CN104498043B - It is a kind of to utilize microbe soil conditioner of waste residue of Chinese herbs production and preparation method thereof - Google Patents
It is a kind of to utilize microbe soil conditioner of waste residue of Chinese herbs production and preparation method thereof Download PDFInfo
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- CN104498043B CN104498043B CN201410690929.1A CN201410690929A CN104498043B CN 104498043 B CN104498043 B CN 104498043B CN 201410690929 A CN201410690929 A CN 201410690929A CN 104498043 B CN104498043 B CN 104498043B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/14—Soil-conditioning materials or soil-stabilising materials containing organic compounds only
- C09K17/18—Prepolymers; Macromolecular compounds
- C09K17/32—Prepolymers; Macromolecular compounds of natural origin, e.g. cellulosic materials
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- C—CHEMISTRY; METALLURGY
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- C09K2101/00—Agricultural use
Abstract
The present invention provides a kind of microbe soil conditioner for utilizing waste residue of Chinese herbs to produce and preparation method thereof, its preparation methods steps：Above-mentioned strain is activated respectively；Activated spawn is mixed, mixed strain and stoste are pressed 1:80 120 mixed culture, obtain compound criteria bacterium solution；Above-mentioned gained bacterium solution and raw material are pressed 1:15 40 mixed culture, obtain the microbe soil conditioner.Microorganism includes environment-friendly type decomposition strain and soil remediation type strain in the microbe soil conditioner；In gained microbe soil conditioner：Moisture weight percentage is≤10%；Microorganism bacterium amount >=2 × 108cfu/g；Glycoside percentage by weight is 0.3 1.0%；Polysaccharide percentage by weight is 0.3 0.8%.Microbe soil conditioner provided by the invention solves a large amount of exhaust emissions of industrial waste residue of Chinese herbs and the effect of improved soil.
Description
Technical field
Utilize the present invention relates to a kind of waste residue of Chinese herbs and produced with soil remediation field, more particularly to one kind using waste residue of Chinese herbs
Microbe soil conditioner.
Background technology
To adapt to the rhythm of life needs of modern people's quick and convenient, after Chinese patent drug is produced, industry carries the field of Chinese medicines
Waste residue of Chinese herbs processing problem after taking just annoyings Chinese patent drug processing industry always.Because waste residue of Chinese herbs carries with substantial amounts of industry
The organic solvent for taking process to remain, such as lipophylic organic solvents：Solvent chloroform, ether, ethyl acetate etc., hydrophily are organic molten
Agent：Methanol, ethanol, acetone etc..In addition a certain amount of plantation farm chemical ingredients are also left in waste residue of Chinese herbs.During these organic solvents make
Medicine waste residue be difficult in nature it is naturally decomposed bury, plus the amount cumulative year after year of waste residue of Chinese herbs, in the Chinese patent drug concentration of production
Area cause great environmental pollution.The Chinese medicine slag of the Chinese patent drug factory discharge in 1 year in Jilin Province somewhere just has 3400 tons
(2012), its composition cover 60 big kinds of Chinese medicine, there is the Radix Astragali, Ligusticum wallichii, the red sage root, honeysuckle, hempleaf groundsel herb, Radix Angelicae Sinensis, nine sections
Tea, etc..
Waste residue of Chinese herbs after industrial abstract PROCESS FOR TREATMENT remains what is had originally in Chinese medicine except the residual of organic solvent
Organic nutrient, micro- and substantial amounts of cellulose, such as the glycoside of the Radix Astragali, polysaccharide；The alkaloid of Ligusticum wallichii；The ketone of the red sage root
Class.It is desirable to have development in various regions to the trial that it is used, have and be processed into feed, organic fertilizer is also made
's.Organic fertilizer most is made, and utilize is natural fermentating process, and thus waste residue of Chinese herbs can only be as the original matrix of organic fertilizer
Additive, it is only 20% that addition, which is no more than waste residue of Chinese herbs in 50%, such as publication number CN101200390A application documents, and
And so fermentation time length, waste residue of Chinese herbs utilization rate are low, it is impossible to solve the Solid state fermentation requirement of a large amount of outputs of the pharmaceutical factory of traditional Chinese medicine；The opposing party
Fertilizer is only played a part of in face because the strain function of preparing organic fertilizer addition using waste residue of Chinese herbs in the prior art is single,
There is no the effect of soil improvement.
