CN104739707A - Traditional Chinese medicine liquid shampoo and preparation method thereof - Google Patents
Traditional Chinese medicine liquid shampoo and preparation method thereof Download PDFInfo
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- CN104739707A CN104739707A CN201310745568.1A CN201310745568A CN104739707A CN 104739707 A CN104739707 A CN 104739707A CN 201310745568 A CN201310745568 A CN 201310745568A CN 104739707 A CN104739707 A CN 104739707A
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Abstract
A traditional Chinese medicine liquid shampoo mainly includes a traditional Chinese medicine liquid, glycerin and deionized water B. The preparation method is as follows: (1), pouring the traditional Chinese medicine liquid into a water phase pot, and adding the glycerin into the water phase pot; (2) adding citric acid, and mixing; (3) adding deionized water A into a stainless steel barrel, adding cationic guar gum, and pouring the mixed liquid into the water phase pot; (4) adding fatty alcohol polyoxyethylene ether ammonium sulfate into the water phase pot; (5) adding dihydrogenated tallow-based phthalic diamide into the water phase pot; (6) adding linoleamide propyl hydroxypropyl quaternary ammonium salt and a methyl glucoside derivative into the water phase pot; (7) adding C12-16 alkyl glycoside and jojoba oil into the water phase pot; (8) heating an emulsification pot; (9) pumping water phase pot solution to the emulsification pot; (10) adding aster saponin; (11) adding macromolecular emulsified silicone oil into the emulsification pot, and adding small molecule emulsified silicone oil; (12) dissolving zinc pyrrolidone carboxylate and sodium benzoate with the deionized water B, and respectively adding the zinc pyrrolidone carboxylate and sodium benzoate into the emulsification pot; (13) adding cocamidopropyl betaine and (14) taking out of the pot. The traditional Chinese medicine liquid shampoo has the advantages of less added traditional Chinese medicine components, efficacy diversification and simple process.
Description
technical fieldthe present invention relates to hair washing technical field, particularly a kind of Chinese medicine shampoo and preparation method thereof.
background technologyshampoo is that the modern institute that has one's hair wash is indispensable, and shampoo on the market at present, of a great variety, function is also had nothing in common with each other, for people provide the selection of multiple hair-protecting health-care.But current most shampoo, more or less all contain chemical substance, as removing scurf and relieving itching ketoconazole, ZPT, 0ctopirox, 17-hydroxyl times his steroid dehydrogenase etc., maintenance silicone oil and cationic polymer, also have essence, antibacterial, antiseptic etc.Although these chemical substances serve positive effect, still there are some side effect.In recent years, begun one's study containing the shampoo of Chinese medicine additive.Its weak point: the Chinese medicine ingredients of interpolation is many, effect is single, complex process.
summary of the inventionthe Chinese medicine ingredients that the object of this invention is to provide a kind of interpolation is few, effect is diversified, the simple a kind of Chinese medicine shampoo of technique and preparation method thereof.
Technical scheme of the present invention is: a kind of Chinese medicine shampoo, its composition mainly comprises herb liquid (Dalian Mei Le biotechnology development corporation, Ltd. is in the patent of invention of December in 2013 application on the 28th), glycerol, citric acid, cation melon glue, deionized water A, AESA, two hydrogenated-tallow group phthalic amide, C12-16 alkyl polyglucoside, sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, Jojoba oil, methyl glucoside derivative, Radix Asteris Saponin, macromole emulsified silicone oil, micromolecule emulsified silicone oil, zinc pyrrolidone carboxylate, sodium benzoate, deionized water B and cocamido propyl betaine.Wherein, be 1 ultimate unit with herb liquid, glycerol, citric acid, cation melon glue, deionized water A, AESA, two hydrogenated-tallow group phthalic amide, C12-16 alkyl polyglucoside, sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, Jojoba oil, methyl glucoside derivative, Radix Asteris Saponin, macromole emulsified silicone oil, micromolecule emulsified silicone oil, zinc pyrrolidone carboxylate, sodium benzoate, the mass ratio of deionized water B and cocamido propyl betaine is 1:0.03026 ~ 0.03699, 1:0.00030 ~ 0.00037,1:0.00227 ~ 0.00277,1:0.11105 ~ 0.15795,1:0.13943 ~ 0.19682,1:0.00908 ~ 0.01110,1:0.11105 ~ 0.15795,1:0.00757 ~ 0.00925,1:0.00378 ~ 0. 00462,1:0.01513 ~ 0.01849,1:0.00757 ~ 0.00925,1:0.02270 ~ 0.02274,1:0.01513 ~ 0.01849,1:0.00454 ~ 0.00555,1:0.00303 ~ 0.00370,1:0.08322 ~ 0.10171,1:0.01513 ~ 0.01849.
