CN104418609A - Splash-ink ringing glaze - Google Patents
Splash-ink ringing glaze Download PDFInfo
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- CN104418609A CN104418609A CN201310360971.2A CN201310360971A CN104418609A CN 104418609 A CN104418609 A CN 104418609A CN 201310360971 A CN201310360971 A CN 201310360971A CN 104418609 A CN104418609 A CN 104418609A
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- glaze
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- scribbling sketch
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Abstract
The present invention relates to a splash-ink ringing glaze and a splash-ink ringing glaze firing method. According to the present invention, raw materials having the specific composition and comprising glass powder, zinc oxide, quartz powder, talc powder, alumina and basic copper carbonate according to the specific weight ratio are adopted and blended into a glaze slurry with water, the glaze slurry is coated on the surface of the porcelain clay being subjected to biscuit firing, high temperature firing is performed by using oxidizing flame, and heating and thermal insulation are performed so as to fire the porcelain product with the splash-ink ringing glaze, wherein the obtained glaze has characteristics of excellent quality and beautiful appearance.
Description
Technical field
The present invention relates to porcelain technique glaze, be specifically related to glaze formula and the method for cooking thereof of enamel.
Background technology
Porcelain is that the mixture that formed by clay, feldspar, quartz etc. is through goods that are shaping, that fire.In order to give the outward appearance of porcelain grace, usually glaze china.
Glaze covers colourless or coloured glassiness thin layer on ceramic products surface or the mixolimnion of vitreum and crystal, be made by glaze basic components and water, colorant etc. there is high strength and full-bodied material.Glaze is attached to ceramic products surface, can improve ceramic products performance, if the physical strength of increase ceramic products, thermostability and dielectric strength etc.
The kind of glaze is a lot, divides, can be divided into enamel, bristol glaze and flint device glaze etc. by base substrate class; High melting glaze, low temperature glaze can be divided into by firing temperature; Transparent, opaque glaze, coloured glaze can be divided into by barment tag, have light glaze, matt glaze, crack glaze (hacking), crystalline glaze etc.; Lime glaze, feldspar glaze, lead glaze, leadless glaze, boron glaze, lead borate glaze etc. can be divided into by glaze composition.
Industrial art ceramic products is the traditional arts and crafts of China, and along with the development of Technology in modern times, fine arts porcelain obtains tremendous expansion.
Summary of the invention
In order to develop the dizzy trace industrial art ceramic products of scribbling sketch, present inventor has performed and study with keen determination, found that: by using the glass powder with specific composition of specified weight proportioning, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather, glaze slurries are modulated into through water, be coated on the china clay surface of biscuiting, use oxydizing flame high-temperature firing, and heating, temperature keeping, the ceramic products obtaining there is the dizzy trace glaze of scribbling sketch can be fired, thus complete the present invention.
The object of the present invention is to provide following aspect:
First aspect, the invention provides the dizzy trace glaze of a kind of scribbling sketch, is made up of the composition of following weight proportion:
Wherein, glass powder is made up of the component of following weight proportion:
Second aspect, the invention provides the dizzy trace glaze of scribbling sketch as above, is made up of the composition of following weight proportion:
The third aspect, the invention provides the dizzy trace glaze of scribbling sketch as above, is made up of the composition of following weight proportion:
Fourth aspect, the invention provides the dizzy trace glaze of scribbling sketch as above, wherein, glass powder is made up of the component of following weight proportion:
5th aspect, the invention provides the dizzy trace glaze of scribbling sketch, it is fired by the glaze in above-mentioned first aspect to fourth aspect described in any aspect and forms.
6th aspect, the invention provides the method for cooking of the dizzy trace glaze of scribbling sketch, it is fired by above-mentioned glaze and forms, and the method comprises the following steps:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, when temperature is increased to 1285-1295 DEG C, start cooling, temperature is incubated when being down to 1110-1130 DEG C, close flame, when kiln temperature is down to room temperature, take out the ceramic products fired.
7th aspect, the invention provides above-mentioned scribbling sketch to swoon the method for cooking of trace glaze, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather, the 80-120 weight part that adds water stirs.
