CN104673473A - Water-based grinding fluid and preparation method thereof - Google Patents
Water-based grinding fluid and preparation method thereof Download PDFInfo
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- CN104673473A CN104673473A CN201310634166.4A CN201310634166A CN104673473A CN 104673473 A CN104673473 A CN 104673473A CN 201310634166 A CN201310634166 A CN 201310634166A CN 104673473 A CN104673473 A CN 104673473A
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Abstract
The invention discloses a water-based grinding fluid and a preparation method thereof. The water-based grinding fluid is prepared from the following components by weight percent: 6-12% of a lubricating agent, 4-8% of an emulsifier, 1-5% of an antirust agent, 4-18% of a pH value regulating agent and 60-85% of water. The invention further provides a preparation method of the water-based grinding fluid. The preparation method comprises the following steps: firstly adding the water, the emulsifier and the pH value regulating agent to a reaction kettle to fully stir uniformly, adding the lubricating agent to the reaction kettle to fully emulsify and stirring uniformly under the reaction temperature of 25-70 DEG C, adding the antirust agent to the reaction kettle to fully mix, and controlling a pH value of the grinding fluid to be 8-10. The water-based grinding fluid has the advantages of good antirust performance, high integral yield of the grinding procedure, good lubricating property and easiness in subsequent cleaning.
Description
Technical field
The present invention relates to a kind of water-based milling liquid, particularly a kind of for carrying out water-based milling liquid of grinding and polishing and preparation method thereof to aluminum products surface.
Background technology
Al and Alalloy goods are applied increasingly extensive in the civilian industries such as aircraft industry and light fixture, opticinstrument, ornaments.In order to improve aluminium and aluminum products surface smoothness and glossiness, before alumilite process process, often need to carry out grinding and polishing process to aluminum products, thus have the surface quality of high minute surface after ensureing aluminum anode process.
Carrying out in abrasive polishing process, grinding fluid plays vital effect.The allotment of grinding fluid is the important factor improving grinding effect, and directly the overall yield of the speed of machined material, the surfaceness of machined material and grinding technics is removed in impact grinding.In grinding and polishing process, grinding miller and surface to be machined rub and produce a large amount of heats, produce more chip simultaneously, in order to take away fricative heat and grinding chip in time, improve service efficiency and the integral grinding yield of grinding pad, need to inject grinding fluid at grinding miller and surface to be machined, the salient features of grinding fluid be cooling, lubricate, clean, antirust.Oiliness lapping liquid has the defects such as serious, the follow-up clean difficulty of environmental pollution due to it, is progressively eliminated at present.In recent years, water-based milling liquid has the advantage that shows and obtains applying more and more widely in visual and germ resistance in cooling, cleaning, processing.But current commercially available multiple water-based milling liquid still comes with some shortcomings, the overall yield as there is etching problem and grinding technics when grinding the placement of rear aluminium alloy is on the low side.
Summary of the invention
In view of foregoing, be necessary to provide that a kind of rust-preventing characteristic is good, grinding yield is high for the water-based milling liquid to aluminum products surface grinding polishing.
A kind of water-based milling liquid, include lubricant, emulsifying agent, rust-preventive agent, pH adjusting agent and water, described lubricant is selected from as carboxylic acid, acid amides, fatty acid ester, alcohols, at least one in soap and sulphur system and chlorine system extreme pressure lubricant, described emulsifying agent is selected from as ethers, at least one in ester class and carbonate, described rust-preventive agent is selected from as barium salt, at least one in heterocycle organism and organic acid, described pH adjusting agent is selected from as mineral alkali, at least one in organic bases, the weight percent of this lubricant is 6 ~ 12%, the weight percent of this emulsifying agent is 4 ~ 8%, the weight percent of this rust-preventive agent is 1 ~ 5%, the weight percent of this pH adjusting agent be 4 ~ 18% and the weight percent of water be 60 ~ 85%.
