CN105748339A - Toothpaste with green tea extract and method for preparing toothpaste - Google Patents
Toothpaste with green tea extract and method for preparing toothpaste Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
The invention provides toothpaste with green tea extract and a method for preparing the toothpaste.The toothpaste comprises, by weight, 0.05-0.2 part of the green tea extract, 0.2-1.5 parts of green tea essence, 25-40 parts of friction agents, 29.5-41.5 parts of humectants, 0.65-1.85 parts of thickening agents, 1.5-4 parts of foaming agents, 0.01-0.1 part of brilliant blue, 0.01-0.1 part of apple green, 0.05-0.35 part of saccharin sodium, 0.2-0.6 part of preservatives, 0.1-0.5 part of whitening agents and 25-35 parts of water.The toothpaste with the green tea extract and the method have the advantages that the toothpaste has functions of preventing decayed teeth and removing halitosis, sterilization and inflammation diminishing effects can be realized, and the toothpaste and the method have excellent clinical application prospects.
Description
Technical field
The present invention relates to toothpaste containing green tea extract and preparation method thereof.
Background technology
Dental care product is cleaning indispensable in people's daily life and health product, and this series products is of a great variety, is mainly used in keeping oral cavity and cleaning of teeth, promotion breath freshening, nurses gingiva, safeguards oral cavity good environment etc.；And indispensable oral cavity cleaning hygienic article in toothpaste people's daily life especially；In recent years, owing to consumer healthcare realizes continuous enhancing, natural, safe requirement is pursued；In order to adapt to consumer demand, therefore having various functional product in domestic and international toothpaste becomes the market mainstream, again owing to Chinese medicinal plant active component has the advantages such as natural, safe, therefore utilizes the functional emphasis becoming Developing of active ingredient of Chinese herbs on market.
The main component of halitosis abnormal smells from the patient is volatile sulfur compounds (volatilesulfurcompounds, VSCs), wherein 90% hydrogen sulfide (H2And methanthiol (CH S)3SH).Big quantity research proves, oral microorganism is in close relations with halitosis and implication medium sulphide content, and wherein spirillum is one of oral microorganism relevant with the generation of volatilize in oral cavity sulfur compound and halitosis.Therefore, for breath freshening, it is necessary to eliminate halitosis.
Folium Camelliae sinensis has the effect such as antibacterial anti-inflammatory, antiviral.Nan Zhandong etc., " Folium Camelliae sinensis extract application in toothpaste ", household chemicals science volume the 10th October the 35th in 2012 is interim, discloses a kind of toothpaste adopting Pu'er tea to prepare, but it is difficult to remove stink substance, it is impossible to effectively maintain breath freshening.
Summary of the invention
It is an object of the invention to provide a kind of toothpaste containing green tea and preparation method thereof.
The present invention contains the toothpaste of green tea extract, and it includes the component of following weight proportion:
Green tea extract 0.05 part-0.2 part；Green tea essence 0.2 part-1.5 parts；Abrasivus 25 parts-40 parts；Wetting agent 29.5-41.5 part；Thickening agent 0.65-1.85 part；Foaming agent 1.5 parts-4 parts；Light blue 0.01 part-0.1 part；Light green 0.01 part-0.1 part；Saccharin sodium 0.05 part-0.35 part；Preservative 0.2 part-0.6 part；Brilliant white agent 0.1-0.5 part；Water 25-35 part.
Preferably, it includes the component of following weight proportion:
Green tea extract 0.2 part；Green tea essence 1.5 parts；Abrasivus 40 parts；Wetting agent 41.5 parts；Thickening agent 1.85 parts；Foaming agent 4 parts；Light blue 0.1 part；Light green 0.1 part；Saccharin sodium 0.35 part；Preservative 0.6 part；Brilliant white agent 0.5 part；35 parts of water.
Preferably, it includes the component of following weight proportion:
Green tea extract 0.1 part；Green tea essence 0.8 part；Abrasivus 30 parts；Wetting agent 34.5 parts；Thickening agent 1.2 parts；Foaming agent 2.5 parts；Light blue 0.05 part；Light green 0.05 part；Saccharin sodium 0.2 part；Preservative 0.4 part；Brilliant white agent 0.3 part；30 parts of water.
Preferably, described green tea extract is prepared as follows:
A, taking green tea, pulverize, add water mixing；
B, supersound extraction, the time of extraction is 15-30min, and the temperature of extraction is 55-70 DEG C, obtains lixiviating solution, is cooled to 15-25 DEG C in 30-50min；
C, filtration, obtain filtrate, centrifugal, obtains the moisture green tea extract not higher than 45wt%.