Eighth aspect, the invention provides above-mentioned scribbling sketch to swoon the method for cooking of trace glaze, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather, 100 weight parts that add water stir.
9th aspect, the invention provides above-mentioned scribbling sketch and to swoon the method for cooking of trace glaze, wherein, in step (1), be milled to particle diameter 200 order with ball mill.
Tenth aspect, the invention provides above-mentioned scribbling sketch and to swoon the method for cooking of trace glaze, wherein, in step (3), start cooling when temperature is increased to 1290 DEG C, insulation when temperature is down to 1120 DEG C.
Scribbling sketch provided by the invention is adopted to swoon trace glaze, through method for cooking provided by the invention, the scribbling sketch with aesthetic appearance can be burnt out to swoon trace glaze, background glaze paint is smoothly opaque, distribute in green mass-tone a large amount of black splotch in irregular shape, black splotch density high part green is denseer, background is formed with the irregular fan-shaped or circular decorative pattern of the pin bunch sample radially expanded from decorative pattern center, radial decorative pattern has feather sample texture, present greyish-green, there is faint metalluster, and have faint concavo-convex fluctuating texture, decorative pattern outline is the profile haloing be made up of multi-level profile haloing band with one fixed width, outermost layer profile haloing band color is the darkest, middle profile haloing band color is the most shallow, in pink colour, the profile haloing band of internal layer is in green, towards decorative pattern central side, there is needle prick shape minute protrusions, decorative pattern is shown one's talent from background, have more visual impact.
Accompanying drawing explanation
Fig. 1 illustrates the picture of gained ceramic products part glaze in embodiment 1.
Embodiment
Below by embodiment, the present invention is described in detail, and the features and advantages of the invention will illustrate along with these and become more clear, clear and definite.
glaze
The invention provides the dizzy trace glaze of scribbling sketch, its glass powder by specified weight proportioning, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather are formulated, wherein glass powder has specific composition, gained glaze can burn out and has aesthetic look, enamel that color and luster is gentle, very attractive in appearance, and the even cunning of enamel, glaze paint glossiness is suitable for, flawless, excellent quality.
Wherein, the glass powder with specific composition plays the effect regulating glaze mobility, elasticity and stability, and can reduce the fusing point of glaze, when its content is at 42-47 weight part, gained enamel has smooth glaze paint, and enamel is even, does not have the bad phenomenon such as crackle and chip.If glass powder consumption is lower than 42 weight parts, cause mobility and the stability deficiency of gained glaze because its consumption is too low, the quality of glaze declines, otherwise, if the consumption of glass powder is higher than 47 weight parts, cause the fusing point of glaze too low because its consumption is too high, mobility is too high, and the quality of glaze may deterioration.
In a preferred embodiment, the consumption of glass powder is 44-46 weight part, particularly preferably 45 weight parts, and now the quality of glaze is best, and glaze paint is smooth especially, and glossiness is suitable for, and enamel is even.
In the present invention, in order to make gained enamel have superior quality, the composition of glass powder used has specific restriction.The present inventor finds through large quantity research, when glass powder has the component composition of following weight proportion, can guarantee that gained enamel has the superior quality of expectation:
In one preferred embodiment, glass powder has the component composition of following weight proportion:
For above-mentioned glass powder, can be fired by conventional glass sintering technology, then pulverize.This is in the limit of power of those skilled in the art, and therefore not to repeat here.
Swoon in trace glaze in scribbling sketch provided by the invention, on the one hand, zinc oxide is used as fusing assistant, there is excellent fluxing action, transparency and the luminance brightness of glaze can be adjusted, improve gloss and the whiteness of glaze paint, reduce the coefficient of expansion of glaze, improve the thermostability of product, improve elasticity and the tension stress deformability of glaze, and the brilliance of glaze colours can be increased while expanding fusion range, promote to form light decorative pattern, on the other hand, zinc oxide is used as crystallizing agent, molten glaze chilling but time, zinc oxide crystallization forms crystal seed, thus drive crystallization, form larger crystal decorative pattern, give the dizzy trace sample decorative pattern radially expanded of glaze beauty.
