CN104418610B - Spill golden peacock blue glaze - Google Patents
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- CN104418610B CN104418610B CN201310361888.7A CN201310361888A CN104418610B CN 104418610 B CN104418610 B CN 104418610B CN 201310361888 A CN201310361888 A CN 201310361888A CN 104418610 B CN104418610 B CN 104418610B
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Abstract
The present invention relates to the method for cooking spilling golden peacock blue glaze and spill golden peacock blue glaze.By using the glass powder with specific composition of specified weight proportioning, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, glaze slurries are modulated into through water, be coated on the china clay surface of biscuiting, use oxydizing flame high-temperature firing, and heating, temperature keeping, the ceramic obtaining having and spill golden peacock blue glaze can be fired.The excellent quality of gained glaze, beautiful appearance, has gorgeous bright green rust, and decorative pattern is full moist, spills gold point and sews beautiful.
Description
Technical field
The present invention relates to ceramic process glaze, be specifically related to glaze formula and the method for cooking thereof of ceramic glaze.
Background technology
Pottery is that the mixture that formed by clay, feldspar, quartz etc. is through goods that are shaping, that fire.In order to give pottery graceful outward appearance, usually give ceramic glazing.
Glaze covers colourless or coloured glassiness thin layer on ceramic surface or the mixolimnion of vitreum and crystal, be made by glaze basic components and water, colorant etc. there is high strength and full-bodied material.Glaze is attached to ceramic surface, can improve ceramic performance, if the physical strength of increase ceramic, thermostability and dielectric strength etc.
The kind of glaze is a lot, divides, can be divided into enamel, bristol glaze and flint device glaze etc. by base substrate class; High melting glaze, low temperature glaze can be divided into by firing temperature; Transparent, opaque glaze, coloured glaze can be divided into by barment tag, have light glaze, matt glaze, crack glaze (hacking), crystalline glaze etc.; Lime glaze, feldspar glaze, lead glaze, leadless glaze, boron glaze, lead borate glaze etc. can be divided into by glaze composition.
In coloured glaze, peacock blue glaze is also referred to as peacock green glaze or bright blue, and the medium temperature glaze of to be a kind of with copper be tinting material, obtains this name because of the bright blue of the peacock dodds that is similar in color.
According to making kind, peacock blue glaze can be divided three classes: peacock blue one-glaze ware, peacock blue blue and white, with peacock blue relevant mixed faience.Wherein, peacock blue blue and white be peacock blue with the underglaze blue combination of low temperature, fire at the drawn peacock blue glaze of cobalt material surface coverage low temperature and form.With the combination that peacock blue relevant mixed faience is the low temperature colored glaze such as peacock blue and yellow, brown.
Craft artistic pottery and porcelain goods are traditional artss and crafts of China, and along with the development of Technology in modern times, artistic pottery and porcelain obtains tremendous expansion, but peacock blue glaze handicraft artistic pottery and porcelain is limited to the formula of peacock blue glaze and sintering technology and develops limited.
Summary of the invention
In order to develop peacock blue glaze handicraft decorative ceramic goods, present inventor has performed and study with keen determination, found that: by using the glass powder with specific composition of specified weight proportioning, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, glaze slurries are modulated into through water, be coated on the china clay surface of biscuiting, use oxydizing flame high-temperature firing, and heating, temperature keeping, the ceramic products obtaining having and spill golden peacock blue glaze can be fired, thus complete the present invention.
The object of the present invention is to provide following aspect:
First aspect, the invention provides one and spills golden peacock blue glaze, be made up of the composition of following weight proportion:
Wherein, glass powder is made up of the component of following weight proportion:
Second aspect, the invention provides and spill golden peacock blue glaze as above, be made up of the composition of following weight proportion:
The third aspect, the invention provides and spill golden peacock blue glaze as above, be made up of the composition of following weight proportion:
Fourth aspect, the invention provides and spill golden peacock blue glaze as above, and wherein, glass powder is made up of the component of following weight proportion:
5th aspect, the invention provides and spill golden peacock blue glaze, and it is fired by the glaze in above-mentioned first aspect to fourth aspect described in any aspect and forms.
6th aspect, the invention provides the method for cooking spilling golden peacock blue glaze, and it is fired by above-mentioned glaze and forms, and the method comprises the following steps:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, when temperature is increased to 1290-1300 DEG C, start cooling, temperature is incubated when being down to 1070-1090 DEG C, close flame, when kiln temperature is down to room temperature, take out the ceramic products fired.