Preferably, in step a, described pulverizing is that to be crushed to fineness be 45-75 order, described in the mixing that adds water be tea powder is minced with water according to parts by weight 1:(110-190 at 15-25 DEG C of temperature) ratio mix；In step b, the power of supersound extraction is 1200w；In step c, described filtration is filter pressing, and described centrifugal rotating speed is 5000-7500r/min, and the centrifugal time is 10-20min.
Preferably, described wetting agent is sorbitol and PEG400, and the consumption of the two is 28-38 part and 1.5-3.5 part, and the consumption of the two is preferably 32-38 part and 2.5-3.5 part；
And/or, described abrasivus is hydrated silica；
And/or, described thickening agent is carboxymethyl cellulose, carrageenan 3189 and xanthan gum, the consumption of the two respectively 0.5-1.0 part, 0.05-0.35 part and 0.1-0.5 part；
And/or, described foaming agent is sodium lauryl sulphate；
And/or, described light blue is 1% light blue；
And/or, described light green be 1% light green；
And/or, described preservative is sodium benzoate；
And/or, described brilliant white agent is titanium dioxide.
The preparation method that present invention also offers aforementioned toothpaste, step is as follows:
(1) raw material is taken according to aforementioned proportioning, soluble in water to saccharin sodium and preservative；
(2) wetting agent is added in Manufacturing medicine extract machine, thickening agent, light green and light blue are added wherein, stirs 6-10min；
(3) add the solution of above-mentioned steps (1), continue stirring and be completely dispersed to thickening agent, light green and light blue；
(4) add abrasivus and brilliant white agent, stir 10min under vacuo；
(5) add green tea extract, continue stirring 6-10min, add Green tea essence, mixing.
Preferably, step (1), (4), (5) middle rotating speed stirred are 5000 turns/min.
The toothpaste that the present invention contains green tea extract has pre-anti-caries, goes effect of halitosis, has the effect of bactericidal antiphlogistic, and potential applicability in clinical practice is good.
Below by detailed description of the invention, the present invention is described in further details, but it is not limitation of the present invention, foregoing according to the present invention, ordinary technical knowledge and customary means according to this area, without departing under the above-mentioned basic fundamental thought premise of the present invention, it is also possible to make the amendment of other various ways, replacement or change.
Detailed description of the invention
The embodiment present invention contains the preparation of the toothpaste of green tea extract
1, the source of material and preparation
Green tea extract, is prepared as follows:
(1) green tea is taken, at circulating chilled water, on the rocks or become fineness to mince for the tea powder of 45-75 order with liquid nitrogen, dry ice for attrition grinding in the cooling system of cold media；(2) at 15-25 DEG C of temperature, the tea powder of step (1) gained is minced and mix homogeneously according to the ratio of parts by weight 1:110-190 with water, ultrasonic (ultrasonic power is 1200W) ripple lixiviate 15-30min, lixiviate temperature 55-70 DEG C, obtains lixiviating solution；(3) lixiviating solution of step (2) gained is cooled to rapidly 15-25 DEG C in 30-50min, tea grounds is removed in filter pressing, the extracting solution stayed is centrifugal 10-20min when revolution is 5000-7500r/min, the centrifugal gained supernatant of removal, repeated centrifugation operates 3-10 time, obtains the green tea extract of moisture≤45wt%.
Green tea essence: buy the fragrant (Shanghai) Co., Ltd. in moral；Buy the fragrant (Shanghai) Co., Ltd. in moral.
2, preparation
The weight proportion of each component is as shown in table 1 below:
The preparation of above-mentioned toothpaste:
(1) soluble in water to saccharin sodium and sodium benzoate；
(2) sorbitol and PEG400 are added in Manufacturing medicine extract machine, light green to thickening agent CMC, carrageenan 3189 and xanthan gum and 1%, 1% light blue are added wherein, stirs (rotating speed is 5000 turns/min) 6-10min；
(3) adding the solution of above-mentioned steps (1), continuation stirring is light green to thickening agent and 1%, 1% light blue is completely dispersed；
(4) hydrated silica and titanium dioxide are added, under vacuo stirring (rotating speed is 5000 turns/min) 10min；
(5) add green tea extract and K12, continue stirring (rotating speed is 5000 turns/min) 6-10min, add Green tea essence, mix,.
