CN104705788A - Preparing method for large-particle additive for cigarette filter - Google Patents

Preparing method for large-particle additive for cigarette filter Download PDF

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Publication number
CN104705788A
CN104705788A CN201510025134.3A CN201510025134A CN104705788A CN 104705788 A CN104705788 A CN 104705788A CN 201510025134 A CN201510025134 A CN 201510025134A CN 104705788 A CN104705788 A CN 104705788A
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CN
China
Prior art keywords
adhesive agent
essence
cigarette filter
preparation
particle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510025134.3A
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Chinese (zh)
Inventor
缪明明
何沛
刘志华
申钦鹏
刘春波
王昆淼
张涛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Yunnan Industrial Co Ltd
Original Assignee
China Tobacco Yunnan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Yunnan Industrial Co Ltd filed Critical China Tobacco Yunnan Industrial Co Ltd
Priority to CN201510025134.3A priority Critical patent/CN104705788A/en
Publication of CN104705788A publication Critical patent/CN104705788A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

Abstract

The invention relates to a preparing method for a large-particle additive for a cigarette filter. An inner core material with a certain material and particle size is chosen, and a layer of an essence and fragrance or adsorbing material adhesive agent is attached on the surface of the inner core material in a spraying mode. The inner core material of the particle can be safe plastic, chitosan, colloid and the like. The essence and fragrance or adsorbing material adhesive agent is mixed with solvent according to a certain proportion. During the manufacturing process, the essence and fragrance or adsorbing material adhesive agent which is loaded at the surface of the inner core material make a loading layer tend to be evener through the mutual friction between the particles. By adjusting the width of the opening of a nozzle, pressure of a high-pressure pump, the drying temperature and the manufacturing time, the thickness of the manufactured particle attaching layer can be adjusted. The preparing method has the advantages that the controllability is good, the product is stable, the safety performance is high, wastes of fragrances or absorbing materials are avoided, the use ratio of the materials is improved, and the product cost is saved.

