus, stropanthus divericatus, chinaberry and break into meal;
2, getting above-mentioned various raw material by charge ratio is respectively charged into and soaks in damp tank, the water that adds 5.5 times of amounts of above-mentioned crude drug, soak at normal temperatures 8-9 hour, extract secondary 80-95 degree centigrade of boiling, carry about 5-7 hour at every turn, crude drug liquid after second extraction combines, and refilters, and seals up for safekeeping the crude drug liquid running into tank after filtering standby:
3, each filtering liquid medicine of gained is inputted respectively in inspissator, be decompressed to 0.5-0.1Mpa, be concentrated to 1ml and be equivalent to crude drug liquid 3-6g under the 70-90 degree celsius temperature, namely 22-28Be, measure content and collect concentrated medicament, can obtain concentrated paste;
4, each concentrated medicament of gained is got respectively wild anistree 28-38kg, Chinese prickly ash 10-18kg, Celastrus angulatus 14-20kg, stropanthus divericatus 26-36kg, chinaberry 20-30kg is input in reactor, add 75% ethanolic solution in 4: 1 ratios, stir 30-60 minute, put into settling tank precipitation 30-48 hour, the elimination insoluble matter, in the indefinite filtered fluid input of gained destilling tower, be heated to the 80-950C distillation, reclaim ethanol to 1/2 of substance kind, collecting liquid inputs in surplus reactor again, add successively emulsifier 7.5-11.5kg by required proportion scale, turpentine oil 8-16kg, bleeding agent 3.5-5.5kg, preservative 0.6-1.5kg, ethanol 22-28kg, with above-mentioned various auxiliary agent mixing and emulsifying 1.5-3h, namely obtain Greep pesticide wiith no residue.
Optional tween 35-60 of emulsifier etc., preservative can select sorbic acid, benzoic acid to receive etc. in above-mentioned auxiliary agent, and bleeding agent can be selected dimethyl sulfoxide (DMSO) etc.
Prove according to test data, agricultural chemicals of the present invention and 2.5% cream of decamethrin vermins-proof effect have extremely significantly difference.Conclusion is agricultural chemicals of the present invention, can replace the part chemical pesticide fully.
Agricultural chemicals of the present invention, not only have the special pesticide performance, according to toxicological test, regards as low toxicity and nonpersistent pesticide, is a kind of novel green agricultural chemicals.Chemical pesticide is except having high toxicity, also have permanent toxic residue problem, and residual life is long, damaging range is wide, the precipitation accumulation causes serious disease and life harm in human body and animal, this is universally acknowledged global pollution problem, and the extensive degree that chemical pesticide pollutes is well imagined.
Agricultural chemicals of the present invention is that to adopt pure natural plant be that raw material is formulated through science processing, be not only hypotoxicity, and does not have the toxic residue problem, also can be to the natural enemy of insect---birds produce secondary and kill, can to humans and animals, ecological form endanger.
Comprehensive the above, Greep pesticide wiith no residue of the present invention be a kind of feature of environmental protection, without secondary toxicity, high efficiency, noresidue, pollution-free, keep ecological balance, non-harmful novel agrochemical, be to realize the ecological agriculture, the green ecological agricultural, the important guarantee of enviromental protection enterprise, have bright prospects.
Embodiment
A kind of efficient green agricultural chemicals is by vegetable insecticide and special assistant is composite makes.Vegetable insecticide is comprised of wild anise, Chinese prickly ash, Celastrus angulatus, stropanthus divericatus, chinaberry, its formula is: wild anistree 38kg, Chinese prickly ash 18kg, Celastrus angulatus 20kg, stropanthus divericatus 36kg, chinaberry 30kg, auxiliary agent is comprised of turpentine oil, ethanol, Tween-60, sorb, DMSO, and its charge ratio is that turpentine oil 12kg, concentration are 85% ethanol 25kg, 9.5kg Tween-60, sorbic acid 0.8kg, DMSO 4kg.Vegetable insecticide and auxiliary agent charge ratio are 1: 1.
The production method of Greep pesticide wiith no residue:
1, get wild anise, Chinese prickly ash, Celastrus angulatus, stropanthus divericatus, chinaberry and break into meal;
2, getting above-mentioned various raw material by charge ratio is respectively charged into and soaks in damp tank, the water that adds 5.5 times of amounts of above-mentioned crude drug, soak at normal temperatures 8-9 hour, extract secondary 80-95 degree centigrade of boiling, carry about 5-7 hour at every turn, crude drug liquid after second extraction combines, and refilters, and seals up for safekeeping the crude drug liquid running into tank after filtering standby:
3, each filtering liquid medicine of gained is inputted respectively in inspissator, be decompressed to 0.5-0.1Mpa, be concentrated to 1ml and be equivalent to crude drug liquid 3-6g under the 70-90 degree celsius temperature, namely 22-28Be, measure content and collect concentrated medicament, can obtain concentrated paste;
4, each concentrated medicament of gained is got respectively wild anistree 28-38kg, Chinese prickly ash 10-18kg, Celastrus angulatus 14-20kg, stropanthus divericatus 26-36kg, chinaberry 20-30kg is input in reactor, add 75% ethanolic solution in 4: 1 ratios, stir 30-60 minute, put into settling tank precipitation 30-48 hour, the elimination insoluble matter, in the indefinite filtered fluid input of gained destilling tower, be heated to the 80-950C distillation, reclaim ethanol to 1/2 of substance kind, collecting liquid inputs in surplus reactor again, add successively emulsifier 7.5-11.5kg by required proportion scale, turpentine oil 8-16kg, bleeding agent 3.5-5.5kg, preservative 0.6-1.5kg, ethanol 22-28kg, with above-mentioned various auxiliary agent mixing and emulsifying 1.5-3h, namely obtain Greep pesticide wiith no residue.

