CN104781222B - 制造碳酸二烷基酯的方法 - Google Patents

制造碳酸二烷基酯的方法 Download PDF

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Publication number
CN104781222B
CN104781222B CN201380060824.1A CN201380060824A CN104781222B CN 104781222 B CN104781222 B CN 104781222B CN 201380060824 A CN201380060824 A CN 201380060824A CN 104781222 B CN104781222 B CN 104781222B
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CN
China
Prior art keywords
column
carbonate
dialkyl carbonate
weight
transesterification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201380060824.1A
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English (en)
Chinese (zh)
Other versions
CN104781222A (zh
Inventor
P.乌姆斯
F.里泽
A.迪克斯
C.布哈利
T.潘库尔
A.苏桑托
G.龙格
J.范登艾恩德
W.武伊塔克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covestro Deutschland AG
Original Assignee
Covestro Deutschland AG
Bayer MaterialScience AG
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Publication of CN104781222A publication Critical patent/CN104781222A/zh
Application granted granted Critical
Publication of CN104781222B publication Critical patent/CN104781222B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
    • C07C68/065—Preparation of esters of carbonic or haloformic acids from organic carbonates from alkylene carbonates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/128—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/128—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis
    • C07C29/1285—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis of esters of organic acids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201380060824.1A 2012-11-21 2013-11-19 制造碳酸二烷基酯的方法 Expired - Fee Related CN104781222B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12193568.8 2012-11-21
EP12193568 2012-11-21
PCT/EP2013/074150 WO2014079835A1 (de) 2012-11-21 2013-11-19 Verfahren zur herstellung von dialkylcarbonaten

Publications (2)

Publication Number Publication Date
CN104781222A CN104781222A (zh) 2015-07-15
CN104781222B true CN104781222B (zh) 2017-03-08

Family

ID=47263117

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380060824.1A Expired - Fee Related CN104781222B (zh) 2012-11-21 2013-11-19 制造碳酸二烷基酯的方法

Country Status (7)

Country Link
US (1) US9475751B2 (enExample)
EP (1) EP2922810B1 (enExample)
JP (1) JP2016501855A (enExample)
KR (1) KR20150084859A (enExample)
CN (1) CN104781222B (enExample)
ES (1) ES2618524T3 (enExample)
WO (1) WO2014079835A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20160105665A (ko) * 2015-02-27 2016-09-07 롯데첨단소재(주) 디알킬카보네이트의 제조방법
KR20160105664A (ko) * 2015-02-27 2016-09-07 롯데첨단소재(주) 디알킬카보네이트의 제조방법
US10829635B2 (en) 2016-03-11 2020-11-10 Lg Chem, Ltd. Economical method of preparing a resin composition including polyalkylene carbonate with improved thermal stability and processability
KR20170109975A (ko) * 2016-03-22 2017-10-10 롯데첨단소재(주) 디알킬 카보네이트의 제조방법

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007096343A1 (en) * 2006-02-22 2007-08-30 Shell Internationale Research Maatschappij B.V. Process for the production of dialkyl carbonate and alkanediol
EP2322261A2 (de) * 2009-11-14 2011-05-18 Bayer MaterialScience AG Verfahren zur Reinigung von Dialkylcarbonaten
EP2354115A2 (de) * 2010-02-03 2011-08-10 Bayer MaterialScience AG Verfahren zur Herstellung von Dialkylcarbonaten