The manufacture method of Chinese medicine shampoo realizes according to the following steps:
(1) getting herb liquid pours in aqueous phase pot, and glycerol joins in aqueous phase pot, and heated and stirred is to dissolving completely, and temperature controls at 75 DEG C;
(2) citric acid is added, stirring and dissolving;
(3) deionized water A is in stainless steel cask, by the dispersion of cation melon glue wherein, after the abundant moistening of cation melon glue, is poured into by mixed liquor in aqueous phase pot, stirs;
(4) AESA joins in aqueous phase pot, is stirred to and dissolves completely;
(5) two hydrogenated-tallow group phthalic amide joins in aqueous phase pot, is stirred to and dissolves completely;
(6) sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, methyl glucoside derivative join in aqueous phase pot, are stirred to and dissolve completely;
(7) C12-16 alkyl polyglucoside, Jojoba oil join in kettle, stir and within 10 minutes, cause evenly;
(8) emulsifying pot is heated to 40 DEG C, beats vacuum 0.07MPa(and do not add drainage screen);
(9) treat that aqueous phase pot solution is uniformly dissolved completely, stop stirring, solution is extracted in emulsifying pot, about temperature 70 C.Start emulsifying pot to stir, stir fast 80rpm;
(10) logical cooling water temperature, keep the cooling rate of falling 2 DEG C for 3 minutes, temperature reduces to 59 DEG C, stirs 20min; Temperature drops to 51 DEG C, adds Radix Asteris Saponin, stirs 5 minutes;
(11) 49 DEG C add macromole emulsified silicone oil and stir 5min in emulsifying pots, then add micromolecule emulsified silicone oil, stir 10 minutes;
(12) deionized water B, point two heatable container splendid attires, dissolve zinc pyrrolidone carboxylate and sodium benzoate respectively, can suitably heat, temperature does not exceed 50 DEG C; After dissolving completely, join in emulsifying pot respectively, 10 minutes interval times;
(13) greenhouse cooling adds cocamido propyl betaine to 45 DEG C, stirs; Sampling is PH, viscosity, after each index is adjusted, prepares discharge tank, opens ultra violet lamp room;
(14) temperature drops to about 38 DEG C, takes the dish out of the pot; Weigh yield rate, deliver to rest chamber.
The present invention compared with prior art tool has the following advantages: the Chinese medicine ingredients of interpolation is few, effect is diversified, technique is simple.
detailed description of the invention
Embodiment 1
The manufacture method of Chinese medicine shampoo realizes according to the following steps:
(1) getting herb liquid 1.1kg pours in aqueous phase pot, and glycerol 0.03026kg joins in aqueous phase pot, and heated and stirred is to dissolving completely, and temperature controls at 75 DEG C;
(2) citric acid 0.00030kg is added, stirring and dissolving;
(3) deionized water A0.11105kg is in stainless steel cask, is disperseed wherein by cation melon glue 0.00227kg, after the abundant moistening of cation melon glue, is poured into by mixed liquor in aqueous phase pot, stir;
(4) AESA 0.13943kg joins in aqueous phase pot, is stirred to and dissolves completely;
(5) two hydrogenated-tallow group phthalic amide 0.00908kg joins in aqueous phase pot, is stirred to and dissolves completely;
(6) sub-oleamidopropyl hydroxypropyl quaternary ammonium salt 0.00757kg, methyl glucoside derivative 0.01513kg join in aqueous phase pot, are stirred to and dissolve completely;
(7) C12-16 alkyl polyglucoside 0.11105kg, Jojoba oil 0.00378kg join in kettle, stir and within 10 minutes, cause evenly;
(8) emulsifying pot is heated to 40 DEG C, beats vacuum 0.07MPa(and do not add drainage screen);
(9) treat that aqueous phase pot solution is uniformly dissolved completely, stop stirring, solution is extracted in emulsifying pot, about temperature 70 C, start emulsifying pot and stir, stir fast 80rpm;
(10) logical cooling water temperature, keep the cooling rate of falling 2 DEG C for 3 minutes, temperature reduces to 59 DEG C, stirs 20min; Temperature drops to 51 DEG C, adds Radix Asteris Saponin 0.00757kg, stirs 5 minutes;
(11) 49 DEG C add macromole emulsified silicone oil 0.02270kg and stir 5min in emulsifying pots, then add micromolecule emulsified silicone oil 0.01513kg, stir 10 minutes;
(12) deionized water B0.08322kg, point two heatable container splendid attires, dissolve zinc pyrrolidone carboxylate 0.00454kg and sodium benzoate 0.00303kg respectively, can suitably heat, temperature does not exceed 50 DEG C; After dissolving completely, join in emulsifying pot respectively, 10 minutes interval times;
(13) greenhouse cooling adds cocamido propyl betaine 0.01513kg to 45 DEG C, stirs; Sampling is PH, viscosity, after each index is adjusted, prepares discharge tank, opens ultra violet lamp room;
(14) temperature drops to about 38 DEG C, takes the dish out of the pot; Weigh yield rate, deliver to rest chamber.
