CN104547344A - Aloe care lotion and preparation method thereof - Google Patents
Aloe care lotion and preparation method thereof Download PDFInfo
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- CN104547344A CN104547344A CN201510032712.6A CN201510032712A CN104547344A CN 104547344 A CN104547344 A CN 104547344A CN 201510032712 A CN201510032712 A CN 201510032712A CN 104547344 A CN104547344 A CN 104547344A
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Abstract
The invention discloses aloe care lotion, which contains aloe nanosuspension liquid stock, a saussurea involucrata extract, a chamomile extract, sodium hyaluronate and a polymeric material. The preparation method comprises the following steps: putting aloe leaves into a homogenizer, and crushing and micronizing processed material particles through high-frequency strong ultrasonic cavitation action to form 1-700nm nanoparticles to obtain the aloe nanosuspension liquid stock; and stirring and mixing the obtained aloe nanosuspension liquid stock, the saussurea involucrata extract, the chamomile extract, thesodium hyaluronate, the polymeric material and a matrix to obtain the required aloe care lotion. The aloe care lotion has a unique biological slow-release function, is capable of effectively repairing and protecting vagina and wall cervix, comprehensively nourishing, and removing vaginal dryness, sufferings and discomfort caused by various reasons, has a significant inhibition function on a plurality of pathogenes capable of causing bacterial, mycotic, trichomonas, senile and mixed infection vaginitis, cervical erosion and kinds of sexually transmitted diseases, and is capable of effectively removing inflammation and preventing cross infection. The aloe care lotion is free of thrill, free of toxins or harm and free of side effects after being used.
Description
[technical field]
The present invention relates to a kind of Aloe nursing lotion and preparation method thereof.
[background technology]
Aloe is a kind of perennial meat section herbaceous plant, just has the laudatory title of " first aid plant ", " noiseless doctor ", " ten thousand answer good medicine ", " rare treasures " since ancient times, has magical function in medicine, health care, beauty treatment etc.Larger progress has been had in recent years to the pharmacological research of Aloe, the functions such as the medical treatment of Aloe, health care, beauty treatment are absolutely proved, think that Aloe has the effect such as anti-inflammation, treatment acne, acne, whitening and speckle dispelling, also special curative effect is had to constipation and hemorrhoid, the fresh juice of normal directly use Aloe among the people, but easily cause allergic reaction.Have multiple external and aloe products for oral administration at present, but particularly dissolution rate that is water-insoluble and slightly solubility solid material is not high due to the active ingredient of Aloe, and have impact on its result of use yet.
At present, the gynaecologic vaginal nursing health products on market is numerous.But mostly only focus on Disinfection Effect, and it is shorter to execute the effect time.
[summary of the invention]
The present invention provides a kind of Aloe nursing lotion and preparation method thereof for the problems referred to above exactly, and gained Aloe nursing lotion has antibacterial, nursing, lubrication, and has slow-release function and to make to execute the effect time longer.
In order to solve above technical problem, the concrete technical scheme of the present invention is as follows:
A kind of Aloe nursing lotion, comprise the Aloe nano suspending liquid natural juice of 30-90%, the hyaluronate sodium of 0.05-5%, the camomile extract of 0.05-2%, the polymeric material of 0.1-10%, the substrate of 0.80-53%, above percent is percetage by weight; Polymeric material used is carrageenan, arabic gum, alginate, starch, dextrin, Cera Flava, agar, chitosan; Substrate is sodium bicarbonate, sodium carbonate, sodium hydroxide, triethanolamine or carbamide, ethanol, isopropyl alcohol, glycerol or propylene glycol, ammonium lauryl sulfate, AESA and refining ostrich oil.
Preferably, also containing the antioxidant of 0.05-2% and the antiseptic of 0.05-0.5%.
Preferably, the Margarita powder micropowder below the vitamin E of the vitamin A or derivatives thereof containing 0.01-0.2%, the vitamin C or derivatives thereof of 0.01-0.2%, 0.01-0.5%, 100 orders of 0.01-1%, the Herba melissae axillaris powder of 0.01-1%, the propolis of 0.01-2% and the ultrafine zinc oxide particle of 0.01-1%.