Claims (1)

1. an efficient green agricultural chemicals and production method, it is formulated by vegetable insecticide and special assistant, it is characterized in that vegetable insecticide made by anise, Chinese prickly ash, Celastrus angulatus, stropanthus divericatus, chinaberry formula, its formula is: wild anistree 28-38kg, Chinese prickly ash 10-18kg, Celastrus angulatus 14-20kg, stropanthus divericatus 26-36kg, chinaberry 20-30kg; Described auxiliary agent comprises emulsifier, turpentine oil, bleeding agent, preservative and ethanol, and the proportion scale of auxiliary agent is emulsifier 8-11kg, turpentine oil 9-15kg, bleeding agent 4-6kg, preservative 0.6-1.5kg, ethanol 22-28kg.Vegetable insecticide is 1: 1 with the weight batching ratio of auxiliary agent.
CN2013103454868A 2013-08-09 2013-08-09 Efficient green pesticide and production method thereof Pending CN103385261A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104430565A (en) * 2014-12-31 2015-03-25 江苏健神生物农化有限公司 Botanical pesticide and preparation method thereof
CN104789109A (en) * 2015-05-12 2015-07-22 重庆市品胜涂料有限公司 Environment-friendly and water-borne finish paint for woodenware and preparation method of environment-friendly and water-borne finish paint
CN105145691A (en) * 2015-09-18 2015-12-16 张滋柠 Household preparation and use method of biological insecticidal bacteriostatic agent
CN105230677A (en) * 2015-10-15 2016-01-13 重庆市盛尚茶业有限公司 Pesticide used for tea tree planting and preparation method and application thereof
CN107079773A (en) * 2017-06-27 2017-08-22 李宝智 The non-irrigated plateau fruit tree in Weihe north and weeds aquaponic method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144040A (en) * 1995-08-25 1997-03-05 郑州新源化工研究所 Botanic efficient insecticide without residual toxicity
CN1237349A (en) * 1999-06-25 1999-12-08 西北农业大学 Two kinds of celastrus angulatus water base insecticidal preparation
CN1276160A (en) * 2000-05-09 2000-12-13 吕世禄 0.36% aqueous matrine solution
CN1502243A (en) * 2002-11-20 2004-06-09 邓志宏 Broad-spectrum pesticide using plant composition as raw material and preparation process thereof
KR20060071380A (en) * 2006-06-02 2006-06-26 김규석 Natural inseticide
JP2008162920A (en) * 2006-12-27 2008-07-17 Yanagi Tomotama Composition for controlling plant pest
CN101611729A (en) * 2008-06-29 2009-12-30 王兴鹏 The compound method of a kind of plant medical agent control rice fulgorid worm

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144040A (en) * 1995-08-25 1997-03-05 郑州新源化工研究所 Botanic efficient insecticide without residual toxicity
CN1237349A (en) * 1999-06-25 1999-12-08 西北农业大学 Two kinds of celastrus angulatus water base insecticidal preparation
CN1276160A (en) * 2000-05-09 2000-12-13 吕世禄 0.36% aqueous matrine solution
CN1502243A (en) * 2002-11-20 2004-06-09 邓志宏 Broad-spectrum pesticide using plant composition as raw material and preparation process thereof
KR20060071380A (en) * 2006-06-02 2006-06-26 김규석 Natural inseticide
JP2008162920A (en) * 2006-12-27 2008-07-17 Yanagi Tomotama Composition for controlling plant pest
CN101611729A (en) * 2008-06-29 2009-12-30 王兴鹏 The compound method of a kind of plant medical agent control rice fulgorid worm

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
中国土农药志编辑委员会: "《中国土农药志》", 31 December 1959, 科学出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104430565A (en) * 2014-12-31 2015-03-25 江苏健神生物农化有限公司 Botanical pesticide and preparation method thereof
CN104789109A (en) * 2015-05-12 2015-07-22 重庆市品胜涂料有限公司 Environment-friendly and water-borne finish paint for woodenware and preparation method of environment-friendly and water-borne finish paint
CN104789109B (en) * 2015-05-12 2017-07-11 重庆市品胜涂料有限公司 A kind of environment-friendly water-based lacquer as woodenware finish and preparation method thereof
CN105145691A (en) * 2015-09-18 2015-12-16 张滋柠 Household preparation and use method of biological insecticidal bacteriostatic agent
CN105230677A (en) * 2015-10-15 2016-01-13 重庆市盛尚茶业有限公司 Pesticide used for tea tree planting and preparation method and application thereof
CN105230677B (en) * 2015-10-15 2018-01-16 重庆市盛尚茶业有限公司 Insecticide for tealeaves tree planting and its preparation method and application
CN107079773A (en) * 2017-06-27 2017-08-22 李宝智 The non-irrigated plateau fruit tree in Weihe north and weeds aquaponic method

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Application publication date: 20131113