7th aspect, the invention provides the above-mentioned method for cooking spilling golden peacock blue glaze, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, the 80-120 weight part that adds water stirs.
Eighth aspect, the invention provides the above-mentioned method for cooking spilling golden peacock blue glaze, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, 100 weight parts that add water stir.
9th aspect, the invention provides the above-mentioned method for cooking spilling golden peacock blue glaze, wherein, in step (1), is milled to below particle diameter 200 order with ball mill.
Tenth aspect, the invention provides the above-mentioned method for cooking spilling golden peacock blue glaze, wherein, in step (3), starts cooling when temperature is increased to 1297 DEG C, is incubated when temperature is down to 1080 DEG C.
Adopt and provided by the inventionly spill golden peacock blue glaze, through method for cooking provided by the invention, can burn out there is aesthetic appearance spill golden peacock blue glaze, background displaing yellow, background is spilt golden effect, background is formed with the irregular fan-shaped or circular decorative pattern of the pin bunch sample radially expanded from decorative pattern center, radial decorative pattern has feather sample texture, present beautiful green rust, there is strong metalluster, decorative pattern outline is have the more strong skeletal lines of the metalluster of one fixed width, make the boundary of decorative pattern and background more clearly clear, blue decorative pattern is shown one's talent from yellow background, have more visual impact.
Accompanying drawing explanation
Fig. 1 illustrates the picture of gained ceramic products part glaze in embodiment 1
Fig. 2 illustrates the picture of gained ceramic products part glaze in embodiment 2
Tool stops embodiment
Below by embodiment, the present invention is described in detail, and the features and advantages of the invention will illustrate along with these and become more clear, clear and definite.
glaze
The invention provides and spill golden peacock blue glaze, its glass powder by specified weight proportioning, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide are formulated, wherein glass powder has specific composition, gained glaze can burn out and has aesthetic look, lovely luster and have the ceramic glaze spilling golden effect, very attractive in appearance, and the even cunning of enamel, glaze paint glossiness is high, flawless, excellent quality.
Wherein, the glass powder with specific composition plays the effect regulating glaze mobility, elasticity and stability, and can reduce the fusing point of glaze, when its content is at 45-50 weight part, gained enamel has smooth glaze paint, and enamel is even, does not have the bad phenomenon such as crackle and chip.If glass powder consumption is lower than 45 weight parts, cause mobility and the stability deficiency of gained glaze because its consumption is too low, the quality of glaze declines, otherwise, if the consumption of glass powder is higher than 50 weight parts, cause the fusing point of glaze too low because its consumption is too high, mobility is too high, and the quality of glaze may deterioration.
In a preferred embodiment, the consumption of glass powder is 46-48 weight part, particularly preferably 47 weight parts, and now the quality of glaze is best, and glaze paint is smooth especially, and glossiness is splendid, and enamel is even.
In the present invention, in order to make gained enamel have superior quality, the composition of glass powder used has specific restriction.The present inventor finds through large quantity research, when glass powder has the component composition of following weight proportion, can guarantee that gained enamel has the superior quality of expectation:
In one preferred embodiment, glass powder has the component composition of following weight proportion:
For above-mentioned glass powder, can be fired by conventional glass sintering technology, then pulverize.This is in the limit of power of those skilled in the art, and therefore not to repeat here.
Spill in golden peacock blue glaze provided by the invention, on the one hand, zinc oxide is used as fusing assistant, there is excellent fluxing action, transparency and the luminance brightness of glaze can be increased, improve the gloss of glaze paint and certainly spend, reduce the coefficient of expansion of glaze, improve the thermostability of product, improve elasticity and the tension stress deformability of glaze, and the brilliance of glaze colours can be increased while expanding fusion range, promote to form gorgeous green rust, on the other hand, zinc oxide is used as crystallizing agent, molten glaze chilling but time, zinc oxide crystallization forms crystal seed, thus crystalline substance is prayed in drive, form larger crystal decorative pattern, give the decorative pattern of glaze beauty and spill gold point and sew.
Spill in golden peacock blue glaze provided by the invention, the consumption of zinc oxide is 24-28 weight, and when its consumption is within the scope of this, gained glaze not only has excellent quality, and has the green rust of expectation and the decorative pattern of beauty and spill golden effect.When use quantity not sufficient 24 weight part of zinc oxide, because it uses quantity not sufficient, effect of fluxing reduces, and the quality of gained glaze declines, and, cause crystallization difficulty because its consumption is too low, be difficult to the decorative pattern of formation expectation and spill golden effect.Otherwise if the consumption of zinc oxide is higher than 28 weight parts, cause praying crystalline substance be difficult to control for its consumption is too high, the quality of gained glaze and outward appearance are not good.
