CN104666184A - Traditional Chinese medicine toothpaste with capability of freshening breath - Google Patents

Abstract

The invention discloses a traditional Chinese medicine toothpaste with the capability of freshening breath and relates to the technical field of toothpastes. The traditional Chinese medicine toothpaste is prepared from the following components in percentage by weight: 0.5-2 percent of a fennel extractive, 0.5-2 percent of a radix curcumae extractive, 0.5-2 percent of a coptis chinensis extractive, 0.5-2 percent of a green tea extractive, 5-7 percent of modified bamboo charcoal powder, 21-50 percent of a humectant, 1.2-1.5 percent of a thickener, 10-45 percent of a friction agent, 2.0-2.2 percent of a foaming agent, 0.2-0.3 percent of saccharin sodium, 0.10 percent of nipagin ester, 0.2-0.3 percent of sodium pyrophosphate and the balance of purified water. Compared with the prior art, the traditional Chinese medicine toothpaste disclosed by the invention has the advantages that the oral gas is improved commonly by utilizing the adsorption ability of the modified bamboo charcoal powder, the bacteriostatic ability of the coptis chinensis extractive and the green tea extractive and the aromas of the fennel extractive and the radix curcumae extractive, so that the fresh air in an oral cavity is prolonged.

Description

Breath freshening Chinese medicinal toothpaste

Technical field

The present invention relates to Chinese medicinal toothpaste technical field, especially breath freshening Chinese medicinal toothpaste.

Background technology

Dental care product is clean and health product indispensable in people's daily life, and this series products is of a great variety, is mainly used in keeping oral cavity and cleaning of teeth, promotion breath freshening, nurses gingiva, safeguards oral cavity good environment etc.; And toothpaste indispensable cavity sanitary product in people's daily life especially; In recent years, because consumer healthcare realizes continuous enhancing, more requirement is proposed to toothpaste, also to increase some auxiliary prevention oral diseases except cleaning one's teeth, oral cavity being had to the function of nursing health effect, therefore in domestic and international toothpaste, there is various functional product and become the market mainstream, again due to the advantage that Chinese medicinal plant active component has the Western medicine such as natural, safe incomparable, therefore with the functional emphasis becoming Developing of active ingredient of Chinese herbs on market.

Breath freshening is the basic expressions that oral cavity does not have abnormal flavour, and halitosis certainly will produce halitosis.The Main Ingredients and Appearance of halitosis abnormal smells from the patient is volatile sulfur compounds (volatilesulfur compounds, VSCs), and wherein 90% is hydrogen sulfide (H2S) and methanthiol (CH3SH).Large quantity research proves, oral microorganism and halitosis and implication medium sulphide content in close relations, wherein spirillum is one of oral microorganism relevant with the generation of volatilize in oral cavity sulfur compound and halitosis.Therefore, breath freshening be made, must halitosis be removed.

Summary of the invention

The problem that the present invention solves is to provide a kind of breath freshening Chinese medicinal toothpaste, and this Chinese medicinal toothpaste has the effect that effectively can extend the oral cavity halitosis pure and fresh time.

In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is: the percentage by weight of its component is as follows:

Fructus Foeniculi extract 0.5%-2%; Radix Curcumae extract 0.5-2%; Rhizoma Coptidis extract 0.5-2%; Green tea extract 0.5-2%; Modified bamboo powdered carbon 5-7%; Wetting agent 21%-50%; Thickening agent 1.2%-1.5%; Abrasivus 10%-45%; Foaming agent 2.0%-2.2%; Saccharin sodium 0.2%-0.3%; Nipagin ester 0.10%; Tetrasodium pyrophosphate 0.2%-0.3%; Pure water surplus.

In technique scheme, scheme can also be more specifically: described wetting agent is the mixture of sorbitol, glycerol, and described abrasivus is the one in calcium phosphate dibasic dihydrate, aluminium hydroxide or silicon dioxide; Described thickening agent is the one in sodium carboxymethyl cellulose, hydroxyethyl-cellulose or carrageenan; Described foaming agent is the one in sodium lauryl sulphate, sodium lauroyl sarcosine.