By the mode of test example, beneficial effects of the present invention is described below:
The clinical trial of test example 1 toothpaste of the present invention
(1) sulfide analyzer analytic process
Use portable sulfide analyzer, directly read the ppb concentration value in subject oral cavity medium sulphide content, record implication value.
Method requires: before test, first instrument is adjusted 0, advises experimenter to remain silent 2min.Being connected with analyzer plastic suction pipe one end during test, the other end inserts 3cm in experimenter's mouth, it is impossible to contact with back, lip.Advise experimenter's nasal respiration, when peak value occurs in instrument, take out suction pipe, record peak value.Again measure after numerical value back to zero, repeat 3 times, take its meansigma methods.
(2) samples selection:
With VSCs more than 150ppb person for entry standard, and experimenter can not have respiratory system, digestive system, whole body system disease, suffer from extensive dental caries and periodontal disease, above for three days on end during experiment can not use non-hormone anti-inflammatory agent or antibiotic person.
(3) material:
Consumer uses embodiment 2,3,5 toothpaste and blank toothpaste respectively.A toothpaste is embodiment 2, B toothpaste be embodiment 3, C toothpaste be embodiment 5, D toothpaste is the blank sample without fresh breath, tooth protection composition.
(4) test operation:
At the trial, 160 people of inclusive criteria are randomly divided into 4 groups, often organize 40 people.Give the different toothpaste of each experimenter and toothbrush by group, and given some on the spot guidance by special messenger and brush teeth, brush 3min every time, after 1 hour, 12 hours, return to inspection place recheck.Hereafter, toothpaste and toothbrush are taken home the every day of each use sooner or later once by experimental subject, and each 3min can not use other oral health care products during this period or take anti-inflammatory drug, using 1 week and 2 Zhou Houzai recheck.Result is shown in table 2 below:
By the implication value of portable sulfide analyzer detection before and after experiment
| Toothpaste | Before experiment | After 1 hour | After 12 hours | After 1 week | After 2 weeks |
| No. A | 500.2±25.3 | 210.3±20.1 | 301.2±22.3 | 242±31.2 | 201±24.1 |
| No. B | 489.2±23.2 | 212.3±15.9 | 285.2±21.3 | 231.6±25.1 | 202.8±26.7 |
| No. C | 495.3±21.6 | 198.6±19.6 | 256.9±18.7 | 225.6±20.1 | 189.6±24.8 |
| No. D | 487.5±24.6 | 398.6±19.8 | 421.3±25.8 | 397.5±23.1 | 389.6±21.0 |
Interpretation of result: from upper table it can be seen that, after using toothpaste to brush teeth, the implication value often organized has certain decline, illustrates that using toothpaste to brush teeth can keep the pure and fresh of oral cavity to a certain extent, but uses the fresh breath contained by this experiment, tooth protection component dentifrice to brush teeth, can improve breath freshening degree.After brushing teeth 12 hours, use No. A, No. B, C toothpaste better than the fresh breath effects using control sample, illustrates to use effect containing fresh breath, tooth protection component dentifrice with the prolongation breath freshening time of this experiment；After brushing teeth 1 week, after 2 weeks, use No. A, No. B, C toothpaste there is good fresh breath effect, wherein, the effect of No. B (embodiment 3) and No. C (embodiment 5) is more excellent, and the effect of No. C (embodiment 5) is optimum.
Result of the test illustrates, toothpaste of the present invention can effectively maintain breath freshening, it is preferred that formula: green tea extract 0.1-0.2 part；Green tea essence 0.8-1.5 part；Abrasivus 30-40 part；Wetting agent 34.5-41.5 part；Thickening agent 1.2-1.85 part；Foaming agent 2.-4.05 part；Light blue 0.05-0.1 part；Light green 0.05-0.1 part；Saccharin sodium 0.2-0.35 part；Preservative 0.4-0.6 part；Brilliant white agent 0.3-0.5 part；Water 30-35 part；Most preferred formula is the formula of embodiment 3: green tea extract 0.2 part；Green tea essence 1.5 parts；Abrasivus 40 parts；Wetting agent 41.5 parts；Thickening agent 1.85 parts；Foaming agent 4.0 parts；Light blue 0.1 part；Light green 0.1 part；Saccharin sodium 0.35 part；Preservative 0.6 part；Brilliant white agent 0.5 part；35 parts of water.