Swoon in trace glaze in scribbling sketch provided by the invention, the consumption of zinc oxide is 24-28 weight, and when its consumption is within the scope of this, gained glaze not only has excellent quality, and has decorative pattern and the color and luster of expectation.When use quantity not sufficient 24 weight part of zinc oxide, because it uses quantity not sufficient, effect of fluxing reduces, and the quality of gained glaze declines, and, cause crystallization difficulty because its consumption is too low, be difficult to the dizzy trace sample decorative pattern radially expanded forming expectation.Otherwise if the consumption of zinc oxide is higher than 28 weight parts, be difficult to control for the too high crystallization that causes of its consumption, the quality of gained glaze and outward appearance are not good.
In one preferred embodiment, the consumption of zinc oxide is 24-26 weight, particularly preferably 25 weight parts, the now excellent quality of gained glaze, and attractive appearance.
Swoon in trace glaze in scribbling sketch provided by the invention, silica powder can increase glaze fusing point, widen melting temperature range, itself and glass powder combine the fusing point for regulating glaze, on the other hand, silica powder can improve the viscosity of glaze, reduce the mobility of glaze, reduce thermal expansivity, improve the mechanical property of glaze, as increased the hardness of glaze paint and wear resistance etc., improve stability and the steadiness of glaze.
Swoon in trace glaze in scribbling sketch provided by the invention, the consumption of silica powder is 24-28 weight part.When its consumption is within the scope of this, glaze has suitable melt temperature scope, and gained glaze has good quality, stability and steadiness excellence.If silica powder consumption is lower than 24 weight parts, because it can cause the melt temperature of glaze too low by quantity not sufficient, the quality badness of gained glaze, stability and steadiness deficiency.Otherwise if the consumption of silica powder is higher than 28 weight parts, cause the melt temperature of glaze too high because its consumption is too high, fire difficulty, energy consumption is high, and too high firing temperature can cause quality and the appearance degradation of glaze.
In one preferred embodiment, the consumption of silica powder is 24-26 weight, particularly preferably 25 weight parts, the now excellent quality of gained glaze, stability and steadiness good.
Swoon in trace glaze in scribbling sketch provided by the invention, talcum powder can improve the elasticity of glaze, promote that middle layer is formed, reduce the fracture prone of glaze, promote that enamel is even, and talcum powder has and regulates the glossiness of glaze paint, contribute to being formed the glaze paint with certain matte effect, give prominence to scribbles sketch swoons the gloss of trace sample decorative pattern and attractive in appearance.
Swoon in trace glaze in scribbling sketch provided by the invention, talcous consumption is 3-5 weight part.When its consumption is within the scope of this, gained glaze decorative pattern is that full moist scribbling sketch is swooned trace sample decorative pattern.If when talcous consumption is lower than 3 weight part, cause the quality of glaze to reduce because its consumption is too low, decorative pattern is imperfect or have and break.Otherwise if talcous consumption is higher than 5 weight parts, glaze paint glossiness is too low, appearance degradation.
In one preferred embodiment, talcous consumption is 3.5-4.5 weight, particularly preferably 4 weight parts, and the now scribbling sketch of gained glaze is swooned, and trace sample decorative pattern is full moistens, and lines is attractive in appearance, and glossiness is suitable for.
Swoon in trace glaze in scribbling sketch provided by the invention, aluminum oxide is for adjusting the stability of glaze, improve chemical stability and physical strength, improve thermostability, on the other hand, aluminum oxide, for regulating crystallization color, makes the crystallization color greening of the ventilation breather as toner even dark green, thus has scribbling sketch effect.
Swoon in trace glaze in scribbling sketch provided by the invention, the consumption of aluminum oxide is 0.8-1.2 weight part.When its consumption is within the scope of this, gained glaze has excellent quality and outward appearance, and stability is high, and color and luster is good.If the consumption of aluminum oxide is lower than 0.8 weight part, for the too low stability deterioration causing gained glaze of its consumption, color and luster is not good.Otherwise, if the consumption of aluminum oxide is higher than 1.2 weight parts, high for the too high melt temperature of glaze that causes of its consumption, increase and fire difficulty, and the glossiness of gained glaze reduces.