Preferably, the surfactant also containing 0.01-10%.
Preferably, comprise the Aloe nano suspending liquid natural juice of 50%, the hyaluronate sodium of 2%, camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 7% of 1%, the ethanol of 26.5%, the ammonium lauryl sulfate of 3%, the AESA of 3%, refining ostrich oil, 2% surfactant of 1.2%.
Preferably, also containing the potassium sorbate of 0.5-1.5% and the carbomer of 0.6-0.8%.
Preferably, the Herba Saussureae Involueratae extract also containing 1-2%.
Preferably, comprise the Aloe nano suspending liquid natural juice of 55%, the hyaluronate sodium of 3%, camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 6% of 1.4%, the ethanol of 17.5%, the ammonium lauryl sulfate of 3%, 3% AESA, 1.2% refining ostrich oil, 3% surfactant, the Herba Saussureae Involueratae extract of 1%, the potassium sorbate of 1% and 0.6% carbomer.
The preparation method of above-mentioned Aloe nursing lotion, it is characterized in that: choose 3 years thick Aloe prophylls of leave, non-woven fabrics is pasted in incision after cutting, and be built in less than 4 DEG C temperature cold preservations in 2 hours for subsequent use, during use, will through cleaning, Folium Aloe after disinfecting or the inside gelling after removing leaf skin, add 0.05% native cellulose E, under lOOOrpm-lOOOOrpm rotating speed, 5min-30min is processed through refiner or homogenizer, then by high frequency intense ultrasonic wave field cavitation, machined object granule is pulverized in high pressure homogenisers, ultramicronising, under lOMpa-300Mpa high pressure, produce the moment effluxvelocity of 200m/s-600m/s, make material particles produce cavitation and make its cracking, promote the increase of amorphous particle ratio in suspension or become amorphous particle completely, form the nanoparticle of lnm-700nm size, obtain Aloe nano suspending liquid: by gained Aloe nano suspending liquid, camomile extract, Herba Saussureae Involueratae extract and hyaluronate sodium, polymeric material and substrate stir 5min-20min with 200rpm-5000rpm rotating speed at 20 DEG C-80 DEG C, obtain required Aloe nursing lotion.
The present invention by nano aloe and high efficiency nutritious Moisture factor hyaluronate sodium composite, by liposome enclose and nanometer emulsified, there is unique biological slow-released function, the active ingredient of nano aloe is retained for a long time in intravaginal, it is longer that slow releasing in 24 hours and making executes the effect time, in addition, Aloe not only makes the solid material dissolution rate of its active ingredient particularly water-insoluble and slightly solubility increase after nanorize, the miscible effect of volatilization wet goods composition and water improves, stability strengthens, specific surface area increases, viscosity changes, adhesion strength increases, absorbability improves, make script only partly discharge the composition that maybe cannot discharge and be able to sufficient release, and more easily infiltrate in thalline and significantly improve antibacterial effect, bacillary to causing, mycotic, trichomonas, senile, and mixed infective vaginitis, but the multiple pathogens of cervical erosion and various sexually transmitted disease (STD) has and kills function significantly, can effectively diminish inflammation, guard against cross infection.Camomile extract is one of the gentleest quintessence oil, containing angelic acid, isopropylformic acid., the positive composition such as butyl ester, isoamyl alcohol, the sterilization of tool strengthening antiinflammatory, infection, antivirus action, and its character is gentle, after mixing with nano aloe natural juice, compatibility performance is good, can eliminate the myalgia that headache, migraine or fever flu cause; And energy aging resistance, moist skin, millet paste also can be used as the nourishing agent of hair.Drink Flos Matricariae chamomillae tea and have sedation, allow people become gentle genial.In addition, for sleep, stabilizing the emotions is also helpful, and have and suppress inflammation, healing of wound, it has the effect of sterilizing, maintenance laceration of skin; Be used in maintenance, moisturizing can be had, the calm skin restrain pore of releiving; Add that there is refrigerant, to help skin tissue regeneration effect, and Aloe nano suspending liquid natural juice is used in combination, can extend the service time of the active ingredient of nano aloe, has good antibacterial effect.