A preparation method for water-based milling liquid, comprises the following steps:
Water, emulsifying agent, pH adjusting agent are joined in reactor and fully stirred evenly, and this emulsifying agent is selected from as at least one in ethers, ester class and carbonate, and this pH adjusting agent is selected from as at least one in mineral alkali, organic bases;
Lubricant is joined fully emulsified in reactor stirring, temperature of reaction is 25 ~ 70 DEG C, and this lubricant is selected from as at least one in carboxylic acid, fatty acid amide, fatty acid ester, alcohols, soap and sulphur system and chlorine system extreme pressure lubricant;
Joined in reactor by rust-preventive agent and mix, and control 8 ~ 10 by the pH of water-based milling liquid, this rust-preventive agent is selected from as barium salt, at least one in heterocycle organism and organic acid.
Present invention also offers a kind of using method of the water-based milling liquid for aluminum products surface grinding polishing, comprise the following steps:
Grinding fluid and water are pressed after 1:1 ~ 10 dilute, with abrasive material be the grinding pads such as P400 ~ P2400 sand paper, polishing wheel with the use of.
Compared to existing technology, the water-based milling liquid of aluminum products surface grinding polishing of the present invention has following advantage:
The compound prescription system be made up of lubricant, emulsifying agent and rust-preventive agent in the present invention effectively can form a kind of oil film in aluminum alloy surface, and isolated air and aluminium surface contact are corroded to prevent aluminum alloy surface, have excellent rust prevention during manufacture.
Select comparatively gentle pH adjusting agent in the present invention, this pH adjusting agent can produce chemical interactions (polishing force comprises mechanicals efforts and chemical interactions) in process of lapping, can not corrode aluminium alloy again simultaneously, have the advantages that grinding and polishing operation yield is high.
Blending process of the present invention is simple, easy to operate simultaneously, in follow-up cleaning, clean simple, noresidue.
Embodiment
Below by specific embodiment, the application's water-based milling liquid is described in detail.It should be noted that, described embodiment is only used for illustrating the composition, content and preparation method thereof of described aluminum products surface grinding polishing water-based milling liquid, and limits the protection domain of the application never in any form.
Aluminum products surface grinding polishing described in the application water-based milling liquid mainly contains lubricant, emulsifying agent, rust-preventive agent, pH adjusting agent and water.In this water-based milling liquid, the weight percent of this lubricant is 6 ~ 12%, the weight percent of this emulsifying agent is 4 ~ 8%, the weight percent of this rust-preventive agent is 1 ~ 5%, the weight percent of this pH adjusting agent be 4 ~ 18% and the weight percent of water be 60 ~ 85%.
This water-based milling liquid also can comprise sterilant and defoamer.When this water-based milling liquid comprises sterilant and defoamer, in this water-based milling liquid, the weight percent of lubricant is 2 ~ 12%, the weight percent of emulsifying agent is 2 ~ 8%, the weight percent of rust-preventive agent is 1 ~ 10%, the weight percent of pH adjusting agent is 0.5 ~ 20%, the weight percent of sterilant is 0.05 ~ 0.5%, and the weight percent of defoamer is 0.1 ~ 0.5%, and the weight percent of water is 50 ~ 80%.Preferably, the weight percent of this lubricant is 6 ~ 12%, the weight percent of this emulsifying agent is 4 ~ 8%, the weight percent of this rust-preventive agent is 1 ~ 5%, the weight percent of this pH adjusting agent is 3 ~ 18%, the weight percent of this sterilant is 0.1 ~ 0.5%, and the weight percent of this defoamer is 0.1 ~ 0.5%, and the weight percent of this water is 60 ~ 80%.
Described lubricant is selected from as at least one in carboxylic acid, acid amides, fatty acid ester, alcohols, soap and sulphur system and chlorine system extreme pressure lubricant.
This carboxylic acid is selected from as at least one in stearic acid, Palmiticacid.This acid amides is selected from as fatty acid amide.Described alcohols is selected from as at least one in fatty alcohol, glycerol polyoxyethylene glycol.This soap is selected from as lipid acid acid metallic soap.Preferably, described lubricant is selected from as at least one in fatty acid amide, fatty alcohol, polyoxyethylene glycol, glycerol.This lubricant can take away fricative heat and grinding chip in time, improves cleansing power.
