CN104419249B - 一种环保型黑色刮开油墨的制备方法 - Google Patents
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Abstract
本发明涉及一种环保型黑色刮开油墨的制备方法，按质量百分比由以下组分组成：丙烯酸树脂5％～10％、氯醋树脂5％～15％、碳黑颜料26％～40％、气相二氧化硅8％～16％、助剂2％～8％、溶剂25％～45％；本发明制得的环保型黑色刮开油墨在贮存时不沉淀，遮盖力好、光泽高；不糊版、不粘版，粘性适中，流动流平性好，印刷性能优良；有很好的耐热性、耐磨性、稳定性、耐折度，使印制的成品在运输、销售中不易破损、划伤；且无毒、无异味，是真正的环保健康型刮开油墨；广泛应用于各种类型的彩票、奖券、票据、电话充值卡，游戏点卡、上网卡、抽奖卡、学习卡、电码防伪标识卡、速显册及儿童刮画等印刷。
Description
技术领域
本发明属于印刷包装材料技术领域，涉及一种环保型黑色刮开油墨，本发明还涉及该种黑色刮开油墨的制备方法。
背景技术
随着市场经济的发展和人们物质文化生活水平的提高，各种类型的彩票、奖券、票据等大量出现，印制彩票、奖券、票据时的油墨也在不断增长，其中刮开油墨的用量也越来越大，除彩票、奖券、票据外，在电信、IT、商业和教育等行业也越来越广泛，如电信行业的电话充值卡，游戏点卡、上网卡、抽奖卡、学习卡、电码防伪标识卡、速显册及儿童刮画等领域。
目前市面上刮开油墨存在耐磨性、耐折度较差，光泽、遮盖力低或刮开时油墨去不尽；还有的在制造刮开油墨时所选树脂的要求要用芳烃类或酮类溶剂，油墨干后仍残留有害的芳烃类或酮类溶剂，对人体和环境必然造成严重的危害，因此开发一种环保型刮开油墨尤其必要。
发明内容
为了解决上面所述的技术问题，本发明采取以下技术方案：本发明涉及一种环保型银色刮开油墨，按质量百分比由以下组分组成：丙烯酸树脂5％～10％、氯醋树脂5％～15％、碳黑颜料26％～40％、气相二氧化硅8％～16％、助剂2％～8％、溶剂25％～45％。
其中，丙烯酸树脂选用分子量在5000～10000热塑型丙烯酸树脂。
氯醋树脂选用酯溶型三元氯醋树脂。
碳黑颜料选用卡博特的Mongul-L、REGAL400R、Monarch1300或Monarch900，德固萨的Special biack4、Special biack6、Special biack550、FW18、FW285或FW200，三菱化学的MA7、MA100或＃40，哥伦比亚化学的Raven3500、Raven1255或Raven3600以及其它中高色素碳黑。
助剂至少包括润湿分散剂、流平剂、微细蜡浆的一种或其组合。
溶剂选取用醋酸丁酯、醋酸乙酯、PMA、DBE、乙二醇丁醚、丙二醇丁醚、脱芳D40溶剂的一种或其组合。
本发明提出一种环保型黑色刮开油墨的制备方法，其制备工艺如下：按配方重量比计，把部分溶剂加入分散釜中，加入丙烯酸树脂、氯醋树脂溶解均匀，加入润湿分散剂、气相二氧化硅、碳黑颜料，高速分散30～40min，移到三棍碾磨机碾磨至细度≤20μm，在调缸中低速搅拌下加入蜡浆、流平剂和剩余的溶剂，搅拌调节好粘度，过滤包装即制得一种环保型黑色刮开油墨。
本发明制得的环保型黑色刮开油墨在贮存时不沉淀，遮盖力、光泽高；不糊版、不粘版，粘性适中，流动流平性好，印刷性能优良；有很好的耐热性、耐磨性、稳定性、耐折度，使印制的成品在运输、销售中不易破损、划伤；且无毒、无异味，是真正的环保健康型刮开油墨。广泛应用于各种类型的彩票、奖券、票据、电话充值卡，游戏点卡、上网卡、抽奖卡、学习卡、电码防伪标识卡、速显册及儿童刮画等印刷。