Description

A kind of preparation method of cigarette filter bulky grain additive
Technical field
The present invention relates to technical field of cigarettes, specifically a kind of preparation method of cigarette filter bulky grain additive.
Background technology
Filter tip is as the bridge between smoker and main flume, can not only part harmful components in filtering flue gas, and on cigarette tipped with filters, can TPM in effectively catching cigarette mainstream flue gas, reduce tar content, reduce the harm of flue gas to health and environment.
Research for many years and practical application display, filter tip not only Harm reduction techniques fall in Jiao play a part very important, while also can play the perfuming effect of cigarette.And this perfuming mode has fragrance controllability good, and do not produce thermal cracking, security is a little high, just progressively become research focus and the main flow of perfuming cigarette.But this perfuming mode also exists certain defect, namely only have outer fragrance component to work, internal layer does not participate in fragrance release substantially, and waste is serious.Therefore need the filter tip particulate additive adopting a kind of support type, by the skin of fragrance component load at cheap inner nuclear material, improve spices utilization rate.
Summary of the invention
The object of this invention is to provide a kind of preparation method of cigarette filter particulate additive, avoid the waste of spices or sorbing material, improve the utilization rate of material, save product cost.
The technical scheme of technical solution problem of the present invention is:
Select granularity inner nuclear material, at its surperficial spray attachment last layer spices adhesive agent or sorbing material adhesive agent, this particle inner nuclear material can be safety plastic, shitosan, colloid etc.;
Preparation method is as follows:
Inner nuclear material is dropped in heatable cylinder, the little 0.5-1mm of particle diameter needed for the fineness ratio of inner nuclear material, then by essence and flavoring agent adhesive agent or the mixing of sorbing material adhesive agent solvent, the ratio of adhesive agent and solvent is 4-6/4-6 w/w;
Suspension puts into storage vat, high-pressure pump is utilized to be transported in feeding shaft by essence and flavoring agent adhesive agent or sorbing material adhesive agent solution, being sprayed into by nozzle can in heated roller, essence and flavoring agent adhesive agent or sorbing material adhesive agent are loaded on the surface of inner nuclear material particle, and make load layer be tending towards even by friction each other, obtain filter tip particle.
By the pressure of the width of adjustment nozzle folding, high-pressure pump, baking temperature and Production Time, the thickness of made granular absorption layer can be regulated.
The composition of essence and flavoring agent adhesive agent: they are mixed by essence and flavoring agent 1-20%w/w, auxiliary material 70-90%w/w, food coloring 0.1-1%w/w, adhesive 1-10% w/w.
Described essence and flavoring agent is geraniol, ground coffee, agalloch eaglewood powder etc., and auxiliary material is starch, shitosan etc., and food coloring is caramel, edible natural pigment etc., and adhesive is sodium alginate, carragheen etc.
The composition of sorbing material adhesive agent: sorbing material 30-80%w/w, the 10-40%w/w such as supplementary product starch or shitosan, food coloring 0-1%w/w, adhesive 1-10% w/w;
Described sorbing material can be active carbon, bentonite, natural porous material etc.; Auxiliary material can be starch, shitosan etc., and food coloring can be caramel, edible natural pigment etc.; Adhesive can be sodium alginate, carragheen etc. .
Described solvent is water or ethanol.
Finally, filter tip particle is put into mouth rod former and produce, obtain the cigarette filter containing filter tip particle.
The advantage that the present invention has compared with the prior art: the method controllability is good, product is stablized, and security is high, and avoids the waste of spices or sorbing material, improves the utilization rate of material, has saved product cost.
Accompanying drawing explanation
Fig. 1 is the structural representation of spray attachment device of the present invention.
Wherein, 1-dog-house, 2-can heated roller, the snap close of 3-dog-house and cylinder junction, 4-feeding shaft, 5-nozzle, 6-storage vat, 7-high-pressure pump.
Detailed description of the invention
Device as shown in Figure 1, comprising can heated roller 2, storage vat 6, high-pressure pump 7, heated roller 2 can be provided with dog-house 1 and the snap close 3 with cylinder junction, heated roller center line can there is feeding shaft 4, feeding shaft has multiple nozzle 5, feeding shaft connects storage vat 6, and storage vat connects high-pressure pump 7.In length range in cylinder, arrange a nozzle every 30cm, the opening degree of nozzle can regulate.
Utilize device as shown in Figure 1, open snap close 3 and inner nuclear material is dropped in heated roller 2, and can close dog-house via dog-house 1, lock snap close 3.The granularity of inner nuclear material can adopt different sizes as required, and needed for general Selection radio, the little 0.5-1mm of particle diameter is advisable.Again essence and flavoring agent adhesive agent or sorbing material adhesive agent suspension are put into storage vat, start high-pressure pump and can heated roller 2.Utilize the pressure of high-pressure pump to be transported in feeding shaft 4 by essence and flavoring agent adhesive agent solution, and sprayed into by nozzle 5 can in heated roller 2.Now, due to can heated roller 2 in the rolling, essence and flavoring agent adhesive agent or sorbing material adhesive agent will be loaded on the surface of inner nuclear material particle, and make load layer be tending towards even by friction each other.Meanwhile, due to the heating of cylinder, the solvent in essence and flavoring agent adhesive agent or sorbing material will be gone by evaporation, the whole load of last active ingredient on the particle of inner nuclear material, the filter tip particulate additive needed for formation.By the pressure of the width of adjustment nozzle folding, high-pressure pump, baking temperature and Production Time, the thickness of made particle spray attachment layer can be regulated.
Embodiment 1:
At plastic grain area load one deck Powdered Activated Carbon that diameter is 2mm.In manufacturing process, in the active carbon adhesive agent used, active carbon is 75% w/w, and auxiliary material is starch is 20%w/w, and adhesive is sodium alginate is 5% w/w, they is mixed.Solvent is water, and the ratio of active carbon adhesive agent and water is 4/6 w/w.By spray attachment device by the above process, finally at plastic grain area load, a layer thickness is the active carbon layer of 0.5mm, obtains filter tip particle.This filter tip particle is added the content that significantly can reduce carbon monoxide in flue gas in cigarette filter.
Embodiment 2:
At chitosan particle area load one deck coffee powder that diameter is 2mm.In manufacturing process, in the ground coffee adhesive agent used, ground coffee is 15% w/w, and auxiliary material shitosan is 70%w/w, adhesive be sodium alginate is 15% w/w, they is mixed.Solvent is water, and the ratio of adhesive agent and water is 5/5 w/w.By spray attachment device, finally a layer thickness is the ground coffee last layer of 0.5mm at plastic grain area load, obtains filter tip particle.This particle is added in cigarette filter and can strengthen cigarette flavor, promotes cigarette quality.
Embodiment 3:
At gelatin particle area load one deck green tea powder that diameter is 3mm.In manufacturing process, in the green tea powder adhesive agent used, green tea powder is 14% w/w, and auxiliary material shitosan is 70%w/w; Edible pigment, chlorophyll is 1%; Adhesive carragheen is 15% w/w, they is mixed, and solvent is ethanol, and the ratio of adhesive agent and ethanol is 6/4 w/w.By spray attachment device, finally a layer thickness is the green tea powder layer of 1mm at plastic grain area load, obtains filter tip particle.This particle is added in cigarette filter and can strengthen cigarette flavor, promotes cigarette quality, and effectively can reduce the harmful components such as the phenol in flue gas.
Embodiment 4:
At hollow silica gel glue particle surface load one deck agalloch eaglewood spices that diameter is 3mm.In manufacturing process, in the agalloch eaglewood spices adhesive agent used, agalloch eaglewood powder is 5% w/w, and supplementary product starch is 85%w/w; Edible pigment caramel colorant is 0.5%; Adhesive carragheen is 9.5% w/w.Solvent is water, and the ratio of adhesive agent and water is 4/6 w/w, they is mixed.By spray attachment device, finally a layer thickness is the agalloch eaglewood spice layer of 0.7mm at plastic grain area load, obtains filter tip particle.This particle is added in cigarette filter and can strengthen cigarette flavor, promotes cigarette quality.
Embodiment 5:
Utilizing device described in literary composition, is macroreticular resin particle surface load one deck Herba Menthae powder of 1mm at diameter.In manufacturing process, in the Herba Menthae powder adhesive agent used, Herba Menthae powder is 20% w/w, and supplementary product starch is 75%w/w; Edible pigment, chlorophyll is 1%; Adhesive sodium alginate is 4% w/w, they is mixed, and solvent is water, and the ratio of adhesive agent and water is 5/5w/w.By spray attachment device, finally a layer thickness is the peppermint bisque of 0.5mm at plastic grain area load, obtains filter tip particle.This particle is added in cigarette filter and can strengthen cigarette flavor, promotes cigarette quality.