The said Fructus Foeniculi of the present invention is the dry mature fruit of Umbelliferae herbaceos perennial Fructus Foeniculi.Gas is aromatic, and taste is sweet, Xin Wen, and dispersing cold for relieving pain can control hernia stomachache, testis swelling and hanging down of either of the testes distending pain, dysmenorrhea.

Radix Curcumae of the present invention is the tuber of Zingiberaceae herbaceos perennial Rhizoma Curcumae Longae, RADIX CURCUMAE, Rhizoma Curcumae etc.Feeble QI is fragrant, has Rhizoma Zingiberis Recens taste.Arduous cold, blood-activating and qi-promoting pain relieving, dispersing the stagnated live-QI to relieve the stagnation of QI, breast, the side of body, the stomachache for the treatment of qi depression to blood stasis.Especially women's abdominal pain during menstruation, mammary swelling etc.Clear dampness-heat in the liver and gallbladder, and can cholagogic and lithagogue, for cholelithiasis.Can also control early rich by turmeric powder.

Rhizoma Coptidis of the present invention, another name Wang Lian, Zhi Lian are the rhizome of ranunculaceae plant Rhizoma Coptidis, Coptis deltoidea C.Y.Cheng et Hsiao, coptis omeiensis or Coptis teeta; Rhizoma Coptidis is used as medicine with rhizome, has inhibitory action to various pathogenic bacteria.

Green tea extract of the present invention is the active component extracted from green tea blade, mainly comprises tea polyphenols (catechin) etc.; There is the effect such as antioxidation, scavenging free radicals.

Modification bamboo charcoal of the present invention, its bamboo charcoal than great, space is many, has super large surface area, specific surface area is up to more than 300m2/g, be 6 times of general active carbon, extremely strong absorption property can effectively absorb mercaptan, thioether class smells the various harmful chemicals such as taste, and material eliminates bad smell.Modified through copper nitrate, bamboo charcoal not only remains original performance, and due to the existence of Cu2+, greatly strengthen the bactericidal property of bamboo charcoal, absorbing volatile sulphur compound, the ability as hydrogen sulfide, methyl mercaptan and diethyl sulfide also significantly improves.

Use with the form of Fructus Foeniculi extract, Radix Curcumae extract, Rhizoma Coptidis extract and green tea extract in the present invention, the extracting method of Fructus Foeniculi extract of the present invention, Radix Curcumae extract, Rhizoma Coptidis extract and green tea extract is that the medicinal effects of every taste Chinese medicine is broken into fine powder, cross 150 mesh sieves, 3 hours are extracted with the alcohol heating reflux of 10 times amount, extract 3 times, then extracting solution concentrating under reduced pressure become extractum or be dried to powdery; Extracting method is not limited to said method, and the additive method such as supercritical extraction, ultrasonic extraction also can be adopted to extract.

Prove through overtesting, add using Fructus Foeniculi extract, Radix Curcumae extract, Rhizoma Coptidis extract and green tea extract as active ingredient of Chinese herbs in this toothpaste, add modified bamboo powdered carbon again, utilize the bacteriostasis of the absorbability of modified bamboo powdered carbon, Rhizoma Coptidis extract and green tea extract and Fructus Foeniculi extract, the fragrance of Radix Curcumae extract improves oral cavity gas jointly, intraoral fresh air is extended.

Detailed description of the invention

Below in conjunction with embodiment, the present invention will be further described.In following each embodiment, involved percentage ratio except as otherwise noted, is all calculate by weight percentage.