The trophic factors such as natural aloe extract acemannan, hyaluronate sodium and angelic acid that the present invention is rich in, effectively can repair and protect vagina and wall of cervix, and the vaginal dryness that nourishing comprehensively, elimination a variety of causes cause, pruritus are uncomfortable.Use rear nothing to irritate, nontoxic, harmless, without any side effects.The present invention expands the medicine resource of Chinese medicine Aloe and Flos Matricariae chamomillae, improves the biological effect of Aloe and Flos Matricariae chamomillae, reduces cost of material; Its preparation technology is suitable for suitability for industrialized production, yield is high, quality good, production efficiency is high.
[detailed description of the invention]
Below in conjunction with detailed description of the invention, the present invention is further detailed explanation.
In order to those skilled in the art can understand technical scheme provided by the present invention better, set forth below in conjunction with specific embodiment.
embodiment 1:
Nano aloe nursing lotion, Aloe nano suspending liquid natural juice containing 30%, 1% be Flos Matricariae chamomillae, 2% hyaluronate sodium, the polymeric material chitosan of 2% (gelatin of 2%, the starch of 7%) of 11%, substrate (sodium bicarbonate of 0.3%, the ethanol of 46.5%, the ammonium lauryl sulfate of 3%, the AESA of 3%, the refining ostrich oil > of 1.2% of 54%.
embodiment
2
:
Nano aloe nursing lotion, Aloe nano suspending liquid natural juice containing 50%, the hyaluronate sodium of 2%, 1% camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 7%, the ethanol of 26.5%, the ammonium lauryl sulfate of 3%, the AESA of 3%, refining ostrich oil, 2% surfactant of 1.2%.
embodiment 3:
Nano aloe nursing lotion, containing the Aloe nano suspending liquid natural juice of 90%, the camomile extract of 0.5%, 1% sodium pyrosulfite, 0.5% Nipagin ester, Dowicol2000, EDTA, one or more in KathonCG or other composition, 0.05% vitamin A (or derivatives thereof), 0.5% vitamin E (or derivatives thereof), 0.5% Herba melissae axillaris powder, the hyaluronate sodium of 0.5%, the polymeric material of 0.45%, substrate (the triethanolamine of 0.5% of 6%, the isopropyl alcohol of 5%, the ammonium lauryl sulfate of 0.1%, the AESA of 0.3%, the refining ostrich oil of 0.1%).
embodiment 4:
Nano aloe nursing lotion, containing the Aloe nano suspending liquid natural juice of 85%, the camomile extract of 2%, 1% sodium pyrosulfite, 0.5% Nipagin ester, Dowicol2000, EDTA, one or more in KathonCG or other composition, 0.05% vitamin A (or derivatives thereof), 0.5% vitamin E (or derivatives thereof), 0.5% Herba melissae axillaris powder, the hyaluronate sodium of 1%, the polymeric material of 0.45%, substrate (the triethanolamine of 0.5% of 7%, the isopropyl alcohol of 3%, the ammonium lauryl sulfate of 0.1%, the AESA of 0.3%, the refining ostrich oil of 0.1%), the potassium sorbate of 1.2% and 0.8% carbomer.
embodiment 5:
Nano aloe nursing lotion, Aloe nano suspending liquid natural juice containing 50%, the hyaluronate sodium of 2%, 1% camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 7%, the ethanol of 26.5%, the ammonium lauryl sulfate of 3%, the AESA of 3%, refining ostrich oil, 2% surfactant of 1.2%.
