CN104492372A - 一种用于吸附废水中重金属材料的制备方法及其应用 - Google Patents
一种用于吸附废水中重金属材料的制备方法及其应用 Download PDFInfo
- Publication number
- CN104492372A CN104492372A CN201410704542.7A CN201410704542A CN104492372A CN 104492372 A CN104492372 A CN 104492372A CN 201410704542 A CN201410704542 A CN 201410704542A CN 104492372 A CN104492372 A CN 104492372A
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- Prior art keywords
- flyash
- heavy metal
- waste water
- adsorbing
- nickel slag
- Prior art date
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- Granted
Links
- 239000000463 material Substances 0.000 title claims abstract description 53
- 229910001385 heavy metal Inorganic materials 0.000 title claims abstract description 37
- 239000002351 wastewater Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical group [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 63
- 239000002131 composite material Substances 0.000 claims abstract description 23
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 16
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 150000002500 ions Chemical class 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 239000010883 coal ash Substances 0.000 claims abstract description 6
- 239000002699 waste material Substances 0.000 claims abstract description 6
- 229910052759 nickel Inorganic materials 0.000 claims description 36
- 239000002893 slag Substances 0.000 claims description 36
- 239000010881 fly ash Substances 0.000 claims description 32
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 15
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 15
- 244000144972 livestock Species 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 12
- 238000007493 shaping process Methods 0.000 claims description 12
- 238000009395 breeding Methods 0.000 claims description 11
- 230000001488 breeding effect Effects 0.000 claims description 11
- 239000007767 bonding agent Substances 0.000 claims description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 8
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 7
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 6
- 230000032683 aging Effects 0.000 claims description 6
- 238000000498 ball milling Methods 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000013467 fragmentation Methods 0.000 claims description 6
- 238000006062 fragmentation reaction Methods 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 229910017604 nitric acid Inorganic materials 0.000 claims description 6
- 230000020477 pH reduction Effects 0.000 claims description 6
- 239000002002 slurry Substances 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 229920002689 polyvinyl acetate Polymers 0.000 claims description 3
- 239000011118 polyvinyl acetate Substances 0.000 claims description 3
- 239000004801 Chlorinated PVC Substances 0.000 claims description 2
- 229920002367 Polyisobutene Polymers 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 229920000457 chlorinated polyvinyl chloride Polymers 0.000 claims description 2
- 238000003795 desorption Methods 0.000 claims description 2
- 238000001179 sorption measurement Methods 0.000 abstract description 31
- 239000002440 industrial waste Substances 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000465 moulding Methods 0.000 abstract 1
- 238000003825 pressing Methods 0.000 abstract 1
- 238000002474 experimental method Methods 0.000 description 5
- 230000000274 adsorptive effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 244000144977 poultry Species 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000009388 chemical precipitation Methods 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 239000002910 solid waste Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 229910020489 SiO3 Inorganic materials 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 210000004884 grey matter Anatomy 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000009304 pastoral farming Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000009374 poultry farming Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- CCEKAJIANROZEO-UHFFFAOYSA-N sulfluramid Chemical group CCNS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F CCEKAJIANROZEO-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/42—Materials comprising a mixture of inorganic materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4875—Sorbents characterised by the starting material used for their preparation the starting material being a waste, residue or of undefined composition
- B01J2220/4887—Residues, wastes, e.g. garbage, municipal or industrial sludges, compost, animal manure; fly-ashes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/20—Nature of the water, waste water, sewage or sludge to be treated from animal husbandry
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Water Treatment By Sorption (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410704542.7A CN104492372B (zh) | 2014-11-27 | 2014-11-27 | 一种用于吸附废水中重金属材料的制备方法及其应用 |
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CN201410704542.7A CN104492372B (zh) | 2014-11-27 | 2014-11-27 | 一种用于吸附废水中重金属材料的制备方法及其应用 |