Embodiment 2
The manufacture method of Chinese medicine shampoo realizes according to the following steps:
(1) getting herb liquid 0.9kg pours in aqueous phase pot, and glycerol 0.03699kg joins in aqueous phase pot, and heated and stirred is to dissolving completely, and temperature controls at 75 DEG C;
(2) citric acid 0.00037kg is added, stirring and dissolving;
(3) deionized water A0.15795kg is in stainless steel cask, is disperseed wherein by cation melon glue 0.00277kg, after the abundant moistening of cation melon glue, is poured into by mixed liquor in aqueous phase pot, stir;
(4) AESA 0.19682kg joins in aqueous phase pot, is stirred to and dissolves completely;
(5) two hydrogenated-tallow group phthalic amide 0.01110kg joins in aqueous phase pot, is stirred to and dissolves completely;
(6) sub-oleamidopropyl hydroxypropyl quaternary ammonium salt 0.00925kg, methyl glucoside derivative 0.01849kg join in aqueous phase pot, are stirred to and dissolve completely;
(7) C12-16 alkyl polyglucoside 0.15795kg, Jojoba oil 0.0046kg join in kettle, stir and within 10 minutes, cause evenly;
(8) emulsifying pot is heated to 40 DEG C, beats vacuum 0.07MPa(and do not add drainage screen);
(9) treat that aqueous phase pot solution is uniformly dissolved completely, stop stirring, solution is extracted in emulsifying pot, about temperature 70 C, start emulsifying pot and stir, stir fast 80rpm;
(10) logical cooling water temperature, keep the cooling rate of falling 2 DEG C for 3 minutes, temperature reduces to 59 DEG C, stirs 20min; Temperature drops to 51 DEG C, adds Radix Asteris Saponin 0.00925kg, stirs 5 minutes;
(11) 49 DEG C add macromole emulsified silicone oil 0.02774kg and stir 5min in emulsifying pots, then add micromolecule emulsified silicone oil 0.01849kg, stir 10 minutes;
(12) deionized water B0.10171kg, point two heatable container splendid attires, dissolve zinc pyrrolidone carboxylate 0.00555kg and sodium benzoate 0.00370kg respectively, can suitably heat, temperature does not exceed 50 DEG C; After dissolving completely, join in emulsifying pot respectively, 10 minutes interval times;
(13) greenhouse cooling adds cocamido propyl betaine 0.01849kg to 45 DEG C, stirs; Sampling is PH, viscosity, after each index is adjusted, prepares discharge tank, opens ultra violet lamp room;
(14) temperature drops to about 38 DEG C, takes the dish out of the pot; Weigh yield rate, deliver to rest chamber.
Claims (2)
1. a Chinese medicine shampoo, is characterized in that: the raw material herb liquid comprised, glycerol, citric acid, cation melon glue, deionized water A, AESA, two hydrogenated-tallow group phthalic amide, C12-16 alkyl polyglucoside, sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, Jojoba oil, methyl glucoside derivative, Radix Asteris Saponin, macromole emulsified silicone oil, micromolecule emulsified silicone oil, zinc pyrrolidone carboxylate, sodium benzoate, deionized water B and cocamido propyl betaine are 1 ultimate unit with herb liquid, glycerol, citric acid, cation melon glue, deionized water A, AESA, two hydrogenated-tallow group phthalic amide, C12-16 alkyl polyglucoside, sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, Jojoba oil, methyl glucoside derivative, Radix Asteris Saponin, macromole emulsified silicone oil, micromolecule emulsified silicone oil, zinc pyrrolidone carboxylate, sodium benzoate, the mass ratio of deionized water B and cocamido propyl betaine is 1:0.03026 ~ 0.03699, 1:0.00030 ~ 0.00037,1:0.00227 ~ 0.00277,1:0.11105 ~ 0.15795,1:0.13943 ~ 0.19682,1:0.00908 ~ 0.01110,1:0.11105 ~ 0.15795,1:0.00757 ~ 0.00925,1:0.00378 ~ 0. 00462,1:0.01513 ~ 0.01849,1:0.00757 ~ 0.00925,1:0.02270 ~ 0.02274,1:0.01513 ~ 0.01849,1:0.00454 ~ 0.00555,1:0.00303 ~ 0.00370,1:0.08322 ~ 0.10171,1:0.01513 ~ 0.01849.