Therefore, seek a kind of effective processing method of energy, solve the exhaust emission of a large amount of industrial waste residue of Chinese herbs, and to it
Processing recycles, and waste residue of Chinese herbs is able to enter back into ecological recycle system green and healthyly and is played a part of improved soil
The urgency for just turning into the processing of industrial waste residue of Chinese herbs is waited to need to solve the problems, such as.
The content of the invention
The present invention for above technical problem provide it is a kind of using waste residue of Chinese herbs production microbe soil conditioner and
Its preparation method, it is therefore an objective to solve the emission pollution problem of a large amount of industrial waste residue of Chinese herbs.
The concrete technical scheme of the present invention is as described below：
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, the microbe soil conditioner include micro- life
Thing, the microorganism include environment-friendly type and decompose strain and soil remediation type strain.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, the environment-friendly type decompose strain component and
The weight proportion of each component includes：
The component of the soil remediation type strain and the weight proportion of each component include：
Sphingol single-cell 20-40%；
Lactobacillus plantarum 20-30%.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, the microbe soil conditioner is pulvis, its
In：Moisture weight percentage is≤10%, microorganism bacterium amount >=2 × 108cfu/g；The microbe soil conditioner includes
Effective bioactive ingredients of waste residue of Chinese herbs remaining：Glycoside percentage by weight is 0.3-1.0%, and polysaccharide percentage by weight is
0.3-0.8%.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, it is characterised in that comprise the following steps that：
1) above-mentioned strain is activated respectively；
2) activated spawn is mixed, by mixed strain and stoste by weight proportion 1：80-120 is mixed, and must be answered
Close culture bacterium solution；
3) by above-mentioned gained bacterium solution and raw material by weight proportion 1：15-40 is mixed, and obtains the microbe soil improvement
Agent；
Wherein, the raw material includes：Waste residue of Chinese herbs raw material, brown sugar, dibastic sodium phosphate, calcium carbonate.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, step 2 stoste press following percentage by weight
With taking：Romote antiquity brown sugar 5-10%, dibastic sodium phosphate 0.5-5%, calcium carbonate 0.5-5%, water 80-95%.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, step 3 raw material press following percentage by weight
With taking：Waste residue of Chinese herbs raw material 50-85%, brown sugar 2-5%, dibastic sodium phosphate 1-5%, calcium carbonate 0.5-5%；8th, will according to right
Seek the method described in 7, it is characterised in that the waste residue of Chinese herbs raw material are prepared by following methods：Waste residue of Chinese herbs after drying,
It is 20-40% that moisture is adjusted into part by weight with stalk or clear water.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, step 1 condition of culture are 20-35 DEG C, training
The foster time asks 48-72h.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, under the conditions of 20-35 DEG C, half seals the step 2
After closing culture 2-5 days, closed culture 10-15 days.
A kind of microbe soil conditioner produced using waste residue of Chinese herbs, for the step 3 under the conditions of 20-35 DEG C, half is close
After closing culture 1-5 days, closed culture 12-15 days.The present invention uses above-mentioned technical proposal, compared with prior art, has as follows
Technique effect：
The composite fermentation technology of strain and soil remediation type strain is decomposed by environment-friendly type, one is carried out to industrial waste residue of Chinese herbs
Secondary property integration transformation, have found one kind disposably can largely handle industrial waste residue of Chinese herbs, dissolve industrial waste residue of Chinese herbs pollution simultaneously
The industrial waste residue of Chinese herbs of pollution sources is entered back into the preparation method of ecological recycle system soil conditioner green and healthyly, and carry
Supply the continuous cropping obstacle to soil, play the new soil for repairing improving effect the problems such as the pollution by chemical fertilizer of agricultural chemicals hormone, disruption of ecological balance
Earth modifying agent.
Brief description of the drawings
Accompanying drawing 1 is cucumber yield bar chart in embodiment three
Embodiment
Embodiment one：
1. prepared by strain
Will from Chinese agriculture Microbiological Culture Collection administrative center buy flavobacterium breve (Empedobacters brevis,
ACCC02769), Sphingobacterium multivorum (Sphingobacterium multivorum, ACCC02849), brevibacterium epidermidis
(Brevibacterium Brevibacterium, ACCC02655), bacillus subtilis (Bacillus subtilis,
ACCC01872)；Soil remediation type strain flock mating ratio be Sphingol single-cell (Sphingomonas yanoikuyae,
ACCC01034), Lactobacillus plantarum (Lactobacillus plantarum, ACCC11016) is transferred into MRS Liquid Cultures respectively
In the conical flask of base, cultivate 48 hours at 30 DEG C, taken out after culture medium muddiness, it is stand-by to be put into 4 DEG C of refrigerators preservations.