In one preferred embodiment, the consumption of zinc oxide is 24-26 weight, particularly preferably 25 weight parts, the now excellent quality of gained glaze, and beautiful appearance.
Spill in golden peacock blue glaze provided by the invention, silica powder can increase glaze fusing point, widen melting temperature range, itself and glass powder combine the fusing point for regulating glaze, on the other hand, silica powder can improve the viscosity of glaze, reduce the mobility of glaze, reduce thermal expansivity, improve the mechanical property of glaze, as increased the hardness of glaze paint and wear resistance etc., improve stability and the steadiness of glaze.
Spill in golden peacock blue glaze provided by the invention, the consumption of silica powder is 24-28 weight part.When its consumption is within the scope of this, glaze has suitable melt temperature scope, and gained glaze has good quality, stability and steadiness excellence.If silica powder consumption is lower than 24 weight parts, because it can cause the melt temperature of glaze too low by quantity not sufficient, the quality badness of gained glaze, stability and steadiness deficiency.Otherwise if the consumption of silica powder is higher than 28 weight parts, cause the melt temperature of glaze too high because its consumption is too high, fire difficulty, energy consumption is high, and too high firing temperature can cause quality and the appearance degradation of glaze.
In one preferred embodiment, the consumption of silica powder is 24-26 weight, particularly preferably 25 weight parts, the now excellent quality of gained glaze, stability and steadiness good.
Spill in golden peacock blue glaze provided by the invention, titanium dioxide is mainly as crystalline catalysts, the crystallization of initiated oxidation zinc, help crystallisation is formed, and regulates crystal form to be partially circular, impels gained glaze have the decorative pattern of expectation and spill gold point and sew, on the other hand, titanium dioxide can improve the refraction of light of glaze and absorb ultraviolet performance, makes glaze have higher Optical Aesthetic, has more sight.
Spill in golden peacock blue glaze provided by the invention, the consumption of titanium dioxide is 1.5-2.5 weight part.When its consumption is within the scope of this, glaze decorative pattern is full partially circular or fan-shaped, with peacock blue color with spill gold point and combine and give glaze with the aesthetic appearance expected.If when the consumption of titanium dioxide is lower than 1.5 weight part, cause the effect of catalysis initiated oxidation zinc crystallization inadequate because its consumption is too low, zinc oxide prays brilliant reduction, and the quality of glaze can be caused to reduce, the deterioration of crystallization decorative pattern.Otherwise if the consumption of titanium dioxide is higher than 2.5 weight parts, the effect of its catalysis initiated oxidation zinc crystallization is excessively strong, zinc oxide is prayed brilliant too high, and the quality of glaze also can be caused to reduce, the deterioration of crystallization decorative pattern.
In one preferred embodiment, the consumption of titanium dioxide is 1.8-2.2 weight, particularly preferably 2 weight parts, and now the circular decorative pattern of gained glaze is full attractive in appearance, and glossiness is high.
Spill in golden peacock blue glaze provided by the invention, aluminum oxide is for adjusting the stability of glaze, improve chemical stability and physical strength, improve thermostability, on the other hand, aluminum oxide, for regulating crystallization color, makes the crystallization yellowish of the nickel sesquioxide as toner, thus has and spill gold point and sew effect.
Spill in golden peacock blue glaze provided by the invention, the consumption of aluminum oxide is 0.8-1.2 weight part.When its consumption is within the scope of this, gained glaze has excellent quality and outward appearance, and stability is high, spills gold point and sews effective.If the consumption of aluminum oxide is lower than 0.8 weight part, causes the stability deterioration of gained glaze because its consumption is too low, spill golden poor effect.Otherwise, if the consumption of aluminum oxide is higher than 12 weight parts, causes the melt temperature of glaze high because its consumption is too high, increase and fire difficulty, and the glossiness of gained glaze reduces.
In one particularly preferably embodiment, the consumption of aluminum oxide is 1 weight part, and now glaze has good quality and outward appearance, and stability is high, spills gold point and sews bright and beautiful.
Spill in golden peacock blue glaze provided by the invention, glass powder, zinc oxide, silica powder, titanium dioxide is basis of formation glaze together with aluminum oxide, based on glaze composition, regulate the melt temperature of glaze, meltbility, fluxibility, stability, mobility, viscosity etc. respectively, make gained glaze have the hardness of expectation, gloss, brightness and decorative pattern etc.