Comparative example
Substituting green tea extract and Green tea essence in the embodiment of the present invention 2,3,5 with Pu'er tea and Pu'er tea essence, all the other adjuvants and consumption are all identical, prepare toothpaste, detect its effect according to the method for test example 1, and result is table 3 below such as:
By the implication value of portable sulfide analyzer detection before and after experiment
| Toothpaste | Before experiment | After 1 hour | After 12 hours | After 1 week | After 2 weeks |
| No. E | 501.3±25.4 | 254.3±20.3 | 332.2±23.3 | 273.2±27.3 | 237±25.7 |
| No. F | 490.2±22.2 | 261.3±16.9 | 315.2±23.3 | 265.6±25.5 | 236.8±26.7 |
| No. G | 496.3±21.7 | 250.8±19.3 | 296.9±19.7 | 265.6±23.1 | 229.6±25.9 |
| No. H | 49.2±24.2 | 399.2±18.9 | 423.3±24.8 | 399.5±25.5 | 398.6±21.6 |
Effectiveness comparison such as table 4 below by toothpaste of the present invention Yu the toothpaste of comparative example:
Implication value
| Toothpaste | Before experiment | After 1 hour | After 12 hours | After 1 week | After 2 weeks |
| No. A | 500.2±25.3 | 210.3±20.1* | 301.2±22.3* | 242±31.2* | 201±24.1* |
| No. B | 489.2±23.2 | 212.3±15.9* | 285.2±21.3* | 231.6±25.1* | 202.8±26.7* |
| No. C | 495.3±21.6 | 198.6±19.6* | 256.9±18.7* | 225.6±20.1* | 189.6±24.8* |
| No. D | 487.5±24.6 | 398.6±19.8 | 421.3±25.8 | 397.5±23.1 | 389.6±21.0 |
| No. E | 501.3±25.4 | 254.3±20.3 | 332.2±23.3 | 273.2±27.3 | 237±25.7 |
| No. F | 490.2±22.2 | 261.3±16.9 | 315.2±23.3 | 265.6±25.5 | 236.8±26.7 |
| No. G | 496.3±21.7 | 250.8±19.3 | 296.9±19.7 | 265.6±23.1 | 229.6±25.9 |
| No. H | 49.2±24.2 | 399.2±18.9 | 423.3±24.8 | 399.5±25.5 | 398.6±21.6 |
Note: No. A: compare with No. E, *: P < 0.05；
No. B: compare with No. F, *: P < 0.05；
No. C: compare with No. G, *: P < 0.05；
No. D: compare with No. H, *: P < 0.05.
Matched group (No. D with No. H) is compared and is not significantly different from, compared with contrast toothpaste (No. D, No. E, No. F), toothpaste of the present invention (No. A, No. B, No. C) is significantly higher than contrast toothpaste (P < 0.05) except the ability of implication stink substance, it is possible to more effectively maintain breath freshening.
Result of the test illustrates, the present invention adopts green tea extract and the specific adjuvant of the present invention, under specific proportioning the toothpaste of preparation can effectively maintain breath freshening, effect is significantly better than toothpaste prepared by Pu'er tea.
To sum up, the toothpaste that the present invention contains green tea extract has pre-anti-caries, goes effect of halitosis, has the effect of bactericidal antiphlogistic, it is possible to effectively maintaining breath freshening, application prospect is good.
Claims (10)
1. the toothpaste containing green tea extract, it is characterised in that: it includes the component of following weight proportion:
Green tea extract 0.05 part-0.2 part；Green tea essence 0.2 part-1.5 parts；Abrasivus 25 parts-40 parts；Wetting agent 29.5-41.5 part；Thickening agent 0.65-1.85 part；Foaming agent 1.5 parts-4.0 parts；Light blue 0.01 part-0.1 part；Light green 0.01 part-0.1 part；Saccharin sodium 0.05 part-0.35 part；Preservative 0.2 part-0.6 part；Brilliant white agent 0.1-0.5 part；Water 25-35 part.
2. toothpaste according to claim 1, it is characterised in that: it includes the component of following weight proportion:
Green tea extract 0.1-0.2 part；Green tea essence 0.8-1.5 part；Abrasivus 30-40 part；Wetting agent 34.5-41.5 part；Thickening agent 1.2-1.85 part；Foaming agent 2.-4.05 part；Light blue 0.05-0.1 part；Light green 0.05-0.1 part；Saccharin sodium 0.2-0.35 part；Preservative 0.4-0.6 part；Brilliant white agent 0.3-0.5 part；Water 30-35 part.
