CN104644542B - A kind of Value of natural bath & shower dew containing Sasanguasaponin - Google Patents
A kind of Value of natural bath & shower dew containing Sasanguasaponin Download PDFInfo
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- CN104644542B CN104644542B CN201510109997.9A CN201510109997A CN104644542B CN 104644542 B CN104644542 B CN 104644542B CN 201510109997 A CN201510109997 A CN 201510109997A CN 104644542 B CN104644542 B CN 104644542B
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Abstract
The invention discloses a kind of Value of natural bath & shower dew containing Sasanguasaponin and preparation method thereof, raw materials by weight portion meter:37 parts of Sasanguasaponin, 46 parts of Hederagenin, 0.5 1.5 parts of sapindoside, 35 parts of wild tea oil, 0.1 0.5 parts of glycyrrhizic acid, 0.5 1 parts of otoginsenoside, 0.5 1 parts of trifoliate orange Dulcis saponin(es, 0.1 0.5 parts of sponge gourd saponin(e, 25 parts of Baical Skullcap root P.E, 13 parts of garlic P.E, 13 parts of Bitter Melon P.E, 35 parts of dried tremella extract, 13 parts of starch, 0.1 0.5 parts of citric acid, 0.1 0.5 parts of sodium citrate, 0.1 0.5 parts of sodium chloride, 40 50 parts of deionized water.The shower cream of the present invention is made up of a variety of different vegetalitas saponin(es; there are good emulsifying capacity and dirt-removing power, stability and security are good, are a kind of natural plant shower gel; energy anti-inflammatory, antibacterial, antipruritic, moisturizing etc., play protection, regulation, improve the effect of skin.
Description
Technical field
The invention belongs to bath article field, and in particular to a kind of Value of natural bath & shower dew and its preparation side containing Sasanguasaponin
Method.
Background technology
Shower cream is daily daily chemical product, and its demand is increasing, and the shower cream species of in the market is various, but due to
Biochemical composition, the shower creams such as the preservative of surfactant and other tool carcinogenicity of most of shower cream all containing synthesis make
It is single with making skin excessively dry, acting on, the effect of washing is largely limited to, necessarily negative is produced to the health of people
Influence and threaten, therefore the importance of the shower cream of safety, multi-functionization is just welcome and paid attention to by people, and present invention exploitation
Shower cream except normal decontamination, sebum etc. act on, moreover it is possible to anti-inflammatory, antibacterial, moisturizing, moisturizing etc., play protection, regulation,
The effect of improving skin etc..
The content of the invention
It is an object of the invention to provide it is a kind of containing Sasanguasaponin Value of natural bath & shower dew and preparation method thereof, the shower cream by
A variety of different vegetalitas saponin(e compositions, have good emulsifying capacity and dirt-removing power, stability and security are good, natural for one kind
Plant body wash, energy anti-inflammatory, antibacterial, antipruritic, moisturizing etc., play protection, regulation, improve the effect of skin.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of Value of natural bath & shower dew containing Sasanguasaponin, raw materials by weight portion meter:Sasanguasaponin 3-7 parts, Hederagenin
4-6 parts, sapindoside 0.5-1.5 parts, wild tea oil 3-5 parts, glycyrrhizic acid 0.1-0.5 parts, otoginsenoside 0.5-1 parts, trifoliate orange Dulcis soaps
Glycosides 0.5-1 parts, sponge gourd saponin(e 0.1-0.5 parts, Baical Skullcap root P.E 2-5 parts, garlic P.E 1-3 parts, Bitter Melon P.E 1-3 parts,
Dried tremella extract 3-5 parts, starch 1-3 parts, citric acid 0.1-0.5 parts, sodium citrate 0.1-0.5 parts, sodium chloride 0.1-0.5 parts,
Deionized water 40-50 parts.
