CN106918648A - A kind of ultrasonic examination low temperature couplant composition and preparation method thereof - Google Patents

A kind of ultrasonic examination low temperature couplant composition and preparation method thereof Download PDF

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Publication number
CN106918648A
CN106918648A CN201710166022.9A CN201710166022A CN106918648A CN 106918648 A CN106918648 A CN 106918648A CN 201710166022 A CN201710166022 A CN 201710166022A CN 106918648 A CN106918648 A CN 106918648A
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CN
China
Prior art keywords
composition
low temperature
couplant
ultrasonic examination
examination low
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CN201710166022.9A
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Chinese (zh)
Inventor
包美红
宋小林
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Beijing Hexin Hexin Science And Technology Development Co Ltd
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Beijing Hexin Hexin Science And Technology Development Co Ltd
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Priority to CN201710166022.9A priority Critical patent/CN106918648A/en
Publication of CN106918648A publication Critical patent/CN106918648A/en
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/22—Details, e.g. general constructional or apparatus details
    • G01N29/28—Details, e.g. general constructional or apparatus details providing acoustic coupling, e.g. water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707—Polyethers, e.g. polyalkyleneoxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/26—Organic compounds containing oxygen
    • C11D7/263—Ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3218—Alkanolamines or alkanolimines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3281—Heterocyclic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/34—Organic compounds containing sulfur
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/40—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
    • C10M2207/046—Hydroxy ethers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/48—Slushing oils

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Emergency Medicine (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)

Abstract

The invention discloses a kind of ultrasonic examination low temperature couplant composition and preparation method thereof, said composition is made up of following raw material：Base oil, BTA, triethanolamine, petroleum sodium sulfonate, barium mahogany sulfonate, butyl and antifreeze additive.The couplant temperature applicable range is wide, and easy cleaning, rust-proof type are good, be more easy to use under low temperature, improves flaw detection precision and simultaneously ensures ultrasonic low temperature flaw detection effect.

Description

A kind of ultrasonic examination low temperature couplant composition and preparation method thereof
Technical field
The present invention relates to couplant field, more particularly to a kind of ultrasonic examination low temperature couplant composition and its preparation side Method.
Background technology
Ultrasonic examination low temperature couplant composition is presently used for, the mostly of use are oil base class couplants, such as machine oil, change Depressor oil, lubricating grease etc., but viscosity index (VI) is different, and usage amount is difficult to grasp, and low temperature cannot be used, and cause use cost high, is visited Hinder precision low or even cause the supersonic detector cannot to work.Not only clear up difficult, and there is pollution environment, be harmful to human body Problem.
The content of the invention
Based on the problems of prior art, it is an object of the invention to provide a kind of ultrasonic examination low temperature couplant group Compound and preparation method thereof, its temperature applicable range is wide, and viscosity index (VI) is low, is more easy to use under low temperature, it is ensured that ultrasonic low temperature is visited Hinder effect.
The purpose of the present invention is achieved through the following technical solutions：
The embodiment of the present invention provides a kind of a kind of 1, ultrasonic examination low temperature couplant composition, it is characterised in that the group Compound is made up of the raw material of following parts by weight：
The embodiment of the present invention also provides a kind of ultrasonic examination low temperature couplant composition, of the present invention for preparing Couplant composition, said composition each component is taken by formula of the present invention, under 0~40 DEG C of temperature conditions, in order will Base oil, BTA, triethanolamine, petroleum sodium sulfonate, barium mahogany sulfonate, butyl and antifreeze additive are successively Add, 30~90 minutes stirring while adding, until liquid-transparent, uniform not stratified, that is, obtain the couplant composition.
As seen from the above technical solution provided by the invention, couplant composition provided in an embodiment of the present invention, by Using the base oil and BTA, triethanolamine, petroleum sodium sulfonate, barium mahogany sulfonate, diethyl of specified quantitative in formula Glycol butyl ether and anti-addition are frozen agent addition agent and are coordinated so that the couplant is a kind of composition of lower viscosity oil-based, environmental protection, Solvent-borne type couplant pollution environment, the defect of harmful human body are avoided, and water miscible couplant is more prone to cleaning.The coupling Mixture composite flash-point is higher than 150 DEG C, non-ignitable not quick-fried, greatly improves the security in flaw detection operating process.The couplant Composition has cleaning action, and just flaw detection substrate surface is cleaned while flaw detection, kills two birds with one stone, and greatly improves Operating efficiency.In addition, flaw detection couplant composition of the invention can improve ultrasonic weave efficiency：Specially：Flaw detection speed can be improved Degree：Good fluidity, viscosity is low, Fast Filling space exploration, reduces the flaw detection time, improves flaw detection precision, reduces usage amount, drop Low production cost.Do not corrode metal：It is corrosion-free to ferrous metal and non-ferrous metal.Safety and environmental protection：Flash-point is high, nontoxic, It is biodegradable using raw material without natrium nitrosum and heavy metal.Applied environment is wide：Can make under 0 DEG C~50 DEG C environment With not influenceed by high humility and high-heat environment.Rust is not returned in flaw detection：It is different from other, metal surface after couplant flaw detection of the present invention Can antirust be up to 1 year.The use of base oil is that the easy-to-use water of light viscosity oil is cleaned：The present invention is without nothing contained in traditional couplant Machine salt, the residue after flaw detection is easy to be rinsed well with water.
Specific embodiment
With reference to particular content of the invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched State, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, Belong to protection scope of the present invention.
The embodiment of the present invention is specifically described in further detail below.
The embodiment of the present invention provides a kind of ultrasonic examination low temperature couplant composition, and said composition is by following parts by weight Raw material composition：
In above-mentioned couplant composition, antifreeze additive uses polyethylene glycol.
In above-mentioned couplant composition, the temperature in use of couplant composition is -50 DEG C~50 DEG C.
The embodiment of the present invention provides a kind of ultrasonic examination low temperature couplant composition, for preparing above-mentioned couplant group Compound, said composition each component is taken by above-mentioned formula, under 0~40 DEG C of temperature conditions, in order by base oil, the nitrogen of benzo three Azoles, triethanolamine, petroleum sodium sulfonate, barium mahogany sulfonate and antifreeze additive are sequentially added, 30~90 minutes stirring while adding, directly It is uniform not stratified to liquid-transparent, that is, obtain the couplant composition.
Couplant composition of the invention is described further with reference to specific embodiment:
Material name Embodiment 1 Embodiment 2 Embodiment 3
Base oil HVI 150 75.0 80.0 85.0
BTA 2.0 1.5 0.5
Triethanolamine 10.0 7.0 5.0
Petroleum sodium sulfonate 5.0 4.0 3.0
Barium mahogany sulfonate 2.0 1.0 1.0
Butyl 0.5 0.6 0.2
Antifreeze additive 5.5 5.9 5.3
Following table gives main physical and chemical index (JB/T 7453-94) table of couplant composition obtained in the present invention：
The couplant temperature can be seen that by the main physical and chemical index of above-described embodiment and couplant composition of the present invention The scope of application is wide, and easy cleaning, rust-proof type are good, be more easy to use under low temperature, improves flaw detection precision and simultaneously ensures ultrasonic low temperature flaw detection effect Really.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto, Any one skilled in the art in the technical scope of present disclosure, the change or replacement that can be readily occurred in, Should all be included within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection model of claims Enclose and be defined.