3. toothpaste according to claim 1, it is characterised in that: it includes the component of following weight proportion:
Green tea extract 0.2 part；Green tea essence 1.5 parts；Abrasivus 40 parts；Wetting agent 41.5 parts；Thickening agent 1.85 parts；Foaming agent 4.0 parts；Light blue 0.1 part；Light green 0.1 part；Saccharin sodium 0.35 part；Preservative 0.6 part；Brilliant white agent 0.5 part；35 parts of water.
4. the toothpaste according to claims 1 to 3 any one, it is characterised in that: described green tea extract is prepared as follows:
A, taking green tea, pulverize, add water mixing；
B, supersound extraction, the time of extraction is 15-30min, and the temperature of extraction is 55-70 DEG C, obtains lixiviating solution, is cooled to 15-25 DEG C in 30-50min；
C, filtration, obtain filtrate, centrifugal, removes supernatant, obtains the moisture green tea extract not higher than 45wt%.
5. toothpaste according to claim 4, it is characterised in that:
In step a, described pulverizing is that to be crushed to fineness be 45-75 order, described in the mixing that adds water be tea powder is minced with water according to parts by weight 1:(110-190 at 15-25 DEG C of temperature) ratio mix.
6. toothpaste according to claim 4, it is characterised in that: in step b, the power of supersound extraction is 1200w.
7. toothpaste according to claim 4, it is characterised in that: in step c, described filtration is filter pressing, and described centrifugal rotating speed is 5000-7500r/min, and the centrifugal time is 10-20min.
8. the toothpaste according to claims 1 to 3 any one, it is characterised in that:
Described wetting agent is sorbitol and PEG400, and the consumption of the two is 28-38 part and 1.5-3.5 part, and the consumption of the two is preferably 32-38 part and 2.5-3.5 part；
And/or, described abrasivus is hydrated silica；
And/or, described thickening agent is carboxymethyl cellulose, carrageenan 3189 and xanthan gum, the consumption of the two respectively 0.5-1.0 part, 0.05-0.35 part and 0.1-0.5 part；
And/or, described foaming agent is sodium lauryl sulphate；
And/or, described light blue is 1% light blue；
And/or, described light green be 1% light green；
And/or, described preservative is sodium benzoate；
And/or, described brilliant white agent is titanium dioxide.
9. the preparation method of toothpaste described in claim 1～8 any one, it is characterised in that: step is as follows:
(1) each component is weighed by proportioning described in claim 1～8 any one, soluble in water to saccharin sodium and preservative；
(2) wetting agent is added in Manufacturing medicine extract machine, then thickening agent, light green and light blue are added wherein, stir 6-10min；
(3) add the solution of above-mentioned steps (1), continue stirring and be completely dispersed to thickening agent, light green and light blue；
(4) add abrasivus and brilliant white agent, stir 10min under vacuo；
(5) add green tea extract, continue stirring 6-10min, add Green tea essence, mixing.
10. preparation method according to claim 9, it is characterised in that: in step (1), (4), (5), the rotating speed of stirring is 5000 turns/min.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106580836A (en) * | 2017-01-24 | 2017-04-26 | 广州薇美姿实业有限公司 | Oral care composition containing plant factor and application thereof |
| CN106726693A (en) * | 2017-01-20 | 2017-05-31 | 两面针（江苏）实业有限公司 | One kind refreshes the mind toothpaste and preparation method thereof |
| CN108078874A (en) * | 2018-02-09 | 2018-05-29 | 杭州纳美智康科技有限公司 | A kind of green tea toothpaste and its preparation process |
| CN111228171A (en) * | 2020-01-15 | 2020-06-05 | 拉芳家化股份有限公司 | Preparation method of toothpaste rich in tea amino acid |
| CN113057922A (en) * | 2021-04-08 | 2021-07-02 | 许耿防 | Toothpaste capable of efficiently removing tooth stains, whitening teeth, and refreshing breath and preparation method thereof |
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| CN102764207A (en) * | 2012-06-12 | 2012-11-07 | 云南云道茶业有限公司 | Pu'er tea toothpaste and preparation method thereof |
| WO2014056212A1 (en) * | 2012-10-13 | 2014-04-17 | Zhang Bin | Multi-action toothpaste |
| CN104398438A (en) * | 2014-12-08 | 2015-03-11 | 成都锦汇科技有限公司 | Toothpaste for preventing ozostomia |
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