具体实施方式
按照表1的组分配方准备材料实施。
表1：三个实施例组分配方 质量份
实施例1：
按照表1中实例1按配方重量比把混合溶剂20份加入分散釜中，加入丙烯酸树脂7份、氯醋树脂9份溶解均匀，加入润湿分散剂2.5份、气相二氧化硅12份、碳黑粉32份，高速分散30～40min，移到三棍碾磨机碾磨至细度≤20μm，在调缸中低速搅拌下加入细蜡浆5.5份、流平剂0.5份和剩余的溶剂11.5份，搅拌调节好粘度，过滤包装即制得一种环保型黑色刮开油墨。
实施例2，实施例3制备步骤参照实施例1。
按照国家相关标准，对本发明的环保型黑色刮开油墨的性能进行检测，测试结果如表2所示。
表2环保型黑色刮开油墨性能测试结果
| 测试项目 | 标准要求 | 测试结果 |
| 外观 | 黑色 | 黑色 |
| 细度μm | ≤30 | 20 |
| 表干mm/min | 11～13 | 12 |
| 实干min/100mm | 15～20 | 18 |
| 透光点cm2， | ≤10 | 3 |
| 刮开度g | 8～11 | 10 |
| 在室温水中浸泡48h | 刮开度基本不变 | 合格 |
| 在50℃，湿度90％放置48h | 刮开度基本不变 | 合格 |
| 在-20℃放置48h | 刮开度基本不变 | 合格 |
| 芳烃含量mg·kg-1 | ≤0.1 | 0.03 |
| 游离甲醛mg·kg-1 | ≤0.1 | 0.01 |
| 可溶性铅mg·kg-1 | ≤90 | ≤12 |
| 可溶性镉mg·kg-1 | ≤75 | 未检出 |
| 可溶性铬mg·kg-1 | ≤60 | ≤10 |
| 可溶性汞mg·kg-1 | ≤60 | 未检出 |
尽管本发明已作了详细说明并引证了实施例，但对于本领域的普通技术人员，显然可以按照上述说明而做出的各种方案、修改和改动，都应该包括在权利要求的范围之内。
Claims (4)
1.一种环保型黑色刮开油墨，其特征在于：以质量百分比计，包括如下组分：丙烯酸树脂5％～10％、酯溶型三元氯醋树脂5％～15％、碳黑颜料26％～40％、气相二氧化硅8％～16％、其它助剂2％～8％、溶剂25％～45％；
其中，所述的丙烯酸树脂为分子量在5000～10000热塑型丙烯酸树脂；所述的其它助剂至少包括润湿分散剂、流平剂、微细蜡浆的一种或几种的组合。
2.如权利要求1所述的一种环保型黑色刮开油墨，其特征在于：所述的碳黑颜料为卡博特的Mongul-L、REGAL400R、Monarch1300或Monarch900，德固萨的Special biack 4、Special biack 6、Special biack 550、FW18、FW285或FW200，三菱化学的MA7、MA100或#40，哥伦比亚化学的Raven3500、Raven1255或Raven3600的任一种。
3.如权利要求1所述的一种环保型黑色刮开油墨，其特征在于：所述的溶剂选为醋酸丁酯、醋酸乙酯、PMA、DBE、乙二醇丁醚、丙二醇丁醚、脱芳D40溶剂的一种或几种的组合。
4.一种如权利要求1所述的一种环保型黑色刮开油墨的制备方法，其特征在于：所述的制备方法，其制备工艺如下：按配方重量比计，把部分溶剂加入分散釜中，加入丙烯酸树脂、酯溶型三元氯醋树脂溶解均匀，加入润湿分散剂、气相二氧化硅、碳黑颜料，高速分散30～40min，移到三辊碾磨机碾磨至细度≤20μm，在调缸中低速搅拌下加入微细蜡浆、流平剂和剩余的溶剂，搅拌调节好粘度，过滤包装即制得一种环保型黑色刮开油墨。
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