Described emulsifying agent is selected from as at least one in ethers, ester class and carbonate.This ethers is selected from as at least one in alkylphenol polyoxyethylene, polyoxyethylene groups alcohol ether, this ester class is selected from as Triethanolamine Esters of Stearic Acid, and this carbonate is selected from as at least one in Sodium dodecylbenzene sulfonate, sodium laurylsulfonate, petroleum sodium sulfonate, lauric monoglyceride sodium sulfate, fatty alcohol-polyoxyethylene ether phosphoric acid salt, sodium polyacrylate, toxilic acid and acrylic copolymer.Preferably, this emulsifying agent is selected from as at least one in Sodium dodecylbenzene sulfonate, sodium laurylsulfonate and toxilic acid and acrylic copolymer.
Described rust-preventive agent is selected from as at least one in barium salt, heterocycle organism and organic acid.This barium salt is selected from as at least one in barium mahogany sulfonate, nonyl naphthalene barium sulfonate, and this heterocycle organism is selected from as at least one in methyl benzotriazazole, mercaptobenzothiazole, and this organic acid is selected from as dodecenylsuccinic acid.Preferably, this rust-preventive agent is selected from as methyl benzotriazazole.The composite aluminum products itself that can prevent of this rust-preventive agent and emulsifying agent produce corrosion phenomenon, have excellent rust prevention during manufacture.
Described pH adjusting agent is selected from as at least one in mineral alkali, organic bases.This mineral alkali is selected from as at least one in sodium hydroxide, potassium hydroxide, and this organic bases is selected from as at least one in diethanolamine, trolamine, hexamethylenetetramine, α-amino isopropyl alcohol, triethylamine and polymine.Preferably, this pH adjusting agent is selected from as at least one in trolamine and polymine.
Described sterilant is selected from as at least one in salt, nipagin esters and isothiazolinone.This salt is selected from as at least one in dodecyl dimethyl Benzylmagnesium chloride amine, Sodium Benzoate and sorb potassium alcoholate.Preferably, this sterilant is selected from as at least one in dodecyl dimethyl Benzylmagnesium chloride amine and Sodium Benzoate.This sterilant mainly plays the fungi-proofing effect of mildew-resistant.
Described defoamer is selected from as at least one in silicone oil, polyethers and higher alcohols.This silicone oil is selected from as at least one in dimethyl silicone oil, polyether modified silicon oil.Preferably, this defoamer is dimethyl silicone oil.This defoamer can play foam in eliminative reaction system, prevents a large amount of bubble from producing dispersion in atmosphere.
This water is preferably deionized water.
The compound prescription system that the application's aluminum products surface grinding polishing water-based milling liquid is made up of lubricant, emulsifying agent and rust-preventive agent effectively can form a kind of oil film in aluminum alloy surface, isolated air and aluminium surface contact are corroded to prevent aluminum alloy surface, have excellent rust prevention during manufacture.In addition, the application selects comparatively gentle pH adjusting agent, can produce chemical interactions (polishing force comprises mechanicals efforts and chemical interactions) in process of lapping, can not corrode aluminium alloy again simultaneously, have the advantages that grinding and polishing operation yield is high.
Aluminum products surface grinding polishing water-based milling liquid described in the application can be made up of following methods:
Water, emulsifying agent, pH adjusting agent are joined in reactor and fully stir evenly;
Lubricant is joined fully emulsified in reactor stirring, temperature of reaction is 25 ~ 70 DEG C;
Rust-preventive agent is joined in reactor and mixes, and the pH of water-based milling liquid controls 8 ~ 10.
In the preparation process of this water-based milling liquid, also can add sterilant and defoamer.