The preparation method of described Sasanguasaponin is:10g is dried and extracted after Oil-tea-cake crushes with 50wt.% ethanol solutions
5h, solid-liquid ratio 1:6,55 DEG C of temperature;Filtering, rotary evaporation concentration.The preparation method of described Hederagenin is:10g is taken to do
The ivy leaf of dry crushing, is extracted with 75wt.% ethanol solutions, solid-liquid ratio 1:10,60 DEG C of extraction 2.5h, are filtered, rotation
Turn to be concentrated by evaporation.The preparation method of described sapindoside is:The soapberry kind skin of 10g drying and crushings is taken, with 50wt.% second
Alcoholic solution is extracted, solid-liquid ratio 1:10,60 DEG C of extraction 3h, filtering, rotary evaporation concentration.The preparation side of described glycyrrhizic acid
Method is:The haulm of liquorice that 10g is dried is extracted after crushing with 35wt.% ethanol solutions, solid-liquid ratio 1:10,48 DEG C of extractions
4h, filtering, rotary evaporation concentration.The preparation method of described otoginsenoside is:Take 10g to dry buckeye dry seed, carry out
Crush, extracted with 55wt.% ethanol solutions, solid-liquid ratio 1:10,45 DEG C of extraction 4h, filtering, rotary evaporation concentration.It is described
The preparation methods of trifoliate orange Dulcis saponin(es be:The foetid vibrunum leaf and fruit leaf for taking 10g to dry, is crushed, is carried out with 55wt.% ethanol solutions
Extraction, solid-liquid ratio 1:5,45 DEG C of extraction 4h, filtering, rotary evaporation concentration.The preparation method of described sponge gourd saponin(e is:Take
10g dries sponge gourd cauline leaf, is crushed, is extracted with 60wt.% methanol solutions, solid-liquid ratio 1:5,80 DEG C of extraction 4h, mistake
Filter, rotary evaporation concentration.
The preparation method of described Baical Skullcap root P.E is:Dry radix scutellariae is crushed, ultrasonic extraction, solid-liquid ratio 1:
10, temperature 60 C, time 1.5h, filtering, rotary evaporation concentration;The preparation method of described Bitter Melon P.E is:Squeeze the juice, mistake
Filter, rotary evaporation concentration;The preparation method of described garlic P.E is to take uncooked garlic to squeeze the juice, and the water to double is soaked
One week, filtering;The preparation method of described dried tremella extract is:Dry white fungus is crushed, with 1:5 solid-liquid ratio is in 80 DEG C of bars
3h is extracted under part, is filtered, rotary evaporation concentration.
Preparation method:Deionized water is heated to 60 DEG C, adds Sasanguasaponin, Hederagenin, sapindoside, wild tea
Oil, glycyrrhizic acid, otoginsenoside, trifoliate orange Dulcis saponin(es, sponge gourd saponin(e, Baical Skullcap root P.E, garlic P.E, Bitter Melon P.E and white fungus carry
Take thing, for temperature control at 60 DEG C ~ 65 DEG C, stirring 30min is allowed to well mixed, is cooled to 40 DEG C, adds starch in adding procedure
And sodium citrate, with lemon acid for adjusting pH, it is eventually adding sodium chloride regulation viscosity.
The remarkable advantage of the present invention is:In natural plant shower gel composition of the present invention:Wild tea oil has height to contain
The unrighted acid of amount, the sebum close to skin, using skin can be allowed more to lubricate in shower cream, while wild tea oil for
Other plant composition also has the rush effect of oozing, and skin is more lubricated soft exquisiteness;Sasanguasaponin is pentacyclic triterpene saponins, is a kind of
The effects such as good nonionic surfactant, HLB value 16, emulsifiable, foaming, scattered, decontamination, have bactericidal action, to mould
Inhibition is best, and use can be antipruritic with delaying skin keratinization in shower cream;Sponge gourd saponin(e in sponge gourd cauline leaf has heat-clearing
Cool blood, active, promotion cell propagation, the effect such as cytoactive, a wider spectrum antibiotic property is improved, conditioning skin can be played in shower cream
Skin, reduce cuticula peeling, anti-inflammatory, protection skin and other effects;Glycyrrhizic acid in radix glycyrrhizae has stronger anti-inflammatory, antibacterial effect, can relax
Solution and regulation skin(Brighten, be antipruritic etc.), protection skin effect well is played in shower cream, is had in acid condition certain