2. the compatibility of flora is cultivated：
(1) the strain that step 1 is cultivated is weighed by following percentage by weight：Flavobacterium breve 5%, Sphingobacterium multivorum
10%, brevibacterium epidermidis 10%, bacillus subtilis 20%；Soil remediation type strain flock mating ratio is Sphingol single-cell 30%,
Lactobacillus plantarum 25%.
(2) strain compound criteria：The strain weighed by more than is put into the raw material of following proportioning by weight 1: 100：Romote antiquity
Brown sugar 10%, sodium sulphate 1.0%, calcium carbonate 0.5%, pure water 88.5%, it is put into 28 DEG C of semi-hermetics after fermentation tank stirs
Culture 2 days, then closed culture, cultivate 10 days.
3. composite fermentation produces：
(1) the major class of waste residue of Chinese herbs raw material has, the Radix Astragali, Ligusticum wallichii, the red sage root, honeysuckle, sarcandra, Radix Angelicae Sinensis, also jujube,
Corydlis bungeana, the root of kudzu vine, whorlleaf stonecrop herb, reed rhizome, radix glycyrrhizae etc.；
(2) with powder of straw water transfer point to 30%.
(3) composite fermentation：By the bacterium solution of 2. compound criterias by weight 1：15 are put into the raw material of following proportioning：Chinese medicine gives up
Slag raw material 94%, brown sugar 5%, dibastic sodium phosphate 0.5%, calcium carbonate 0.5%, it is put into 25 DEG C of semi-hermetics after fermentation tank stirs
Culture 1 day, 28 DEG C it is closed culture 15 days；
4. the preparation of product
(1) the waste residue of Chinese herbs by completion of fermenting enters vibra fluidized bed drying, 80 DEG C of EAT, 50 DEG C of leaving air temp.Into
Product moisture<5%.
Crush pack storage, microbe soil conditioner.
Embodiment two：
1. prepared by strain：With embodiment one；
2. the compatibility of flora is cultivated：
(1) the strain that step 1 is cultivated is weighed by following percentage by weight：Flavobacterium breve 8%, Sphingobacterium multivorum
8%, brevibacterium epidermidis 15%, bacillus subtilis 20%；Soil remediation type strain flock mating ratio is Sphingol single-cell 24%, is planted
Thing lactobacillus 25%.
(2) strain compound criteria：The strain weighed by more than is by weight 1：80 are put into the raw material of following proportioning：Romote antiquity
Brown sugar 5%, sodium sulphate 3%, calcium carbonate 2%, pure water 80%, 25 DEG C of semi-hermetic cultures 3 days are put into after fermentation tank stirs,
Closed culture again, cultivate 12 days.
3. composite fermentation produces：
(1) waste residue of Chinese herbs raw material have semen armeniacae amarae, ilex pubescens, leech, plantain seed, Ramulus Taxilli, caulis clematidis armandii, Sculellaria barbata, Qu
Wheat, rush, Armstrong, pyrrosia lingua, folium isatidis, mulberry leaf, radix glycyrrhizae, sophora flower, pseudo-ginseng, rhizoma alismatis, Scullcap stem and leaf, chrysanthemum indicum, hawthorn, ginseng
Fruit etc..
(2) with powder of straw water transfer point to 25%.
(3) composite fermentation：By the bacterium solution of 2. compound criterias by weight 1：20 are put into the raw material of following proportioning：Chinese medicine gives up
Slag raw material 96%, brown sugar 3%, dibastic sodium phosphate 0.5%, calcium carbonate 0.5%, it is put into 22 DEG C of semi-hermetics after fermentation tank stirs
Culture 2 days, 30 DEG C it is closed culture 10 days；
4. the preparation of product
(1) the waste residue of Chinese herbs by completion of fermenting enters vibra fluidized bed drying, 90 DEG C of EAT, 60 DEG C of leaving air temp.Into
Product moisture<5%.
Crush pack storage, microbe soil conditioner.