In one particularly preferably embodiment, the consumption of aluminum oxide is 1 weight part, and now glaze has good quality and outward appearance, and stability is high, and scribbling sketch color and luster is dense thick.
Swoon in trace glaze in scribbling sketch provided by the invention, glass powder, zinc oxide, silica powder, talcum powder be basis of formation glaze together with aluminum oxide, based on glaze composition, regulate the melt temperature of glaze, meltbility, fluxibility, stability, mobility, viscosity etc. respectively, make gained glaze have the hardness of expectation, gloss, brightness and decorative pattern etc.
Swoon in trace glaze in scribbling sketch provided by the invention, ventilation breather, as toner, regulates background glaze colours and decorative pattern glaze colours.
Swoon in trace glaze in scribbling sketch provided by the invention, the consumption of ventilation breather is 3-5 weight part.When its consumption is within the scope of this, can form green is main background colour, and light gray is main decorative pattern glaze colours.When the consumption of ventilation breather is lower than 3 weight part, background glaze colours and decorative pattern glaze colours all excessively shallow, otherwise when the consumption of ventilation breather is higher than 5 weight part, glaze paint is easily cracked.
In a preferred embodiment, the consumption of ventilation breather is 3.5-4.5 weight part, more preferably 4 weight parts, and now glaze has beautiful outward appearance, bright in colour, and scribbling sketch color and luster is dense thick.
Swoon in trace glaze in scribbling sketch provided by the invention, glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather all adopt powder.Granularity for each powder does not specially require, but preferable particle size is lower than 200 orders.
method for cooking
The invention provides the method for cooking spilling golden peacock blue glaze, comprising:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, when temperature is increased to 1285-1295 DEG C, start cooling, temperature is incubated when being down to 1110-1130 DEG C, close flame, when kiln temperature is down to room temperature, take out the ceramic products fired.
By aforesaid method, can burn out the scribbling sketch with aesthetic appearance and to swoon trace glaze ceramic products, its scribbling sketch color and luster is dense thick, and circular decorative pattern is full moist, has high ornamental value and reserve value.
embodiment
Further describe the present invention below by way of exemplary example, but these examples are only illustrative, do not form any restriction to scope of the present invention.
Firing of the embodiment 1 dizzy trace glaze of scribbling sketch
Take following composition:
Wherein, glass powder, purchased from Beijing traditional Chinese medicines chemical reagent company limited, has following composition:
Above-mentioned weight part is based on 100 parts by weight of glass powder gross weights.
By glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather mix, add 1OOml water, stir, with ball mill ball grinding stirring 2 hours, obtain liquid glaze slurries, by the china clay unpainted clay idol surface of its uniform application in biscuiting, enter kiln oxydizing flame after drying to fire, cooling is started when burning 1290 DEG C, temperature is incubated 2 hours when being down to 1120 DEG C, fire complete, close oxydizing flame, naturally decline Deng kiln temperature, after about 20 hours, when dropping to room temperature Deng kiln temperature, open kiln and take out ceramic products, its surface is with the dizzy trace glaze of scribbling sketch.
Firing of the embodiment 2 dizzy trace glaze of scribbling sketch
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Firing of the embodiment 3 dizzy trace glaze of scribbling sketch
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Firing of the embodiment 4 dizzy trace glaze of scribbling sketch
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Firing of the embodiment 5 dizzy trace glaze of scribbling sketch
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Comparative example 1
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Comparative example 2
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, raw materials used as follows:
Comparative example 3
Fire the dizzy trace glaze ceramic products of scribbling sketch in the same manner as example 1, its difference is only, glass powder has following composition:
Above-mentioned weight part is based on 100 parts by weight of glass powder gross weights
More than joint embodiment and exemplary example are to invention has been detailed description, but these explanations can not be interpreted as limitation of the present invention.It will be appreciated by those skilled in the art that when not departing from spirit and scope of the invention, can carry out multiple equivalencing, modification or improvement to technical solution of the present invention and embodiment thereof, these all fall within the scope of the present invention.Protection scope of the present invention is as the criterion with claims.