embodiment 6:
Nano aloe nursing lotion, Aloe nano suspending liquid natural juice containing 55%, the hyaluronate sodium of 3%, 1.4% camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 6%, the ethanol of 17.5%, the ammonium lauryl sulfate of 3%, 3% AESA, 1.2% refining ostrich oil, 3% surfactant, the Herba Saussureae Involueratae extract of 1%, the potassium sorbate of 1% and 0.6% carbomer.
embodiment 7:
Will be clean (through cleaning, routine disinfection) Folium Aloe or inside gelling refiner after removing leaf skin or homogenizer (rotating speed is 1000-lOOOOrpm) carry out process 5-30min, again by high pressure homogenisers high frequency intense ultrasonic wave field cavitation, machined object granule is pulverized, ultramicronising, under 10-300Mpa high pressure, produce moment effluxvelocity 200-600m/s speed, make material particles produce cavitation and make its cracking, promote the increase of amorphous particle ratio in suspension or become amorphous particle completely, form the nanoparticle of 1-700nm size, obtain Aloe nano suspending liquid, get Aloe nano suspending liquid, Herba Saussureae Involueratae extract, camomile extract, hyaluronate sodium, polymeric material and substrate (also can add pigment, essence as required, supply deionized water), at 20-80 DEG C, stir 5-20min with 200-5000rpm rotating speed, obtain required product.Product relative viscosity 3000-30000 centipoise, transparent, 60 DEG C 24 hours or 4 DEG C 24 hours not stratified, haze-free, product antibacterial effect is excellent.
embodiment 8:
Adopt more than 3 years leaf age Aloes as results object, paddle cutout is sentenced non-woven fabrics and is pasted, and pluck in hands and within latter two hours, be built in less than 4 DEG C and be in store for, during processing, removal foul and damaged part are after clean water, be soaked into and within 30 minutes-24 hours, process containing soaking disinfection in the disinfectant solution such as 50-500mg/L effective chlorine, available iodine or hydrogen peroxide, the inside gelling after adopting aloe full leaf or removing leaf skin.Be processed into the block of less than 2 centimetres sizes with cutting knife, then carried out process 5-30min with refiner or homogenizer.Add oxidant as natural Vitamin E, carotenoid, grape polyphenols, prevent oxidation deterioration, and/or add antiseptic as Nipagin ester, hydroxy methocel, Dowicol 2000, EDTA, one or more in KathonCG or other composition, prevent putrid and deteriorated: add vitamin A or derivatives thereof, vitamin C or derivatives thereof, vitamin E, Margarita powder micropowder, Herba melissae axillaris powder, propolis, ultrafine zinc oxide particle and/or surfactant, then by high frequency intense ultrasonic wave field cavitation, machined object granule is pulverized in high pressure homogenisers, ultramicronising, under lOMpa-300Mpa high pressure, produce the moment effluxvelocity of 200m/s-600m/s, make material particles produce cavitation and make its cracking, promote the increase of amorphous particle ratio in suspension or become amorphous particle completely, form the nanoparticle of 1nm-700nm size, obtain Aloe nano suspending liquid, gained composite aloe nano suspending liquid and camomile extract, hyaluronate sodium, polymeric material and substrate are stirred 5min-20min with 200rpm-5000rpm rotating speed at 20 DEG C-80 DEG C, obtains the nursing of required nano aloe.
Be below antibacterial experiment data and vaginal mucosa stimulation test, eye stimulation test, the chmice acute Oral toxicity result of the test of gained nano aloe nursing lotion of the present invention.
Antibacterial experiment data:
Antimicrobial spectrum and antibacterial effect
| Test bacterium | MIC before process | MIC after process |
| Dysentery bacterium | 8 | 25 |
| Corynebacterium acnes | 7 | 24 |
| Staphylococcus aureus | 17 | 51 |
| Bacillus pyocyaneus | 7 | 15 |
| Hemolytic streptococcus | 5 | 15 |
| Gardnerella | 10 | 40 |
| Aerogenesis klebsiella | 6 | 35 |
| Alcaligenes faecalis | 6 | 30 |
| Cloaca | 6 | 25 |
| Aspergillus niger | 5 | 8 |
| Aspergillus fumigatus | 5 | 10 |
| Albicans | 6 | 13 |
| The anti-addiction bacterium of cotton-shaped table | 6 | 11 |
| Beard and hair addiction bacterium | 6 | 15 |
| Chlamydia trachomatis | 5 | 15 |
Shang Tu MIC unit is mm, and negative control group bacterial restrain is 5mm.
