CN104430625A - Method for preparing special environment-friendly bactericide for flowers and plants - Google Patents
Method for preparing special environment-friendly bactericide for flowers and plants Download PDFInfo
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- CN104430625A CN104430625A CN201410633553.0A CN201410633553A CN104430625A CN 104430625 A CN104430625 A CN 104430625A CN 201410633553 A CN201410633553 A CN 201410633553A CN 104430625 A CN104430625 A CN 104430625A
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Abstract
The invention discloses a method for preparing a special environment-friendly bactericide for flowers and plants. The preparation method comprises the following steps: fermenting with a pasty artemisia ordosica solution and green Chinese onion and garlic bulb filtrate as main raw materials, and a microbial fermentation assistant as an auxiliary material, thereby preparing the special environment-friendly bactericide for flowers and plants. The special environment-friendly bactericide for flowers and plants comprises the following components in parts by weight: 40-60 parts of a pasty artemisia ordosica solution, 20-30 parts of green Chinese onion and garlic bulb filtrate and 10-20 parts of a microbial fermentation assistant. According to the special environment-friendly bactericide for flowers and plants prepared by the method, the pure biological materials serve as raw materials, the bactericide is prepared by fermentation, the preparation method is easy and convenient, the preparation process is environmentally friendly, the environmental pollution is avoided, and the prepared bactericide is wide in fungicidal spectrum and long in duration.
Description
Technical field:
The invention belongs to flowers sterilization technology field, particularly a kind of preparation method of flowers special environment protection bactericide.
Background technology:
In recent years, along with the raising day by day of people's living standard, flowers market is also day by day well sold and in short supply, the flowers imported and exported are also increasing, cause some pathogens import into and be diffused into various places, and along with organic evolution, the kind of pathogen also gets more and more, and causes certain puzzlement to the development of the industry of flowers and plants.Therefore the integrated control technique that biological control is taken as the leading factor more and more comes into one's own.
The bactericide general toxicity of flowers is low, even nontoxic, and the mechanism of bactericide is comparatively complicated, is generally the biosynthesis organizing pathogen albumen.At present, the biological bactericide of flowers mainly contains several: Te Like, benefit plant spirit, cleer and peaceful of polyoxy is multiple special.Sterilization can also be carried out with garlic juice, shallot liquid, rice vinegar liquid, saleratus solution and potassium permanganate in daily life.
Special Garrick has another name called sterilization ling, and be pure biological living preparation, toxicity is low, have the effect of sterilization, hyperparasitism, bacteriolyze, toxic protein and competition, but it is preferably used alone, can not, Basic pesticides acid with other or bactericide mixed.The toxicity that benefit plants spirit is also low, has that fungicidal spectrum is wide, resistance of rainwater washing against and an anti-corrosive fresh-keeping effect, after its dilution can with other acid or neutral combined use of pesticides.Polyoxy have another name called clearly many can bacterium, polyoxy toxin, Pola peace etc., its toxicity is low, uses after dilution, but must not be mixed with Basic pesticides.The multiple spy of root has another name called root-rot 110, and toxicity is extremely low, almost non-toxic, and it, except energy sterilization sterilizing, can also promote weak seedling root growth, makes old root activate shape root, prevent flowers early ageing, but it can not be mixed with Basic pesticides.
Summary of the invention:
The object of this invention is to provide a kind of preparation method of flowers special environment protection bactericide, adopt black sand sagebrush (Artemisia filifolia) solution and shallot head of garlic filtrate as primary raw material, coordinate fermentable auxiliary agent, through the flowers special environment protection bactericide obtained that ferments, this bactericide adopts pure biofermentation to prepare, environmental protection, and fungicidal spectrum is wide, timeliness is long.
Object of the present invention is achieved through the following technical solutions:
A preparation method for flowers special environment protection bactericide, comprises the following steps:
(1) after shallot and the head of garlic being cleaned up, mash rubbing, add water, ultrasonic 10-20min, 90-95 DEG C of poach 2-3h, cold filtration, obtains shallot head of garlic filtrate;
(2) cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state;
(3) the black sand sagebrush (Artemisia filifolia) solution of pulpous state step (2) obtained carries out high-temperature sterilization, be cooled to 20-35 DEG C, add the shallot head of garlic filtrate that step (1) obtains, stir, add fermentable auxiliary agent again, 30-40 DEG C of fermentation 10-12h, obtains flowers special environment protection bactericide.
Preferred as technique scheme, the shallot described in step (1) and the weight ratio of the head of garlic are 2:3.
Preferred as technique scheme, in the shallot head of garlic filtrate described in step (1), the content of the shallot head of garlic is 20-35%.
Preferred as technique scheme, the ultrasonic time described in step (2) is 30-60min.