Surface-active, can leniently remove sebum;Sapindoside in soapberry has good surface-active, can go well
Except the sebum of smegma, there is antibiotic property, especially dermatophyte to have stronger killing action, can consumingly suppress tyrosine
Enzyme, elastoser, hyaluronidase activity, played in shower cream brighten well, anti-aging effects;It is normal in ivy
Spring rattan saponin(e can also suppress tyrosinase, elastoser, hyaluronidase activity, can improve skin surface situation, soft and smooth
Skin, anti-inflammatory anti-itch and water retention, in shower cream using can make skin lubrication, alleviate dry skin;Seven in buckeye
Leaf saponin has moisture absorption and moisture-keeping function, can brighten skin lightening, anti-dermatitis, Reduce allergy, using except having very well in shower cream
Decontamination can also protect skin well;Trifoliate orange Dulcis saponin(es in foetid vibrunum leaf and fruit tree have certain emulsifying capacity, there is moisturizing work
With, the metabolism of cell can be promoted, in shower cream using can increase foaming characteristic, avoid skin excessively dry angling, play
Skin-active acts on;Radix scutellariae mainly contains scutelloside, neobaicalein, sitosterol, benzoic acid more composition, in shower cream use can rise
Reach skin care to antibacterial, anti-inflammatory, the anaphylaxis etc. that mitigates skin, while corrosion-resistant effect can be also played to shower cream;Balsam pear energy
Suppress tyrosinase activity well, suppress the formation of melanin so as to playing skin care effect;Use of the garlic in shower cream
Dermatophyte can be reduced, reaches the effect of itching-relieve skin-care, while can also reduce the main component triglyceride of smegma,
Dirt is adsorbed so as to reduce the excessive sebum of smegma, skin is kept cleaning;Starch is good natural glue, energy
Adjust the mobility of shower cream;Sodium citrate has good complexation of metal ions ability, good thickening power;Citric acid can
With buffer pH, moisturizing can also be played a part of.The reasonable combination of various natural components, there are good washing, moisturizing, skin care
Effect, can not only solve single effect of the bathing of common shower cream, and improve the security used.
Embodiment
Embodiment 1
1st, count in parts by weight:5 parts of Sasanguasaponin, 5 parts of Hederagenin, 3 parts of dried tremella extract, sapindoside 0.5
Part, 3 parts of wild tea oil, 0.1 part of glycyrrhizic acid, 0.5 part of otoginsenoside, 0.5 part of trifoliate orange Dulcis saponin(es, 0.1 part of sponge gourd saponin(e, garlic P.E
2 parts, 2 parts of Bitter Melon P.E, 2 parts of starch, 3 parts of Baical Skullcap root P.E, 0.5 part of citric acid, 0.5 part of sodium citrate, sodium chloride 0.1-
Part, deionized water 40-50 parts.
2nd, deionized water is heated to 60 DEG C and adds radix scutellariae, balsam pear, garlic, dried tremella extract and different saponin(es, during
Temperature control stirs evenly 30min at 60 DEG C ~ 65 DEG C, and temperature drops to 40 DEG C, adds starch, sodium citrate, is adjusted with citric acid
PH, it is eventually adding sodium chloride and adjusts viscosity again.
Embodiment 2
1st, count in parts by weight:Wild 5 parts of tea oil, 5 parts of Sasanguasaponin, 5 parts of Hederagenin, 3 parts of dried tremella extract, without trouble
Sub- 0.5 part of saponin(e, 0.1 part of glycyrrhizic acid, 0.5 part of otoginsenoside, 0.5 part of trifoliate orange Dulcis saponin(es, 0.1 part of sponge gourd saponin(e, garlic P.E 2
Part, 2 parts of Bitter Melon P.E, 2 parts of starch, 3 parts of Baical Skullcap root P.E, 0.5 part of citric acid, 0.5 part of sodium citrate, sodium chloride 0.1-
Part, deionized water 40-50 parts.
2nd, deionized water is heated to 60 DEG C and adds radix scutellariae, balsam pear, garlic, dried tremella extract and different saponin(es, during
Temperature control stirs evenly 30min at 60 DEG C ~ 65 DEG C, and temperature drops to 40 DEG C, first adds wild tea oil, adds starch, sodium citrate,
With lemon acid for adjusting pH, it is eventually adding sodium chloride and adjusts viscosity again.
Properties of product
1st, stability
It is each under the conditions of two kinds of shower creams are placed into subzero 3 DEG C, 40 DEG C to place 24h, as a result do not occur being layered, precipitate, tie
The changes such as brilliant or change color, embodying shower cream has good stability.