Embodiment three：
1. microbe soil conditioner testing result：
| Total glycosides | Total starches | Total bacterium amount | Magnesium | Manganese |
| 0.8% | 0.7% | 3×108cfu/g | 1360μg/g | 74μg/g |
2. it is used for succession cropping obstacle of green cucumber soil：
2 weeks before plantation, every mu of 300 kilograms of dispenser in ground, turn over and bury.Routinely fertilising uses after plantation, every mu of ground dispenser
150 kilograms, while common fertilizer is reduced.Cucumber yield refers to Fig. 1.
The specific embodiment of the present invention is described in detail above, but it is intended only as example, it is of the invention and unlimited
It is formed on particular embodiments described above.To those skilled in the art, it is any to the equivalent modifications that carry out of the present invention and
Substitute also all among scope of the invention.Therefore, the impartial conversion made without departing from the spirit and scope of the invention and
Modification, all should be contained within the scope of the invention.
Claims (8)
- A kind of 1. microbe soil conditioner produced using waste residue of Chinese herbs, it is characterised in that the microbe soil conditioner Including microorganism, the microorganism includes environment-friendly type and decomposes strain and soil remediation type strain；Wherein, the environment-friendly type decomposer The component of kind and the weight proportion of each component include：The component of the soil remediation type strain and the weight proportion of each component include：Sphingol single-cell 20-40%；Lactobacillus plantarum 20-30%.
- 2. microbe soil conditioner according to claim 1, it is characterised in that the microbe soil conditioner is powder Agent, wherein：Moisture weight percentage is≤10%, microorganism bacterium amount >=2 × 108cfu/g；The microbe soil conditioner bag Effective bioactive ingredients containing waste residue of Chinese herbs remaining：Glycoside percentage by weight is 0.3-1.0%, polysaccharide percentage by weight For 0.3-0.8%.
- 3. a kind of preparation method of microbe soil conditioner according to claim 1, it is characterised in that specific steps are such as Under：1) above-mentioned strain is activated respectively；2) activated spawn is mixed, by mixed strain and stoste by weight proportion 1：80-120 is mixed, and obtains compound training Bacteria liquid；3) by bacterium solution obtained by step 2) and raw material by weight proportion 1：15-40 is mixed, and obtains the microbe soil conditioner；Wherein, the raw material includes：Waste residue of Chinese herbs raw material, brown sugar, dibastic sodium phosphate, calcium carbonate；Wherein, the stoste is matched somebody with somebody by following percentage by weight and taken：Romote antiquity brown sugar 5-10%, dibastic sodium phosphate 0.5-5%, calcium carbonate 0.5-5%, water 80-95%.
- 4. according to the method for claim 3, it is characterised in that the step 3) raw material is matched somebody with somebody by following percentage by weight to be taken： Waste residue of Chinese herbs raw material 50-85%, brown sugar 2-5%, dibastic sodium phosphate 1-5%, calcium carbonate 0.5-5%.
- 5. according to the method for claim 3, it is characterised in that the waste residue of Chinese herbs raw material are prepared by following methods：In After drying, it is 20-40% that moisture is adjusted into part by weight with stalk or clear water to medicine waste residue.
- 6. according to the method for claim 3, it is characterised in that the step 1) condition of culture is 20-35 DEG C, incubation time For 48-72h.
- 7. according to the method for claim 3, it is characterised in that the step 2) is under the conditions of 20-35 DEG C, semiclosed culture After 2-5 days, closed culture 10-15 days.
- 8. according to the method for claim 3, it is characterised in that the step 3) is under the conditions of 20-35 DEG C, semi-hermetic culture After 1-5 days, closed culture 12-15 days.
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| CN105176855B (en) * | 2015-04-29 | 2018-01-19 | 齐齐哈尔大学 | One plant of Sphingomonas bacterium obtained through separation and its application in continuous cropping watermelon growing is promoted |
| CN106833655B (en) * | 2016-12-23 | 2019-05-28 | 上海交通大学 | Solidify microbial inoculum for the agricultural land soil Cd microorganism administered |
| CN109758713B (en) * | 2019-01-26 | 2021-02-05 | 吉林省农业科学院 | Biodegradation method of sulfonylurea herbicide |
| CN115259971A (en) * | 2022-08-30 | 2022-11-01 | 苏华山 | Traditional Chinese medicine fermented soil conditioner and preparation method and application thereof |
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