Claims (4)

1. a kind of ultrasonic examination low temperature couplant composition, it is characterised in that said composition by following parts by weight raw material Composition：
2. a kind of ultrasonic examination low temperature couplant composition according to claim 1, it is characterised in that described antifreeze to add Plus agent uses polyethylene glycol.
3. a kind of ultrasonic examination low temperature couplant composition according to claim 1, it is characterised in that the couplant The temperature in use of composition is -50 DEG C~50 DEG C.
4. a kind of ultrasonic examination low temperature couplant composition, it is characterised in that for preparing any one of claims 1 to 3 institute The couplant composition stated, said composition each component is taken by the formula of any one of claims 1 to 3, in 0~40 DEG C of temperature conditions Under, base oil, BTA, triethanolamine, petroleum sodium sulfonate, barium mahogany sulfonate and antifreeze additive are added successively in order Enter, 30~90 minutes stirring while adding, until liquid-transparent, uniform not stratified, that is, obtain the ultrasonic examination low temperature couplant Composition.
CN201710166022.9A 2017-03-20 2017-03-20 A kind of ultrasonic examination low temperature couplant composition and preparation method thereof Pending CN106918648A (en)

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CN106918648A true CN106918648A (en) 2017-07-04

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108132307A (en) * 2017-10-26 2018-06-08 湖南金化科技集团有限公司 A kind of rail examination industry couplant and preparation method thereof
CN108517242A (en) * 2018-03-30 2018-09-11 江苏捷达油品有限公司 A kind of anticorrosive emulsified oil and its preparation method and application of function lasting stability

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108132307A (en) * 2017-10-26 2018-06-08 湖南金化科技集团有限公司 A kind of rail examination industry couplant and preparation method thereof
CN108132307B (en) * 2017-10-26 2020-12-04 湖南金化科技集团有限公司 Industrial coupling agent for steel rail flaw detection and preparation method thereof
CN108517242A (en) * 2018-03-30 2018-09-11 江苏捷达油品有限公司 A kind of anticorrosive emulsified oil and its preparation method and application of function lasting stability

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Application publication date: 20170704