CN104419949B - 水解氨基酸制备方法 - Google Patents
水解氨基酸制备方法 Download PDFInfo
- Publication number
- CN104419949B CN104419949B CN201310547178.3A CN201310547178A CN104419949B CN 104419949 B CN104419949 B CN 104419949B CN 201310547178 A CN201310547178 A CN 201310547178A CN 104419949 B CN104419949 B CN 104419949B
- Authority
- CN
- China
- Prior art keywords
- amino acid
- reaction liquid
- acid
- hydrolysis amino
- fur
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 53
- 238000004519 manufacturing process Methods 0.000 title description 2
- 238000006243 chemical reaction Methods 0.000 claims abstract description 29
- 239000002253 acid Substances 0.000 claims abstract description 22
- 238000005868 electrolysis reaction Methods 0.000 claims abstract description 22
- 239000000376 reactant Substances 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 239000012295 chemical reaction liquid Substances 0.000 claims description 32
- 230000007062 hydrolysis Effects 0.000 claims description 32
- 238000006460 hydrolysis reaction Methods 0.000 claims description 32
- 238000002360 preparation method Methods 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 17
- 238000006386 neutralization reaction Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 238000010348 incorporation Methods 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 4
- MFGOFGRYDNHJTA-UHFFFAOYSA-N 2-amino-1-(2-fluorophenyl)ethanol Chemical compound NCC(O)C1=CC=CC=C1F MFGOFGRYDNHJTA-UHFFFAOYSA-N 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 2
- HUCVOHYBFXVBRW-UHFFFAOYSA-M caesium hydroxide Inorganic materials [OH-].[Cs+] HUCVOHYBFXVBRW-UHFFFAOYSA-M 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 239000003513 alkali Substances 0.000 abstract description 2
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 230000003472 neutralizing effect Effects 0.000 abstract 2
- 239000002699 waste material Substances 0.000 abstract 2
- 235000001014 amino acid Nutrition 0.000 description 41
- 241000196324 Embryophyta Species 0.000 description 13
- 210000003746 feather Anatomy 0.000 description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000003337 fertilizer Substances 0.000 description 7
- 108090000623 proteins and genes Proteins 0.000 description 7
- 102000004169 proteins and genes Human genes 0.000 description 7
- 239000007788 liquid Substances 0.000 description 6
- 235000018102 proteins Nutrition 0.000 description 6
- 238000010586 diagram Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 101710200191 Feather keratin Proteins 0.000 description 4
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 4
- 102000011782 Keratins Human genes 0.000 description 4
- 108010076876 Keratins Proteins 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 235000015097 nutrients Nutrition 0.000 description 4
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 238000005903 acid hydrolysis reaction Methods 0.000 description 3
- 238000005336 cracking Methods 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000004471 Glycine Substances 0.000 description 2
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 230000029553 photosynthesis Effects 0.000 description 2
- 238000010672 photosynthesis Methods 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000036647 reaction Effects 0.000 description 2
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 description 1
- DOBIZWYVJFIYOV-UHFFFAOYSA-N 7-hydroxynaphthalene-1,3-disulfonic acid Chemical compound C1=C(S(O)(=O)=O)C=C(S(O)(=O)=O)C2=CC(O)=CC=C21 DOBIZWYVJFIYOV-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241000272496 Galliformes Species 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 235000004279 alanine Nutrition 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 125000000539 amino acid group Chemical group 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 235000003704 aspartic acid Nutrition 0.000 description 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 description 1
- 238000009933 burial Methods 0.000 description 1
- 229960004424 carbon dioxide Drugs 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 1
- 230000004992 fission Effects 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000013486 operation strategy Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/28—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from natural products