2nd, spumescence
It is measured using Roche foam meter, and is compareed with daily snow shower cream difficult to understand, as a result such as table 1, is as a result represented
This product is with higher foaming capacity and its foam with higher stability.
The shower cream foamability of table 1 and Stability Determination result
3rd, sterilization, fungistatic effect
Assay method, it after 10 times of two kinds of Value of natural bath & shower dew dilution is that disinfectant acts on mould, Epidermophvton that experimental group, which is,
The experiment bacterium solution of tinea bacterium, sample and pour into inoculation with agar, control group makes same after then diluting 10 times of Austria's snow shower cream
Operation, and 48h is cultivated under the conditions of 37 DEG C together, and observe result.As a result such as table 2, the results showed that, Value of natural bath & shower of the invention
Dew has suppression and bactericidal effect well, illustrates that shower cream can well be killed with suppressing dermatophyte and play protection skin
Effect, particularly played an important role using several natural plants saponin(es, radix scutellariae, balsam pear, garlic as main active component.
The bactericidal effect of the shower cream of table 2
4th, wetting, soothing effect
2 three kinds of Austria's snow shower cream, embodiment 1, embodiment shower creams are a set of total 100 sets and subsidiary shower cream wetting
Soothing effect questionnaire, the citizen of all ages and classes sex are issued, survey are withdrawn after 3 months, and statistical analysis is carried out to questionnaire,
As a result such as table 3, show from using interpretation of result, embodiment 1, embodiment 2 do not only have preferable dirt-removing power, in wetting and moisturizing
Significant effect in aspect, will not be as the coarse drying of control group using rear skin, but also it is right to show very lubrication softness, embodiment 1
Become apparent from Oily, embodiment 2 it is most obvious for Dry effect.
The shower cream of table 3 soaks soothing effect
5th, moistening effect
Moistening effect after being washed with moisture of skin external test instrument measure wrist inwall with different shower creams, specific method
For:Take Austria's snow, two kinds of case study on implementation 0.5mL to smear the wrist inwall of wetting in Beijing respectively, cleaned up after 5min with clear water, will
Moisture measure groove is placed on the wrist inwall after shower cream is washed, and determines the phase evaporated in 10min with the vapor of blank control
Change to speed, is represented with TWL, is as a result shown, the relative velocity of two kinds of shower creams of embodiment 1,2 is lower than Austria's snow respectively
56%th, 68%, illustrate that two kinds of shower creams are all higher than the shower cream moisture-retaining capacity of in the market, embodiment 2 is imitated containing wild tea oil moisturizing
Fruit is also good compared with embodiment 1.
6th, to the inhibition of tyrosinase activity
First take Austria's snow, the shower cream 1mL of two embodiments stand-by after diluting ten times, take 1mL shower creams respectively into test tube,
Tyrosinase solution 0.5mL and phosphate buffer 0.9mL is added, at 25 degrees c, moisturizing 10min, then in the case of 25 DEG C of moisturizings
Matrix solution 1mL is added, reacts 5min, absorbance is surveyed in 475nm, another is equally handled with the enzyme of inactivation, and
475nm survey absorbance, and without testing liquid in the case of determine absorbance, calculate the inhibiting rate of tyrosinase, measurement result
The inhibiting rate of display snow difficult to understand is 12%, and embodiment 1 is 81%, and embodiment 2 is 74%, i.e., shower cream of the invention is to tyrosinase
Activity have higher inhibiting rate, show there is good skin effect.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, it should all belong to the covering scope of the present invention.