2. a preparation method for Chinese medicine shampoo, is characterized in that: (1) is got herb liquid and poured in aqueous phase pot, and glycerol joins in aqueous phase pot, and heated and stirred is to dissolving completely, and temperature controls at 75 DEG C;
(2) citric acid is added, stirring and dissolving;
(3) deionized water A is in stainless steel cask, by the dispersion of cation melon glue wherein, after the abundant moistening of cation melon glue, is poured into by mixed liquor in aqueous phase pot, stirs;
(4) AESA joins in aqueous phase pot, is stirred to and dissolves completely;
(5) two hydrogenated-tallow group phthalic amide joins in aqueous phase pot, is stirred to and dissolves completely;
(6) sub-oleamidopropyl hydroxypropyl quaternary ammonium salt, methyl glucoside derivative join in aqueous phase pot, are stirred to and dissolve completely;
(7) C12-16 alkyl polyglucoside, Jojoba oil join in kettle, stir and within 10 minutes, cause evenly;
(8) emulsifying pot is heated to 40 DEG C, beats vacuum 0.07MPa(and do not add drainage screen);
(9) treat that aqueous phase pot solution is uniformly dissolved completely, stop stirring, solution is extracted in emulsifying pot, about temperature 70 C,
Start emulsifying pot to stir, stir fast 80rpm;
(10) logical cooling water temperature, keep the cooling rate of falling 2 DEG C for 3 minutes, temperature reduces to 59 DEG C, stirs 20min; Temperature drops to 51 DEG C, adds Radix Asteris Saponin, stirs 5 minutes;
(11) 49 DEG C add macromole emulsified silicone oil and stir 5min in emulsifying pots, then add micromolecule emulsified silicone oil, stir 10 minutes;
(12) deionized water B, point two heatable container splendid attires, dissolve zinc pyrrolidone carboxylate and sodium benzoate respectively, can suitably heat, temperature does not exceed 50 DEG C; After dissolving completely, join in emulsifying pot respectively, 10 minutes interval times;
(13) greenhouse cooling adds cocamido propyl betaine to 45 DEG C, stirs; Sampling is PH, viscosity, after each index is adjusted, prepares discharge tank, opens ultra violet lamp room;
(14) temperature drops to about 38 DEG C, takes the dish out of the pot; Weigh yield rate, deliver to rest chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310745568.1A CN104739707A (en) | 2013-12-31 | 2013-12-31 | Traditional Chinese medicine liquid shampoo and preparation method thereof |
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| CN201310745568.1A CN104739707A (en) | 2013-12-31 | 2013-12-31 | Traditional Chinese medicine liquid shampoo and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105434232A (en) * | 2015-12-08 | 2016-03-30 | 广州暨南生物医药研究开发基地有限公司 | Shampoo containing folium artemisiae argyi and having anti-itch effect |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101485622A (en) * | 2009-03-03 | 2009-07-22 | 张嘉恒 | Shampoo containing extract of Moringa oleifera and preparation method thereof |
| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
-
2013
- 2013-12-31 CN CN201310745568.1A patent/CN104739707A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101485622A (en) * | 2009-03-03 | 2009-07-22 | 张嘉恒 | Shampoo containing extract of Moringa oleifera and preparation method thereof |
| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 王建新: "《化妆品原料手册》", 30 June 2009, 化学工业出版社 * |
| 黑龙江呼伦贝尔盟医药卫生学会: "《中药参考》", 31 December 1976 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105434232A (en) * | 2015-12-08 | 2016-03-30 | 广州暨南生物医药研究开发基地有限公司 | Shampoo containing folium artemisiae argyi and having anti-itch effect |
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