Publications (2)
Publication Number | Publication Date |
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CN104492372A true CN104492372A (zh) | 2015-04-08 |
CN104492372B CN104492372B (zh) | 2017-06-27 |
Family
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CN201410704542.7A Active CN104492372B (zh) | 2014-11-27 | 2014-11-27 | 一种用于吸附废水中重金属材料的制备方法及其应用 |
Country Status (1)
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CN (1) | CN104492372B (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106315801A (zh) * | 2016-09-08 | 2017-01-11 | 北京神雾环境能源科技集团股份有限公司 | 一种电镀废水净化剂及其制备方法和应用 |
CN108264253A (zh) * | 2018-01-17 | 2018-07-10 | 武汉理工大学 | 一种具有重金属离子清除能力的透水混凝土的制备方法 |
TWI639708B (zh) * | 2017-06-30 | 2018-11-01 | 衍鋐機械股份有限公司 | Method for manufacturing nickel-containing slag plastic product |
CN108910981A (zh) * | 2018-07-31 | 2018-11-30 | 四川绵竹三佳饲料有限责任公司 | 一种含磷废水净化剂及磷矿废渣渗透污水处理方法 |
CN108947435A (zh) * | 2018-07-12 | 2018-12-07 | 昆明理工大学 | 一种协同处置矿山重金属废水的矿山充填材料及其制备方法 |
CN112058212A (zh) * | 2020-08-30 | 2020-12-11 | 昆明理工大学 | 一种利用镍铁渣粉末吸附重金属的方法 |
CN114210299A (zh) * | 2021-12-15 | 2022-03-22 | 国家能源投资集团有限责任公司 | 粉煤灰基除氟吸附剂的制备方法及粉煤灰基除氟吸附剂 |
CN116078343A (zh) * | 2022-12-07 | 2023-05-09 | 上海蓝科石化环保科技股份有限公司 | 一种用于脱除废气中重金属的吸附剂及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2003300723A (ja) * | 2002-04-04 | 2003-10-21 | ▲吉▼田工機株式会社 | 粒状石炭灰のゼオライト化改質方法及び装置 |
CN101422720A (zh) * | 2008-11-24 | 2009-05-06 | 中国科学院生态环境研究中心 | 一种基于原位生成复合金属氧化物的吸附过滤除砷方法 |
CN102908988A (zh) * | 2012-10-08 | 2013-02-06 | 淮海工学院 | 一种具有吸附清除含乙酰二甲胺工业废水的吸附剂及其制备方法 |
CN103831080A (zh) * | 2014-03-12 | 2014-06-04 | 福州大学 | 用于回收废水中重金属离子的镍渣吸附材料及其制备 |
-
2014
- 2014-11-27 CN CN201410704542.7A patent/CN104492372B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2003300723A (ja) * | 2002-04-04 | 2003-10-21 | ▲吉▼田工機株式会社 | 粒状石炭灰のゼオライト化改質方法及び装置 |
CN101422720A (zh) * | 2008-11-24 | 2009-05-06 | 中国科学院生态环境研究中心 | 一种基于原位生成复合金属氧化物的吸附过滤除砷方法 |
CN102908988A (zh) * | 2012-10-08 | 2013-02-06 | 淮海工学院 | 一种具有吸附清除含乙酰二甲胺工业废水的吸附剂及其制备方法 |
CN103831080A (zh) * | 2014-03-12 | 2014-06-04 | 福州大学 | 用于回收废水中重金属离子的镍渣吸附材料及其制备 |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106315801A (zh) * | 2016-09-08 | 2017-01-11 | 北京神雾环境能源科技集团股份有限公司 | 一种电镀废水净化剂及其制备方法和应用 |
TWI639708B (zh) * | 2017-06-30 | 2018-11-01 | 衍鋐機械股份有限公司 | Method for manufacturing nickel-containing slag plastic product |
CN108264253A (zh) * | 2018-01-17 | 2018-07-10 | 武汉理工大学 | 一种具有重金属离子清除能力的透水混凝土的制备方法 |
CN108947435A (zh) * | 2018-07-12 | 2018-12-07 | 昆明理工大学 | 一种协同处置矿山重金属废水的矿山充填材料及其制备方法 |
CN108910981A (zh) * | 2018-07-31 | 2018-11-30 | 四川绵竹三佳饲料有限责任公司 | 一种含磷废水净化剂及磷矿废渣渗透污水处理方法 |
CN112058212A (zh) * | 2020-08-30 | 2020-12-11 | 昆明理工大学 | 一种利用镍铁渣粉末吸附重金属的方法 |
CN114210299A (zh) * | 2021-12-15 | 2022-03-22 | 国家能源投资集团有限责任公司 | 粉煤灰基除氟吸附剂的制备方法及粉煤灰基除氟吸附剂 |
CN114210299B (zh) * | 2021-12-15 | 2023-11-03 | 国家能源投资集团有限责任公司 | 粉煤灰基除氟吸附剂的制备方法及粉煤灰基除氟吸附剂 |
CN116078343A (zh) * | 2022-12-07 | 2023-05-09 | 上海蓝科石化环保科技股份有限公司 | 一种用于脱除废气中重金属的吸附剂及其制备方法 |
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Inventor after: Han Zhe Inventor after: Li Haiyang Inventor after: Dan Ranran Inventor after: Zhu Ying Inventor after: Yang Kai Inventor after: Shao Yanqiu Inventor after: Tang Houquan Inventor after: Jin Jianchao Inventor after: Guo Ru Inventor after: Liu Mei Inventor after: Su Chenghua Inventor before: Han Zhe Inventor before: Wang Xuke Inventor before: Zhu Ying Inventor before: Li Jing Inventor before: Chen Yanling |
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Address after: 256601 No. eight, No. 357, the Yellow River Road, Shandong, Binzhou Co-patentee after: Inst. of New Materials, Shandong Academy of Sciences Patentee after: SHANDONG ANHE SECURITY TECHNOLOGY RESEARCH INSTITUTE CO., LTD. Address before: 250014 Shandong Province, Lixia District, Ji'nan City Hospital Road, No. 19 Co-patentee before: SHANDONG ANHE SECURITY TECHNOLOGY RESEARCH INSTITUTE CO., LTD. Patentee before: Inst. of New Materials, Shandong Academy of Sciences |
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Inventor after: Han Zhe Inventor after: Li Haiyang Inventor after: Dan Ranran Inventor after: Zhu Ying Inventor after: Yang Kai Inventor after: Shao Yanqiu Inventor after: Tang Houquan Inventor after: Jin Jianchao Inventor after: Guo Ru Inventor after: Liu Mei Inventor after: Su Chenghua Inventor before: Han Zhe Inventor before: Zhu Ying Inventor before: Tang Houquan Inventor before: Jin Jianchao Inventor before: Guo Ru Inventor before: Liu Mei Inventor before: Su Chenghua Inventor before: Li Haiyang |
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Address after: 250014 Shandong Province, Lixia District, Ji'nan City Hospital Road, No. 19 Co-patentee after: SHANDONG ANHE SECURITY TECHNOLOGY RESEARCH INSTITUTE CO., LTD. Patentee after: Inst. of New Materials, Shandong Academy of Sciences Address before: 256601 No. eight, No. 357, the Yellow River Road, Shandong, Binzhou Co-patentee before: Inst. of New Materials, Shandong Academy of Sciences Patentee before: SHANDONG ANHE SECURITY TECHNOLOGY RESEARCH INSTITUTE CO., LTD. |
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