Vaginal mucosa stimulation test:
By the 3.5th carrying out in " disinfection technology standard " (third edition) first fascicle " experimental technique specification " (Ministry of Public Health, 2012.4).
Choose healthy White Rabbit 12, be divided into contamination group, vehicle group and blank group, every treated animal 4.Contamination group: roundlet cotton sliver long for the 2.0cm scribbling test specimen urine of the present invention is inserted experimental animal intravaginal; Vehicle group: with the leaching of onesize cotton sliver with sterile saline, insert animal intravaginal.Remove tested material after 4 hours, after 24 hours, put to death animal, take out topical vaginal tissue, observe with or without phenomenons such as hyperemia, edema.Result shows, in the observation period, test group, vehicle group, blank treated animal topical vaginal are organized and all do not occurred erythema or edematous condition, and irritating reaction integral mean value is 0.Judge according to relevant criterion in " disinfection technology standard " (third edition) first fascicle " experimental technique specification " (Ministry of Public Health, 2012.4), the present invention is to rabbit vagina mucosa nonirritant.
Eye irritant test:
By the 3.4th carrying out in " disinfection technology standard " (third edition) first fascicle " experimental technique specification " (Ministry of Public Health, 2012.4).
Choose healthy White Rabbit 4, by eye conjunctival sac on the left of test specimen stock solution 1-2 instillation White Rabbit of the present invention, make eye immediately passive closed 4 seconds, then use normal saline flushing 5 minutes.Right eye compares, instillation normal saline, after eye drip 6,24,48 hours, 4 days with 7 days, observe the damage of rabbit conjunctival, iris and cornea and recovery situation.Result shows, after awarding medicine, test group animal eye conjunctiva iris and cornea all do not show and irritate symptom, and stimulation index integration peak is 0.According to " disinfection technology standard " < third edition) the first fascicle " experimental technique specification " (Ministry of Public Health, 2014.4) middle relevant criterion judgement, the present invention is to lagophthalmos nonirritant.
Chmice acute Oral toxicity result of the test:
By the 3.7th carrying out in " disinfection technology standard " (third edition) first fascicle " experimental technique specification " (Ministry of Public Health, 2012.4).
Experimental animal: kunming mice 50, body weight 18-22 gram, male and female half and half: the quality certification number: dynamic No. 19-082nd, the word of doctor, is provided by Hubei Province's medical experiment animal center.Viewing duration, each dosage group (1250,2500,5000, lOOOOmg/kg) animal do not show obvious poisoning symptom, without animal dead, can judge that test specimen stock solution of the present invention is cutd open kunming mice acute oral LD50 and be greater than 5000mg/k.Judge according to relevant criterion in " disinfection technology standard " (third edition) first fascicle " experimental technique specification " (Ministry of Public Health, 2012.4), the present invention is actual nontoxic.
More than show that but gained nano woman's cleaning and nursing aloe lotion of the present invention has the effect of killing preferably antibacterial, superficial mycosis, deep fungal, and without irritating, nontoxic, harmless, have no side effect.
Below the present invention be described in detail, the above, be only the preferred embodiment of the present invention, do not limit the scope of the present invention, namely allly does impartial change according to the application's scope and modify, and all should still belong to covering scope of the present invention.
