CN104667571A - 芦丁提取浸取设备 - Google Patents
芦丁提取浸取设备 Download PDFInfo
- Publication number
- CN104667571A CN104667571A CN201510063279.2A CN201510063279A CN104667571A CN 104667571 A CN104667571 A CN 104667571A CN 201510063279 A CN201510063279 A CN 201510063279A CN 104667571 A CN104667571 A CN 104667571A
- Authority
- CN
- China
- Prior art keywords
- main body
- extraction
- material container
- rutin
- equipment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 28
- JMGZEFIQIZZSBH-UHFFFAOYSA-N Bioquercetin Natural products CC1OC(OCC(O)C2OC(OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5)C(O)C2O)C(O)C(O)C1O JMGZEFIQIZZSBH-UHFFFAOYSA-N 0.000 title claims abstract description 23
- IVTMALDHFAHOGL-UHFFFAOYSA-N eriodictyol 7-O-rutinoside Natural products OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C=C3C(C(C(O)=C(O3)C=3C=C(O)C(O)=CC=3)=O)=C(O)C=2)O1 IVTMALDHFAHOGL-UHFFFAOYSA-N 0.000 title claims abstract description 23
- FDRQPMVGJOQVTL-UHFFFAOYSA-N quercetin rutinoside Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 FDRQPMVGJOQVTL-UHFFFAOYSA-N 0.000 title claims abstract description 23
- IKGXIBQEEMLURG-BKUODXTLSA-N rutin Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@@H]1OC[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-BKUODXTLSA-N 0.000 title claims abstract description 23
- ALABRVAAKCSLSC-UHFFFAOYSA-N rutin Natural products CC1OC(OCC2OC(O)C(O)C(O)C2O)C(O)C(O)C1OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5 ALABRVAAKCSLSC-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 235000005493 rutin Nutrition 0.000 title claims abstract description 23
- 229960004555 rutoside Drugs 0.000 title claims abstract description 23
- 238000002386 leaching Methods 0.000 title claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 45
- 239000002904 solvent Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 8
- 244000046101 Sophora japonica Species 0.000 description 4
- 235000010586 Sophora japonica Nutrition 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- IKGXIBQEEMLURG-UHFFFAOYSA-N Rutin Chemical compound OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011802 pulverized particle Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- 102100034279 Calcium-binding mitochondrial carrier protein Aralar2 Human genes 0.000 description 1
- 240000008620 Fagopyrum esculentum Species 0.000 description 1
- 235000009419 Fagopyrum esculentum Nutrition 0.000 description 1
- 235000014693 Fagopyrum tataricum Nutrition 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 241000219784 Sophora Species 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000002155 anti-virotic effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004856 capillary permeability Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 108010084210 citrin Proteins 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000015872 dietary supplement Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000008164 mustard oil Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 239000002455 scale inhibitor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
- C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
- C07H17/06—Benzopyran radicals
- C07H17/065—Benzo[b]pyrans
- C07H17/07—Benzo[b]pyran-4-ones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Extraction Or Liquid Replacement (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Claims (4)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510063279.2A CN104667571B (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备 |
CN201610800596.2A CN106397512A (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备的提取方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510063279.2A CN104667571B (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610800596.2A Division CN106397512A (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备的提取方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104667571A true CN104667571A (zh) | 2015-06-03 |
CN104667571B CN104667571B (zh) | 2017-02-08 |
Family
ID=53303481
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510063279.2A Expired - Fee Related CN104667571B (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备 |
CN201610800596.2A Pending CN106397512A (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备的提取方法 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610800596.2A Pending CN106397512A (zh) | 2015-02-06 | 2015-02-06 | 芦丁提取浸取设备的提取方法 |
Country Status (1)
Country | Link |
---|---|
CN (2) | CN104667571B (zh) |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1410423A (zh) * | 2001-09-28 | 2003-04-16 | 张杰克 | 提取芦丁的工艺方法 |
KR20060056583A (ko) * | 2004-11-22 | 2006-05-25 | 춘천시 | 메밀허브로부터 루틴 추출물 및 루틴 분말을 제조하는 방법 |
CN103435667A (zh) * | 2013-09-17 | 2013-12-11 | 南京通泽农业科技有限公司 | 一种从槐米中提取芦丁的新方法 |
CN103752034A (zh) * | 2014-01-26 | 2014-04-30 | 桂林茗兴生物科技有限公司 | 芦丁蒸煮提取出渣装置 |
CN204619424U (zh) * | 2015-02-06 | 2015-09-09 | 徐大鹏 | 芦丁提取浸取设备 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1554464A (zh) * | 2003-12-19 | 2004-12-15 | 上海烟草(集团)公司 | 一种连续萃取的方法 |
CN1687063A (zh) * | 2005-04-19 | 2005-10-26 | 黑龙江麦迪欣澳逸医药技术咨询有限公司 | 一种无菌高纯度氧化苦参碱的制备方法 |
WO2008122990A1 (en) * | 2007-04-04 | 2008-10-16 | Almet Corporation Limited | Compacting upflow extractor and method of using it |
CN203540122U (zh) * | 2013-11-25 | 2014-04-16 | 吉首大学 | 真空脉动式杜仲胶提取装置 |
-
2015
- 2015-02-06 CN CN201510063279.2A patent/CN104667571B/zh not_active Expired - Fee Related
- 2015-02-06 CN CN201610800596.2A patent/CN106397512A/zh active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1410423A (zh) * | 2001-09-28 | 2003-04-16 | 张杰克 | 提取芦丁的工艺方法 |
KR20060056583A (ko) * | 2004-11-22 | 2006-05-25 | 춘천시 | 메밀허브로부터 루틴 추출물 및 루틴 분말을 제조하는 방법 |
CN103435667A (zh) * | 2013-09-17 | 2013-12-11 | 南京通泽农业科技有限公司 | 一种从槐米中提取芦丁的新方法 |
CN103752034A (zh) * | 2014-01-26 | 2014-04-30 | 桂林茗兴生物科技有限公司 | 芦丁蒸煮提取出渣装置 |
CN204619424U (zh) * | 2015-02-06 | 2015-09-09 | 徐大鹏 | 芦丁提取浸取设备 |
Also Published As
Publication number | Publication date |
---|---|
CN106397512A (zh) | 2017-02-15 |
CN104667571B (zh) | 2017-02-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Wei Guozhen Inventor before: Xu Dapeng |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20161010 Address after: 362302 Quanzhou Province, Nanan City, the United States and the United States and the town of innovation road, building innovation, building on the ground floor of the multi dimensional space two Applicant after: HARBIN WEIPING TECHNOLOGY DEVELOPMENT CO., LTD. Address before: 535004, the Guangxi Zhuang Autonomous Region, Qinzhou Qinzhou Economic Development Zone, fruit hill operating area No. 1 Applicant before: Xu Dapeng |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20190909 Address after: 535000 West Suburb Industrial Zone of Jinhaiwan West Street, Qinzhou City, Guangxi Zhuang Autonomous Region Patentee after: Guangxi Mingou Pharmaceutical Co., Ltd. Address before: 362302, Quanzhou, Fujian, Nanan City, Xia Mei Town, innovation road, building two, multi dimensional public space Patentee before: HARBIN WEIPING TECHNOLOGY DEVELOPMENT CO., LTD. |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170208 Termination date: 20210206 |