Composition below in conjunction with embodiment 1 ~ 3 pair of the application's water-based milling liquid is further described (ginseng table 1).The preparation method of each water-based milling liquid of this embodiment 1 ~ 3 is the same.This embodiment 1 ~ 3 is intended to composition and content thereof that water-based milling liquid is described." surplus " that occur in table 1 refers to that in water-based milling liquid, each component total content is the residual content of 100%.
The composition of the water-based milling liquid of table 1 embodiment 1 ~ 3 and content thereof
Performance Detection
By aqueous polishing liquid dilute with water obtained for embodiment 1-3, with solution collocation sand paper after dilution on automatic grinding machine arm to machining after aluminium alloy grind.Carry out yield statistics to 500 aluminium alloys of this operation section grinding, lapped face lines is even, draws grinding yield (ginseng table 2).Use water ultrasonic cleaning after aluminium alloy places 24 hours after grinding, observe aluminum alloy surface luminance brightness, corrosion condition and whether have lapping liquid residual.
The grinding yield of the water-based milling liquid of table 2 embodiment 1 ~ 3
As can be seen from Table 2,500 aluminium alloy gained grinding yields that the water-based milling liquid of the embodiment of the present application 1 ~ 3 grinds this operation section are high, and during for using aluminum products surface grinding polishing, water ultrasonic cleaning is used after aluminium alloy places 24 hours after grinding, aluminum alloy surface light is corrosion-free, remains without lapping liquid.
In sum; although by specific embodiments of the invention to invention has been detailed description; but persons skilled in the art should be understood that; above-described embodiment is the description of the preferred embodiment to the application; but not the restriction to the application's protection domain; persons skilled in the art are in the technical scope disclosed by the application, and the change that can expect easily, all within the protection domain of the application.
Claims (11)
1. a water-based milling liquid, it is characterized in that: described water-based milling liquid contains lubricant, emulsifying agent, rust-preventive agent, pH adjusting agent and water, described lubricant is selected from as carboxylic acid, acid amides, fatty acid ester, alcohols, at least one in soap and sulphur system and chlorine system extreme pressure lubricant, described emulsifying agent is selected from as ethers, at least one in ester class and carbonate, described rust-preventive agent is selected from as barium salt, at least one in heterocycle organism and organic acid, described pH adjusting agent is selected from as mineral alkali, at least one in organic bases, the weight percent of this lubricant is 6 ~ 12%, the weight percent of this emulsifying agent is 4 ~ 8%, the weight percent of this rust-preventive agent is 1 ~ 5%, the weight percent of this pH adjusting agent be 4 ~ 18% and the weight percent of water be 60 ~ 85%.
2. water-based milling liquid as claimed in claim 1, it is characterized in that: described water-based milling liquid also comprises sterilant and defoamer, this sterilant is selected from as at least one in salt, nipagin esters, isothiazolinone, and this defoamer is selected from as at least one in silicone oil, polyethers and higher alcohols.
3. water-based milling liquid as claimed in claim 2, it is characterized in that: the weight percent of described lubricant is 2 ~ 12%, the weight percent of emulsifying agent is 2 ~ 8%, the weight percent of rust-preventive agent is 1 ~ 10%, the weight percent of pH adjusting agent is 0.5 ~ 20%, the weight percent of sterilant is 0.05 ~ 0.5%, and the weight percent of defoamer is 0.1 ~ 0.5%, and the weight percent of water is 50 ~ 80%.
4. water-based milling liquid as claimed in claim 2, it is characterized in that: this salt is selected from as at least one in dodecyl dimethyl Benzylmagnesium chloride amine, Sodium Benzoate and sorb potassium alcoholate, and this silicone oil is selected from as at least one in dimethyl silicone oil and polyether modified silicon oil.
5. water-based milling liquid as claimed in claim 1, it is characterized in that: this carboxylic acid is selected from as at least one in stearic acid, Palmiticacid, this acid amides is selected from as fatty acid amide, this alcohols is selected from as at least one in fatty alcohol, glycerol polyoxyethylene glycol, and this soap is selected from as lipid acid acid metallic soap.