Claims (9)
1. an Aloe nursing lotion, comprise the Aloe nano suspending liquid natural juice of 30-90%, the hyaluronate sodium of 0.05-5%, the camomile extract of 0.05-2%, the polymeric material of 0.1-10%, the substrate of 0.80-53%, above percent is percetage by weight; Polymeric material used is carrageenan, arabic gum, alginate, starch, dextrin, Cera Flava, agar, chitosan; Substrate is sodium bicarbonate, sodium carbonate, sodium hydroxide, triethanolamine or carbamide, ethanol, isopropyl alcohol, glycerol or propylene glycol, ammonium lauryl sulfate, AESA and refining ostrich oil.
2. Aloe nursing lotion according to claim 1, is characterized in that: also containing the antioxidant of 0.05-2% and the antiseptic of 0.05-0.5%.
3. Aloe nursing lotion according to claim 1 and 2, is characterized in that: the Margarita powder micropowder below the vitamin E of the vitamin A or derivatives thereof containing 0.01-0.2%, the vitamin C or derivatives thereof of 0.01-0.2%, 0.01-0.5%, 100 orders of 0.01-1%, the Herba melissae axillaris powder of 0.01-1%, the propolis of 0.01-2% and the ultrafine zinc oxide particle of 0.01-1%.
4. Aloe nursing lotion according to claim 1, is characterized in that: the surfactant also containing 0.01-10%.
5. Aloe nursing lotion according to claim 1, it is characterized in that: comprise the Aloe nano suspending liquid natural juice of 50%, the hyaluronate sodium of 2%, camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 7% of 1%, the ethanol of 26.5%, the ammonium lauryl sulfate of 3%, the AESA of 3%, refining ostrich oil, 2% surfactant of 1.2%.
6. Aloe nursing lotion according to claim 1, is characterized in that: also containing the potassium sorbate of 0.5-1.5% and the carbomer of 0.6-0.8%.
7. Aloe nursing lotion according to claim 6, is characterized in that: the Herba Saussureae Involueratae extract also containing 1-2%.
8. Aloe nursing lotion according to claim 7, it is characterized in that: comprise the Aloe nano suspending liquid natural juice of 55%, the hyaluronate sodium of 3%, camomile extract, the gelatin of 2%, starch, the chitosan of 2%, the sodium bicarbonate of 0.3% of 6% of 1.4%, the ethanol of 17.5%, the ammonium lauryl sulfate of 3%, 3% AESA, 1.2% refining ostrich oil, 3% surfactant, the Herba Saussureae Involueratae extract of 1%, the potassium sorbate of 1% and 0.6% carbomer.
9. the preparation method of Aloe nursing lotion according to claim 1, it is characterized in that: choose 3 years thick Aloe prophylls of leave, non-woven fabrics is pasted in incision after cutting, and be built in less than 4 DEG C temperature cold preservations in 2 hours for subsequent use, during use, will through cleaning, Folium Aloe after disinfecting or the inside gelling after removing leaf skin, add 0.05% native cellulose E, under lOOOrpm-lOOOOrpm rotating speed, 5min-30min is processed through refiner or homogenizer, then by high frequency intense ultrasonic wave field cavitation, machined object granule is pulverized in high pressure homogenisers, ultramicronising, under lOMpa-300Mpa high pressure, produce the moment effluxvelocity of 200m/s-600m/s, make material particles produce cavitation and make its cracking, promote the increase of amorphous particle ratio in suspension or become amorphous particle completely, form the nanoparticle of lnm-700nm size, obtain Aloe nano suspending liquid: by gained Aloe nano suspending liquid, camomile extract, Herba Saussureae Involueratae extract and hyaluronate sodium, polymeric material and substrate stir 5min-20min with 200rpm-5000rpm rotating speed at 20 DEG C-80 DEG C, obtain required Aloe nursing lotion.
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| CN110403844A (en) * | 2019-08-29 | 2019-11-05 | 云南白药清逸堂实业有限公司 | Privates nurses film |
| CN113057928A (en) * | 2021-03-29 | 2021-07-02 | 烟台鲁量新材料科技有限公司 | Gel matrix containing aloe extract, nano zinc oxide antibacterial gel and preparation method thereof |
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Application publication date: 20150429 |