Claims (2)
- A kind of 1. Value of natural bath & shower dew containing Sasanguasaponin, it is characterised in that:Raw materials by weight portion meter:Sasanguasaponin 3-7 parts, Hederagenin 4-6 parts, sapindoside 0.5-1.5 parts, wild tea oil 3-5 parts, glycyrrhizic acid 0.1-0.5 parts, otoginsenoside 0.5-1 parts, trifoliate orange Dulcis saponin(e 0.5-1 parts, sponge gourd saponin(e 0.1-0.5 parts, Baical Skullcap root P.E 2-5 parts, garlic P.E 1-3 Part, Bitter Melon P.E 1-3 parts, dried tremella extract 3-5 parts, starch 1-3 parts, citric acid 0.1-0.5 parts, sodium citrate 0.1- 0.5 part, sodium chloride 0.1-0.5 parts, deionized water 40-50 parts;The preparation method of described Sasanguasaponin is:10g is dried and extracts 5h with 50wt.% ethanol solutions after Oil-tea-cake crushes, Solid-liquid ratio 1:6,55 DEG C of temperature;Filtering, rotary evaporation concentration;The preparation method of described Hederagenin is:The ivy leaf of 10g drying and crushings is taken, with 75wt.% ethanol solutions Extracted, solid-liquid ratio 1:10,60 DEG C of extraction 2.5h, filtering, rotary evaporation concentration;The preparation method of described sapindoside is:The soapberry kind skin of 10g drying and crushings is taken, with 50wt.% ethanol solutions Extracted, solid-liquid ratio 1:10,60 DEG C of extraction 3h, filtering, rotary evaporation concentration;The preparation method of described glycyrrhizic acid is:The haulm of liquorice that 10g is dried is carried out after crushing with 35wt.% ethanol solutions Extraction, solid-liquid ratio 1:10,48 DEG C of extraction 4h, filtering, rotary evaporation concentration;The preparation method of described otoginsenoside is:Take 10g to dry buckeye dry seed, crushed, with 55wt.% second Alcoholic solution is extracted, solid-liquid ratio 1:10,45 DEG C of extraction 4h, filtering, rotary evaporation concentration;The preparation method of described trifoliate orange Dulcis saponin(es is:The foetid vibrunum leaf and fruit leaf for taking 10g to dry, is crushed, with 55wt.% second Alcoholic solution is extracted, solid-liquid ratio 1:5,45 DEG C of extraction 4h, filtering, rotary evaporation concentration;The preparation method of described sponge gourd saponin(e is:Take 10g to dry sponge gourd cauline leaf, crushed, with 60wt.% methanol solutions Extracted, solid-liquid ratio 1:5,80 DEG C of extraction 4h, filtering, rotary evaporation concentration;The preparation method of described Baical Skullcap root P.E is:Dry radix scutellariae is crushed, ultrasonic extraction, solid-liquid ratio 1:10, Temperature 60 C, time 1.5h, filtering, rotary evaporation concentration;The preparation method of described Bitter Melon P.E is:Squeeze the juice, filter, Rotary evaporation concentrates;The preparation method of described garlic P.E is to take uncooked garlic to squeeze the juice, and the water to double carries out immersion one Week, filtering;The preparation method of described dried tremella extract is:Dry white fungus is crushed, with 1:5 solid-liquid ratio is in 80 DEG C of bars 3h is extracted under part, is filtered, rotary evaporation concentration.
- A kind of 2. method of the dew of the Value of natural bath & shower containing Sasanguasaponin prepared as described in claim 1, it is characterised in that:Go from Sub- water is heated to 60 DEG C, adds Sasanguasaponin, Hederagenin, sapindoside, wild tea oil, glycyrrhizic acid, otoginsenoside, trifoliate orange Dulcis Saponin(e, sponge gourd saponin(e, Baical Skullcap root P.E, garlic P.E, Bitter Melon P.E and dried tremella extract, temperature control in adding procedure At 60 DEG C ~ 65 DEG C, stirring 30min is allowed to well mixed, is cooled to 40 DEG C, adds starch and sodium citrate, is adjusted with citric acid PH is saved, is eventually adding sodium chloride regulation viscosity.
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CN105640827A (en) * | 2016-01-05 | 2016-06-08 | 南京科技职业学院 | Method for preparing shampoo by adopting simple physical means |
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CN108451836B (en) * | 2018-06-27 | 2020-01-10 | 广州市科能化妆品科研有限公司 | Shower gel composition and preparation method thereof |
CN108771650A (en) * | 2018-08-07 | 2018-11-09 | 夏战利 | A kind of plant body wash |
CN113081898A (en) * | 2021-04-19 | 2021-07-09 | 武汉允心创造生物科技有限公司 | Moisturizing refreshing shower gel and preparation method thereof |
CN115501130A (en) * | 2022-09-14 | 2022-12-23 | 湖南省林业科学院 | Method for killing mites by using sasanquasaponin |
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