Claims (10)
1. the dizzy trace glaze of scribbling sketch, be made up of the composition of following weight proportion:
Wherein, glass powder is made up of the component of following weight proportion:
2. the dizzy trace glaze of scribbling sketch as claimed in claim 1, be made up of the composition of following weight proportion:
3. the dizzy trace glaze of scribbling sketch as claimed in claim 1, be made up of the composition of following weight proportion:
4. the dizzy trace glaze of scribbling sketch as claimed in claim 1, wherein, glass powder is made up of the component of following weight proportion:
5. the dizzy trace glaze of scribbling sketch, the trace glaze of swooning of the scribbling sketch according to any one of claim 1-4 is fired and is formed.
6. the method for cooking of the dizzy trace glaze of scribbling sketch, it is fired by above-mentioned glaze and forms, and the method comprises the following steps:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, start cooling when temperature is increased to 1285-1295 DEG C, insulation when temperature is down to 1110-1130 DEG C, closes flame, when kiln temperature is down to room temperature, takes out the ceramic products fired.
7. the method for cooking of the dizzy trace glaze of scribbling sketch as claimed in claim 6, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather, the 80-120 weight part that adds water stirs.
8. the method for cooking of the dizzy trace glaze of scribbling sketch as claimed in claim 6, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, talcum powder, aluminum oxide and ventilation breather, 100 weight parts that add water stir.
9. the method for cooking of the dizzy trace glaze of scribbling sketch as claimed in claim 6, wherein, in step (1), is milled to below particle diameter 200 order with ball mill.
10. the method for cooking of the dizzy trace glaze of scribbling sketch as claimed in claim 6, wherein, in step (3), starts cooling when temperature is increased to 1290 DEG C, is incubated when temperature is down to 1120 DEG C.
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| CN201310360971.2A CN104418609B (en) | 2013-08-19 | 2013-08-19 | The dizzy trace glaze of scribbling sketch |
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| CN201310360971.2A CN104418609B (en) | 2013-08-19 | 2013-08-19 | The dizzy trace glaze of scribbling sketch |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107162422A (en) * | 2017-07-11 | 2017-09-15 | 德化县万盛陶瓷有限公司 | A kind of fire-resistant oxidation resistant ceramic glaze and preparation method thereof |
| CN109111118A (en) * | 2018-10-25 | 2019-01-01 | 中山市大盛文化传播有限公司 | ceramic glaze and porcelain |
| CN114656153A (en) * | 2022-01-14 | 2022-06-24 | 格力电器（武汉）有限公司 | Glass powder preparation method, glaze slip preparation method and enamel product |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101264715A (en) * | 2008-02-01 | 2008-09-17 | 杜金树 | Method for manufacturing porcelain imitation artwork |
| CN102515708A (en) * | 2011-12-14 | 2012-06-27 | 李学武 | Method for fabricating blue-and-white peony porcelain |
| CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
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2013
- 2013-08-19 CN CN201310360971.2A patent/CN104418609B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101264715A (en) * | 2008-02-01 | 2008-09-17 | 杜金树 | Method for manufacturing porcelain imitation artwork |
| CN102515708A (en) * | 2011-12-14 | 2012-06-27 | 李学武 | Method for fabricating blue-and-white peony porcelain |
| CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107162422A (en) * | 2017-07-11 | 2017-09-15 | 德化县万盛陶瓷有限公司 | A kind of fire-resistant oxidation resistant ceramic glaze and preparation method thereof |
| CN109111118A (en) * | 2018-10-25 | 2019-01-01 | 中山市大盛文化传播有限公司 | ceramic glaze and porcelain |
| CN114656153A (en) * | 2022-01-14 | 2022-06-24 | 格力电器（武汉）有限公司 | Glass powder preparation method, glaze slip preparation method and enamel product |
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| CN104418609B (en) | 2016-01-06 |
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