6. water-based milling liquid as claimed in claim 1, it is characterized in that: this ethers is selected from as at least one in alkylphenol polyoxyethylene, polyoxyethylene groups alcohol ether, this ester class is selected from as Triethanolamine Esters of Stearic Acid, and this carbonate is selected from as at least one in Sodium dodecylbenzene sulfonate, sodium laurylsulfonate, petroleum sodium sulfonate, lauric monoglyceride sodium sulfate, fatty alcohol-polyoxyethylene ether phosphoric acid salt, sodium polyacrylate, toxilic acid and acrylic copolymer.
7. water-based milling liquid as claimed in claim 1, it is characterized in that: this barium salt is selected from as at least one in barium mahogany sulfonate and nonyl naphthalene barium sulfonate, this heterocycle organism is selected from least one for being in methyl benzotriazazole, mercaptobenzothiazole, this organic acid can be dodecenylsuccinic acid, this mineral alkali is selected from as at least one in sodium hydroxide, potassium hydroxide, this organic bases is selected from as at least one in diethanolamine, trolamine, hexamethylenetetramine, α-amino isopropyl alcohol, triethylamine and polymine, and this water is deionized water.
8. a preparation method for water-based milling liquid, comprises the following steps:
Water, emulsifying agent, pH adjusting agent are joined in reactor and fully stirred evenly, and this water is deionized water, and this emulsifying agent is selected from as at least one in ethers, ester class and carbonate, and this pH adjusting agent is selected from as at least one in mineral alkali, organic bases;
Lubricant is joined fully emulsified in reactor stirring, temperature of reaction is 25 ~ 70 DEG C, and this lubricant is selected from as at least one in carboxylic acid, acid amides, fatty acid ester, alcohols, soap and sulphur system and chlorine system extreme pressure lubricant;
Joined in reactor by rust-preventive agent and mix, and the pH of water-based milling liquid controls 8 ~ 10, this rust-preventive agent is selected from as barium salt, at least one in heterocycle organism and organic acid.
9. the preparation method of water-based milling liquid as claimed in claim 8, it is characterized in that: in the preparation process of described water-based milling liquid, be also added with sterilant and defoamer, this sterilant is selected from as at least one in salt, nipagin esters, isothiazolinone, this defoamer is selected from as at least one in silicone oil, polyethers and higher alcohols, this salt is selected from as at least one in dodecyl dimethyl Benzylmagnesium chloride amine, Sodium Benzoate and sorb potassium alcoholate, this silicone oil is selected from as at least one in dimethyl silicone oil and polyether modified silicon oil, and this water is deionized water.
10. the preparation method of water-based milling liquid as claimed in claim 8, it is characterized in that: this ethers is selected from as at least one in alkylphenol polyoxyethylene, polyoxyethylene groups alcohol ether, this ester class is selected from as Triethanolamine Esters of Stearic Acid, and this carbonate is selected from as at least one in Sodium dodecylbenzene sulfonate, sodium laurylsulfonate, petroleum sodium sulfonate, lauric monoglyceride sodium sulfate, fatty alcohol-polyoxyethylene ether phosphoric acid salt, sodium polyacrylate, toxilic acid and acrylic copolymer.
The preparation method of 11. water-based milling liquids as claimed in claim 8, it is characterized in that: this mineral alkali is selected from as sodium hydroxide, at least one in potassium hydroxide, this organic bases is selected from as diethanolamine, trolamine, hexamethylenetetramine, α-amino isopropyl alcohol, at least one in triethylamine and polymine, this carboxylic acid is selected from as stearic acid, at least one in Palmiticacid, this acid amides is selected from as fatty acid amide, this alcohols is selected from as fatty alcohol, at least one in glycerol polyoxyethylene glycol, this soap is selected from as lipid acid acid metallic soap, this barium salt is selected from as barium mahogany sulfonate, at least one in nonyl naphthalene barium sulfonate, this heterocycle organism is selected from as being methyl benzotriazazole, at least one in mercaptobenzothiazole, this organic acid is selected from as dodecenylsuccinic acid.
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Application publication date: 20150603 |