Preferred as technique scheme, in the pulpous state black sand sagebrush (Artemisia filifolia) solution described in step (2), the concentration of black sand sagebrush (Artemisia filifolia) is 40-60%.
Preferred as technique scheme, the temperature of the high-temperature sterilization described in step (3) is 100-120 DEG C, and the time is 20-30min.
Preferred as technique scheme, the fermentable auxiliary agent described in step (3) is one or more in bacillus laterosporus, bacillus megaterium or bacillus subtilis.
Preferred as technique scheme, the component in the flowers special environment protection bactericide described in step (3), by weight, comprising: pulpous state black sand sagebrush (Artemisia filifolia) solution 40-60 part, shallot head of garlic filtrate 20-30 part, fermentable auxiliary agent 10-20 part.
Beneficial effect of the present invention is: the main component in flowers special environment protection bactericide is black sand sagebrush (Artemisia filifolia); the branches and leaves of black sand sagebrush (Artemisia filifolia) have certain drug effect, can carry out gentle bactericidal to flowers, and stable performance; chronically for flowers provide protection, the interference of bacterium can be prevented.Composition also containing the shallot head of garlic in bactericide prepared by this method, can take precautions against powdery mildew, black spot etc.
The pure biology of flowers special environment protection bactericide prepared by this method is as raw material, each component is fermented, can prevent component ferment in use produce high temperature to the infringement of flowers, this method preparation method is easy, the residue environmentally safe of preparation, can as Fertilizer application, therefore this preparation method environmental protection, and the sterilization of energy high-efficient and lasting.
Embodiment:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only for explaining the present invention, does not form limiting the scope of the present invention.
Embodiment 1:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 20min, 95 DEG C of poach 2h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 35%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 60min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 60%.
By weight, after black for the pulpous state of 40 parts sand sagebrush (Artemisia filifolia) solution 120 DEG C of sterilizing 20min, be cooled to 35 DEG C, add the shallot head of garlic filtrate of 20 parts, stir, add the bacillus laterosporus of 20 parts and bacillus subtilis again as fermentable auxiliary agent, 30 DEG C of fermentation 12h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 85% to the strick precaution rate of China rose.
Embodiment 2:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 10min, 90 DEG C of poach 3h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 20%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 30min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 40%.
By weight, after black for the pulpous state of 60 parts sand sagebrush (Artemisia filifolia) solution 100 DEG C of sterilizing 30min, 20 DEG C are cooled to, add the shallot head of garlic filtrate of 30 parts, stir, then the bacillus subtilis adding 20 parts is as fermentable auxiliary agent, 40 DEG C of fermentation 10h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 88% to the strick precaution rate of China rose.
Embodiment 3:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 15min, 90 DEG C of poach 2.5h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 25%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 50min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 450%.
By weight, after black for the pulpous state of 50 parts sand sagebrush (Artemisia filifolia) solution 110 DEG C of sterilizing 25min, be cooled to 25 DEG C, add the shallot head of garlic filtrate of 25 parts, stir, add the bacillus megaterium of 15 parts and bacillus subtilis again as fermentable auxiliary agent, 35 DEG C of fermentation 11h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 86% to the strick precaution rate of China rose.
Embodiment 4:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 20min, 95 DEG C of poach 3h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 35%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 60min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 60%.
By weight, after black for the pulpous state of 60 parts sand sagebrush (Artemisia filifolia) solution 120 DEG C of sterilizing 30min, be cooled to 35 DEG C, add the shallot head of garlic filtrate of 30 parts, stir, add the bacillus laterosporus of 20 parts, bacillus megaterium and bacillus subtilis again as fermentable auxiliary agent, 40 DEG C of fermentation 12h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 88% to the strick precaution rate of China rose.
Embodiment 5:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 13min, 92 DEG C of poach 2.5h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 20-35%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 40min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 55%.
By weight, after black for the pulpous state of 53 parts sand sagebrush (Artemisia filifolia) solution 115 DEG C of sterilizing 25min, 25 DEG C are cooled to, add the shallot head of garlic filtrate of 26 parts, stir, then the bacillus subtilis adding 12 parts is as fermentable auxiliary agent, 30 DEG C of fermentation 11.5h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 86% to the strick precaution rate of China rose.
Embodiment 6:
After shallot and the head of garlic being cleaned up, by weight being 2:3 mixing, mash rubbing, add water, ultrasonic 10min, 90 DEG C of poach 2h, cold filtration, obtain shallot head of garlic filtrate, wherein the content of the shallot head of garlic is 20%.
Cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic 30min, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state that concentration is 40%.
By weight, after black for the pulpous state of 40 parts sand sagebrush (Artemisia filifolia) solution 100 DEG C of sterilizing 20min, 20 DEG C are cooled to, add the shallot head of garlic filtrate of 20 parts, stir, then the bacillus laterosporus adding 10 parts is as fermentable auxiliary agent, 30 DEG C of fermentation 10h, obtain flowers special environment protection bactericide.