Claims (9)

1. a preparation method for cigarette filter particulate additive, is characterized in that the inner nuclear material selecting certain granules degree, and at its surperficial spray attachment last layer essence and flavoring agent or sorbing material adhesive agent, the inner nuclear material of this particle is safety plastic, shitosan, colloid:
Preparation method is as follows:
Inner nuclear material is dropped in heatable cylinder, the little 0.5-1mm of particle diameter needed for the fineness ratio of inner nuclear material, then by essence and flavoring agent adhesive agent or the mixing of sorbing material adhesive agent solvent, the ratio of adhesive agent and solvent is 4-6/4-6 w/w;
Suspension puts into storage vat, high-pressure pump is utilized to be transported in feeding shaft by essence and flavoring agent adhesive agent or sorbing material adhesive agent solution, being sprayed into by nozzle can in heated roller, essence and flavoring agent adhesive agent or sorbing material adhesive agent are loaded on the surface of inner nuclear material particle, and make load layer be tending towards even by friction each other, obtain filter tip particle.
2. the preparation method of cigarette filter particulate additive according to claim 1, it is characterized in that consisting of of essence and flavoring agent adhesive agent: they are mixed by essence and flavoring agent 1-20%w/w, auxiliary material 70-90%w/w, food coloring 0.1-1%w/w, adhesive 1-10% w/w.
3. the preparation method of cigarette filter particulate additive according to claim 1, is characterized in that described essence and flavoring agent is one or more in geraniol, ground coffee, agalloch eaglewood powder.
4. the preparation method of cigarette filter particulate additive according to claim 1, it is characterized in that consisting of of sorbing material adhesive agent: sorbing material 30-80%w/w, they are mixed by supplementary product starch or shitosan 10-40%w/w, food coloring 0-1%w/w, adhesive 1-10% w/w.
5. the preparation method of cigarette filter particulate additive according to claim 1, is characterized in that described sorbing material is the one in active carbon, bentonite, natural porous material.
6. the preparation method of cigarette filter particulate additive according to claim 1, the auxiliary material stated that it is characterized in that is starch or shitosan.
7. the preparation method of cigarette filter particulate additive according to claim 1, is characterized in that food coloring is caramel or edible natural pigment.
8. the preparation method of cigarette filter particulate additive according to claim 1, is characterized in that adhesive is sodium alginate or carragheen .
9. the preparation method of cigarette filter particulate additive according to claim 1, is characterized in that described solvent is water or ethanol.
CN201510025134.3A 2015-01-19 2015-01-19 Preparing method for large-particle additive for cigarette filter Pending CN104705788A (en)