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Fertilizers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Processing Of Solid Wastes (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW102129959A TW201508007A (zh) | 2013-08-22 | 2013-08-22 | 水解胺基酸製法 |
TW102129959 | 2013-08-22 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104419949A CN104419949A (zh) | 2015-03-18 |
CN104419949B true CN104419949B (zh) | 2017-04-26 |
Family
ID=51318451
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310547178.3A Expired - Fee Related CN104419949B (zh) | 2013-08-22 | 2013-11-06 | 水解氨基酸制备方法 |
CN201420087322.XU Expired - Fee Related CN203782246U (zh) | 2013-08-22 | 2014-02-27 | 水解氨基酸的装置 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201420087322.XU Expired - Fee Related CN203782246U (zh) | 2013-08-22 | 2014-02-27 | 水解氨基酸的装置 |
Country Status (5)
Country | Link |
---|---|
US (1) | US20150053570A1 (ko) |
JP (1) | JP2015040345A (ko) |
KR (1) | KR20150022683A (ko) |
CN (2) | CN104419949B (ko) |
TW (1) | TW201508007A (ko) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108101716A (zh) * | 2018-03-02 | 2018-06-01 | 广州惠农农业科技有限公司 | 一种有机肥及其制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0640786A (ja) * | 1992-07-22 | 1994-02-15 | Tatsumi Chikura | アミノ酸含有肥料およびその製造方法 |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS51115280A (en) * | 1975-04-03 | 1976-10-09 | Shigeo Otake | Process for treating waste liquid from paste-foods production |
JPS602393B2 (ja) * | 1981-09-25 | 1985-01-21 | 株式会社ユアサコーポレーション | アミノ酸の製造法 |
US4386110A (en) * | 1982-01-08 | 1983-05-31 | Hiroshima Prefecture | Electrical treatment method of soybean protein |
US4551274A (en) * | 1983-08-22 | 1985-11-05 | Ralston Purina Company | Electrolytic treatment of vegetable protein |
BE904225A (fr) * | 1985-02-14 | 1986-05-29 | Fuji Oil Co Ltd | Procede de fractionnement de proteines. |
DE3712825A1 (de) * | 1987-04-15 | 1988-11-03 | Diamalt Ag | Gesamteiweiss-abbauprodukt |
JPH01175994A (ja) * | 1987-12-28 | 1989-07-12 | Tosoh Corp | 蛋白質部分分解物の製造法 |
CN1209203C (zh) * | 2002-12-18 | 2005-07-06 | 吕谦 | 一种羽毛粉的加工处理方法 |
CN101476134A (zh) * | 2007-12-31 | 2009-07-08 | 宁波海硕生物科技有限公司 | 复合银板改性阴极电解生产l-半胱氨酸盐酸盐一水物 |
CN101372503B (zh) * | 2008-08-06 | 2011-06-15 | 西北师范大学 | 从羽毛中提取角蛋白的方法 |
CN101575749B (zh) * | 2009-04-03 | 2010-12-08 | 东华大学 | 一种角蛋白晶须增强的同质复合纤维及其制备方法 |
TW201111393A (en) * | 2009-09-18 | 2011-04-01 | Univ Nat Taiwan | Electrolysis for protein modification |
CN101724376B (zh) * | 2009-12-14 | 2011-07-27 | 东北林业大学 | 利用强碱性降解大豆蛋白制备的木材胶黏剂及其制备方法 |
CN101979428B (zh) * | 2010-10-09 | 2012-09-19 | 天津工业大学 | 一种动物毛发溶解剂及角蛋白溶液的制备方法和用途 |
CN102416196A (zh) * | 2011-02-14 | 2012-04-18 | 蒙一纯 | 一种生物医学工程用角蛋白材料的制备方法 |
CN102370044A (zh) * | 2011-09-30 | 2012-03-14 | 哈尔滨工业大学 | 高蛋白质消化效率的大米蛋白的提取方法 |
CN102517600B (zh) * | 2011-12-07 | 2014-08-13 | 四川大学 | 一种带毛动物皮或毛的电降解方法 |
CN102719933B (zh) * | 2012-07-11 | 2014-12-17 | 成都起点投资有限公司 | 一种羽毛蛋白纤维制备方法 |
CN102775489A (zh) * | 2012-07-31 | 2012-11-14 | 上海全宇生物科技遂平有限公司 | 一种角蛋白质固体及其制备方法 |
-
2013
- 2013-08-22 TW TW102129959A patent/TW201508007A/zh not_active IP Right Cessation
- 2013-11-06 CN CN201310547178.3A patent/CN104419949B/zh not_active Expired - Fee Related
-
2014
- 2014-02-27 CN CN201420087322.XU patent/CN203782246U/zh not_active Expired - Fee Related
- 2014-03-30 US US14/229,987 patent/US20150053570A1/en not_active Abandoned
- 2014-08-18 KR KR20140107032A patent/KR20150022683A/ko not_active Application Discontinuation
- 2014-08-20 JP JP2014167033A patent/JP2015040345A/ja active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0640786A (ja) * | 1992-07-22 | 1994-02-15 | Tatsumi Chikura | アミノ酸含有肥料およびその製造方法 |
Non-Patent Citations (2)
Title |
---|
"Production of Feather Protein Concentrate from Feathers by In vitro Enzymatic Treatment, its Biochemical Characterization and Antioxidant Nature;D.J. M 1 ukesh Kumar et al.;《Middle-East Journal of Scientific Research》;20121231;第11卷(第7期);881-886 * |
碱法水解羽毛蛋白的工艺条件研究;尹国强等;《食品科学》;20050915;第26卷(第09期);全文 * |
Also Published As
Publication number | Publication date |
---|---|
KR20150022683A (ko) | 2015-03-04 |
CN203782246U (zh) | 2014-08-20 |
TW201508007A (zh) | 2015-03-01 |
TWI482780B (ko) | 2015-05-01 |
CN104419949A (zh) | 2015-03-18 |
JP2015040345A (ja) | 2015-03-02 |
US20150053570A1 (en) | 2015-02-26 |
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