After measured, the flowers special environment protection bactericide of preparation meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is 84% to the strick precaution rate of China rose.
Through above-described embodiment, known, flowers special environment protection bactericide prepared by this method meets the quality standard of CCGF 402.2-2010 bactericide, after dispenser 30 days, is about 85% to the strick precaution rate of China rose.
Claims (8)
1. a preparation method for flowers special environment protection bactericide, is characterized in that, the method comprises the following steps:
(1) after shallot and the head of garlic being cleaned up, mash rubbing, add water, ultrasonic 10-20min, 90-95 DEG C of poach 2-3h, cold filtration, obtains shallot head of garlic filtrate;
(2) cleaned up by the stem branches and leaves of black sand sagebrush (Artemisia filifolia), shred and be ground to 50 orders, add ethyl acetate, ultrasonic, agitation and filtration, obtains first-time filtrate, then first-time filtrate is carried out being ground to 150 orders, filters, obtains the black sand sagebrush (Artemisia filifolia) solution of pulpous state;
(3) the black sand sagebrush (Artemisia filifolia) solution of pulpous state step (2) obtained carries out high-temperature sterilization, be cooled to 20-35 DEG C, add the shallot head of garlic filtrate that step (1) obtains, stir, add fermentable auxiliary agent again, 30-40 DEG C of fermentation 10-12h, obtains flowers special environment protection bactericide.
2. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, is characterized in that, the shallot described in step (1) and the weight ratio of the head of garlic are 2:3.
3. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, is characterized in that, in the shallot head of garlic filtrate described in step (1), the content of the shallot head of garlic is 20-35%.
4. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, it is characterized in that, the ultrasonic time described in step (2) is 30-60min.
5. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, is characterized in that, in the pulpous state black sand sagebrush (Artemisia filifolia) solution described in step (2), the concentration of black sand sagebrush (Artemisia filifolia) is 40-60%.
6. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, is characterized in that, the temperature of the high-temperature sterilization described in step (3) is 100-120 DEG C, and the time is 20-30min.
7. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, is characterized in that, the fermentable auxiliary agent described in step (3) is one or more in bacillus laterosporus, bacillus megaterium or bacillus subtilis.
8. the preparation method of a kind of flowers special environment protection bactericide as claimed in claim 1, it is characterized in that, component in flowers special environment protection bactericide described in step (3), by weight, comprise: pulpous state black sand sagebrush (Artemisia filifolia) solution 40-60 part, shallot head of garlic filtrate 20-30 part, fermentable auxiliary agent 10-20 part.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410633553.0A CN104430625A (en) | 2014-11-12 | 2014-11-12 | Method for preparing special environment-friendly bactericide for flowers and plants |
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| CN201410633553.0A CN104430625A (en) | 2014-11-12 | 2014-11-12 | Method for preparing special environment-friendly bactericide for flowers and plants |
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| CN104430625A true CN104430625A (en) | 2015-03-25 |
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| CN201410633553.0A Pending CN104430625A (en) | 2014-11-12 | 2014-11-12 | Method for preparing special environment-friendly bactericide for flowers and plants |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106386894A (en) * | 2016-08-31 | 2017-02-15 | 常州亚当生物技术有限公司 | Preparation and applications of insect repellent composite fertilizer |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101697740A (en) * | 2009-04-04 | 2010-04-28 | 冯子龙 | Novel traditional Chinese medicine pesticide and production technology thereof |
| CN102210327A (en) * | 2011-06-09 | 2011-10-12 | 北京融青生态农业有限公司 | Biological broad spectrum bactericide and preparation method thereof |
| CN102265906A (en) * | 2011-05-30 | 2011-12-07 | 杨凌农科大无公害农药研究服务中心 | Artemisia ordosica Kraschen bactericide and preparation method thereof |
-
2014
- 2014-11-12 CN CN201410633553.0A patent/CN104430625A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101697740A (en) * | 2009-04-04 | 2010-04-28 | 冯子龙 | Novel traditional Chinese medicine pesticide and production technology thereof |
| CN102265906A (en) * | 2011-05-30 | 2011-12-07 | 杨凌农科大无公害农药研究服务中心 | Artemisia ordosica Kraschen bactericide and preparation method thereof |
| CN102210327A (en) * | 2011-06-09 | 2011-10-12 | 北京融青生态农业有限公司 | Biological broad spectrum bactericide and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 浙江省科学研究所: "《农药植物手册》", 30 November 1958, 科技卫生出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106386894A (en) * | 2016-08-31 | 2017-02-15 | 常州亚当生物技术有限公司 | Preparation and applications of insect repellent composite fertilizer |
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Application publication date: 20150325 |
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