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Application Number Priority Date Filing Date Title
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104939307A (en) * 2015-07-17 2015-09-30 云南中烟工业有限责任公司 Polarity spice carrier for cigarettes and application
CN105001988A (en) * 2015-07-17 2015-10-28 云南中烟工业有限责任公司 Preparation device and application method of three-layer sandwich-structure spice sustained-release filter tip additive
CN105029671A (en) * 2015-06-19 2015-11-11 武汉群辉科技有限公司 Color mixing method for tobacco product
CN105124754A (en) * 2015-07-17 2015-12-09 云南中烟工业有限责任公司 Non-polar spice carrying core for cigarettes and application of non-polar spice carrying core
CN115433634A (en) * 2022-08-16 2022-12-06 广东中烟工业有限责任公司 Alkali modified visual coloring flavor sustained-release particles and preparation method and application thereof

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CN1379654A (en) * 1999-10-15 2002-11-13 G·S·图层系统有限公司 Machine for coating granular articles and like
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CN101336752A (en) * 2007-07-06 2009-01-07 湖南中烟工业有限责任公司 Filter-tip capable of reducing hydrocyanic acid in cigarette flue gas
CN102271542A (en) * 2009-01-08 2011-12-07 日本烟草产业株式会社 Filter for cigarette
EP2631285A1 (en) * 2010-10-18 2013-08-28 Japan Tobacco, Inc. Method for manufacturing flavor-releasing granules, flavor-releasing granules, and cigarette filter containing flavor-releasing granules

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Publication number Priority date Publication date Assignee Title
US4407863A (en) * 1981-01-14 1983-10-04 Denki Kagaku Kogyo Kabushiki Kaisha Process for producing granule coated with tannic acid metal chelate compound
JPS6047670A (en) * 1983-08-23 1985-03-15 日水製薬株式会社 Adsorbing element for tobacco filter
CN2391611Y (en) * 1999-05-12 2000-08-16 王小伦 Machine for dressing of small pills of medicine
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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105029671A (en) * 2015-06-19 2015-11-11 武汉群辉科技有限公司 Color mixing method for tobacco product
CN104939307A (en) * 2015-07-17 2015-09-30 云南中烟工业有限责任公司 Polarity spice carrier for cigarettes and application
CN105001988A (en) * 2015-07-17 2015-10-28 云南中烟工业有限责任公司 Preparation device and application method of three-layer sandwich-structure spice sustained-release filter tip additive
CN105124754A (en) * 2015-07-17 2015-12-09 云南中烟工业有限责任公司 Non-polar spice carrying core for cigarettes and application of non-polar spice carrying core
CN105001988B (en) * 2015-07-17 2018-07-24 云南中烟工业有限责任公司 A kind of preparation facilities and its application process of three-layer sandwich structure spice slow-releasing additives of filter tip
CN105124754B (en) * 2015-07-17 2019-06-04 云南中烟工业有限责任公司 A kind of cigarette nonpolar fragrance load core and application
CN115433634A (en) * 2022-08-16 2022-12-06 广东中烟工业有限责任公司 Alkali modified visual coloring flavor sustained-release particles and preparation method and application thereof
CN115433634B (en) * 2022-08-16 2023-12-05 广东中烟工业有限责任公司 Alkali modified visual coloring fragrance slow-release particles and preparation method and application thereof

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Application publication date: 20150617