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US3642858A (en) 1969-02-12 1972-02-15 Dow Chemical Co Carbonate synthesis from alkylene carbonates
US3803201A (en) 1971-02-22 1974-04-09 Dow Chemical Co Synthesis of dimethyl carbonate
IT1034961B (it) 1975-04-09 1979-10-10 Snam Progetti Procedimento per la preparazione di dialchilcarbonati
DE2706684A1 (de) 1977-02-17 1978-08-24 Basf Ag Verfahren zur reindarstellung von dimethylcarbonat
DE2740251A1 (de) 1977-09-07 1979-03-22 Bayer Ag Verfahren zur herstellung von dialkylcarbonaten
DE2740243A1 (de) 1977-09-07 1979-03-15 Bayer Ag Verfahren zur herstellung von dialkylcarbonaten
US4851555A (en) 1984-10-25 1989-07-25 Scientific Design Company, Inc. Process for preparing alkylene oxides from alkylene carbonates
US4691041A (en) 1986-01-03 1987-09-01 Texaco Inc. Process for production of ethylene glycol and dimethyl carbonate
US4734519A (en) 1986-06-05 1988-03-29 Mallinckrodt, Inc. Pentaerythritol co-esters
US4661609A (en) 1986-07-31 1987-04-28 Texaco Inc. Process for cosynthesis of ethylene glycol and dimethyl carbonate
DE4129316A1 (de) 1991-09-03 1993-03-04 Bayer Ag Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten
DE4216121A1 (de) 1992-05-15 1993-11-18 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonaten
DE4224770A1 (de) 1992-07-27 1994-02-03 Bayer Ag Verfahren zur Abtrennung von Methanol aus Dimethylcarbonat/Methanol-Gemischen
DE4234525A1 (de) 1992-10-13 1994-04-14 Bayer Ag Verfahren zur Abtrennung von Alkanolen von sauerstoffhaltigen organischen Verbindungen mit höherer Kohlenstoffzahl
DE69620470T2 (de) 1995-12-22 2002-11-21 Asahi Kasei Kabushiki Kaisha, Osaka Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten und diolen
US6346638B1 (en) 1998-06-10 2002-02-12 Asahi Kasel Kabushiki Kaisha Process for continuous production of dialkyl carbonate and diol
AU2827900A (en) 1999-03-03 2000-09-21 Asahi Kasei Kabushiki Kaisha Process for continuously producing dialkyl carbonate and diol
JP2003104937A (ja) 2001-07-27 2003-04-09 Mitsubishi Chemicals Corp エステル交換法ジアルキルカーボネートの製造方法
JP4162883B2 (ja) * 2001-11-09 2008-10-08 三菱化学株式会社 エチレンカーボネートの回収方法
US6620959B1 (en) 2002-04-16 2003-09-16 Exxonmobil Chemical Patents Inc. Process for the production of unsymmetric and/or symmetric dialkyl carbonates and diols
TWI378087B (en) * 2006-02-22 2012-12-01 Shell Int Research Process for the preparation of an alkanediol and a dialkyl carbonate
TW200740731A (en) 2006-02-22 2007-11-01 Shell Int Research Process for the preparation of alkanediol
DE102009030680A1 (de) * 2009-06-26 2010-12-30 Bayer Materialscience Ag Verfahren zur Herstellung von Dialkylcarbonaten aus Alkylencarbonaten und Alkoholen
DE102010042937A1 (de) * 2010-10-08 2012-04-12 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Diarylcarbonaten aus Dialkylcarbonaten

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007096343A1 (en) * 2006-02-22 2007-08-30 Shell Internationale Research Maatschappij B.V. Process for the production of dialkyl carbonate and alkanediol
EP2322261A2 (de) * 2009-11-14 2011-05-18 Bayer MaterialScience AG Verfahren zur Reinigung von Dialkylcarbonaten
EP2354115A2 (de) * 2010-02-03 2011-08-10 Bayer MaterialScience AG Verfahren zur Herstellung von Dialkylcarbonaten

Also Published As

Publication number Publication date
KR20150084859A (ko) 2015-07-22
JP2016501855A (ja) 2016-01-21
US9475751B2 (en) 2016-10-25
EP2922810A1 (de) 2015-09-30
WO2014079835A9 (de) 2014-09-04
US20150299097A1 (en) 2015-10-22
CN104781222A (zh) 2015-07-15
WO2014079835A1 (de) 2014-05-30
EP2922810B1 (de) 2016-12-21
ES2618524T3 (es) 2017-06-21

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Address after: Germany Leverkusen

Applicant after: COVESTRO DEUTSCHLAND AG

Address before: Germany Leverkusen

Applicant before: BAYER MATERIALSCIENCE AG

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170308