The Chinese medicinal toothpaste constitutive material of embodiment 1-5 and weight percent content are as following table:

the preparation of above-mentioned toothpaste:

The salt such as saccharin sodium, tetrasodium pyrophosphate raw material is dissolved in gauge water in advance;

Wetting agent is added in Manufacturing medicine extract machine, thickening agent is added wherein, after high-speed stirred 8-10 minute, previous solu is added in wetting agent, continue to be stirred to thickening agent and disperse completely;

Add abrasivus, modification powdered carbon, foaming agent, under vacuo high-speed stirred 10 minutes;

Add Fructus Foeniculi extract, Radix Curcumae extract, Rhizoma Coptidis extract and green tea extract and Nipagin ester, continue high-speed stirred 5-8 minute under vacuo.Complete cream initial vacuum processed degree requirement at more than 0.096MPa;

Mastic multiple tube is packed.

clinical trial part:

1, sulfide analyzer analytic process

Use portable sulfide analyzer (Halimeter 4710-3 type, American I nterscan company manufactures), directly read the ppb concentration value of experimenter's implication medium sulphide content (volatile sulfur comounds, VSCs), record implication value.

Method requires: before test, first by instrument adjustment 0, advises tester to remain silent 2min.Be connected with analyzer plastic suction pipe one end during test, the other end inserts 3cm in experimenter's mouth, can not contact with back, lip.Advise experimenter's nasal respiration, when peak value appears in instrument, take out suction pipe, record peak value.Again measure after numerical value back to zero, repeat 3 times, get its meansigma methods.

2, samples selection:

Be greater than 150 ppb persons for entry standard with VSCs, and experimenter can not have digestive system, respiratory system, whole body system disease, suffer from extensive dental caries and periodontal disease, experimental session can not use non-hormone anti-inflammatory agent or antibiotic person in continuous more than 3 days.

3, material:

Consumer uses embodiment 2,4,5 toothpaste and blank toothpaste respectively.A toothpaste is embodiment 2, B toothpaste be embodiment 4, C toothpaste be embodiment 5, D toothpaste is not containing the blank sample of fresh breath composition.

4, test operation

At the trial, 160 people of inclusive criteria are divided into 4 groups at random, often organize 40 people.Provide different toothpaste and toothbrush to each experimenter by group, and given some on the spot guidance by special messenger and brush teeth, brush teeth 3 minutes at every turn, got back to after 1 hour, 12 hours and check that place is rechecked.After this, toothpaste and toothbrush are taken home and sooner or later respectively to be used once by experimental subject every day, each 3 minutes, can not use other oral health care products in the meantime or take antiinflammatory medicine, use 1 week and 2 Zhou Houzai recheck.The results are shown in following table:

Experiment before and after with Halimiter detect implication value ( ± s, ppb)

Interpretation of result: can see from upper table, each group implication value there was no significant difference before and after experiment, illustrative experiment baseline has comparability.After using toothpaste to brush teeth, the implication value often organized has certain decline, even if illustrating brushes teeth with ordinary toothpaste also can keep the pure and fresh of implication to a certain extent, but uses the pure and fresh component dentifrice contained by this experiment to brush teeth, the degree of breath freshening can be improved.After brushing teeth 12 hours, use No. A, No. B, C toothpaste be better than using the fresh breath effects of control sample, illustrates use this experiment contain effect that deodorization component dentifrice has the prolongation breath freshening time; After brushing teeth 1 week, two weeks, use No. A, No. B, C toothpaste has good antihalitosis effect.

Claims (2)

1. a breath freshening Chinese medicinal toothpaste, is characterized in that being made up of the component of following percentage by weight:

Fructus Foeniculi extract 0.5%-2%; Radix Curcumae extract 0.5-2%; Rhizoma Coptidis extract 0.5-2%; Green tea extract 0.5-2%; Modified bamboo powdered carbon 5-7%; Wetting agent 21%-50%; Thickening agent 1.2%-1.5%; Abrasivus 10%-45%; Foaming agent 2.0%-2.2%; Saccharin sodium 0.2%-0.3%; Nipagin ester 0.10%; Tetrasodium pyrophosphate 0.2%-0.3%; Pure water surplus.

2. breath freshening Chinese medicinal toothpaste according to claim 1, is characterized in that: described wetting agent is the mixture of sorbitol, glycerol, and described abrasivus is the one in calcium phosphate dibasic dihydrate, aluminium hydroxide or silicon dioxide; Described thickening agent is the one in sodium carboxymethyl cellulose, hydroxyethyl-cellulose or carrageenan; Described foaming agent is the one in sodium lauryl sulphate, sodium lauroyl sarcosine.