Spill in golden peacock blue glaze provided by the invention, nickel sesquioxide, as toner, can form the background glaze colours of yellow system, and form the beautiful green rust decorative pattern glaze colours with metalluster.
Spill in golden peacock blue glaze provided by the invention, the consumption of nickel sesquioxide is 1.5-2.5 weight part.When its consumption is within the scope of this, can large area figure be formed, and clear-cut between decorative pattern and background, decorative pattern has beautiful green rust.If the consumption of nickel sesquioxide is lower than 15 weight parts, decorative pattern is painted not good, otherwise the consumption as nickel sesquioxide is higher than 25 weight parts, and background glaze and figure glaze color can become heavy.
In a preferred embodiment, the consumption of nickel sesquioxide is 18-22 weight part, more preferably 2 weight parts, and now glaze has beautiful outward appearance, bright in colour, spills gold point and sews bright and beautiful.
Spill in golden peacock blue glaze provided by the invention, glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide all adopt powder.Granularity for each powder does not specially require, but preferable particle size is lower than 200 orders.
method for cooking
The invention provides the method for cooking spilling golden peacock blue glaze, comprising:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, when temperature is increased to 1290-1300 DEG C, start cooling, temperature is incubated when being down to 1070-1090 DEG C, close flame, when kiln temperature is down to room temperature, take out the ceramic products fired.
By aforesaid method, can burn out there is aesthetic appearance spill golden peacock blue glaze ceramic products, it is peacock blue beautiful in colour, and circular decorative pattern is full, spills gold point and sews beautiful, have high ornamental value and reserve value.
Embodiment
Further describe the present invention below by way of exemplary example, but these examples are only illustrative, do not form any restriction to scope of the present invention.
Embodiment 1 spills firing of golden peacock blue glaze
Take following composition:
Wherein, glass powder, purchased from Beijing traditional Chinese medicines chemical reagent company limited, has following composition:
Above-mentioned weight part is based on 100 parts by weight of glass powder gross weights.
By glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide mix, add 100ml water, stir, with ball mill ball grinding stirring 2 hours, obtain liquid glaze slurries, by the china clay unpainted clay idol surface of its uniform application in biscuiting, enter kiln oxydizing flame after drying to fire, cooling is started when burning 1297 DEG C, temperature is incubated 2 hours when being down to 1080 DEG C, fire complete, close oxydizing flame, naturally decline Deng kiln temperature, after about 20 hours, when dropping to room temperature Deng kiln temperature, open kiln and take out ceramic, its surface is with spilling golden peacock blue glaze.
Embodiment 2 spills firing of golden peacock blue glaze
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Embodiment 3 spills firing of golden peacock blue glaze
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Embodiment 4 spills firing of golden peacock blue glaze
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Embodiment 5 spills firing of golden peacock blue glaze
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Comparative example 1
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Comparative example 2
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, raw materials used as follows:
Comparative example 3
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, glass powder has following composition:
Above-mentioned weight part is based on 100 parts by weight of glass powder gross weights.
Comparative example 4
Fire in the same manner as example 1 and spill golden peacock blue glaze ceramic products, its difference is only, starts cooling, be incubated 2 hours when temperature is down to 1110 DEG C when burning 1330 DEG C.
More than joint embodiment and exemplary example are to invention has been detailed description, but these explanations can not be interpreted as limitation of the present invention.It will be appreciated by those skilled in the art that when not departing from spirit and scope of the invention, can carry out multiple equivalencing, modification or improvement to technical solution of the present invention and embodiment thereof, these all fall within the scope of the present invention.Protection scope of the present invention is as the criterion with claims.
Claims (10)
1. spill a golden peacock blue glaze, be made up of the composition of following weight proportion:
Wherein, glass powder is made up of the component of following weight proportion:
2. spill golden peacock blue glaze as claimed in claim 1, be made up of the composition of following weight proportion:
3. spill golden peacock blue glaze as claimed in claim 1, be made up of the composition of following weight proportion:
4. spill golden peacock blue glaze as claimed in claim 1, wherein, glass powder is made up of the component of following weight proportion:
5. spill golden peacock blue glaze, the golden peacock blue glaze that spills according to any one of claim 1-4 is fired and is formed.
6. spill the method for cooking of golden peacock blue glaze, its golden peacock blue glaze that spills according to any one of claim 1-4 is fired and is formed, and the method comprises the following steps:
(1) obtaining liq glaze slurries: glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide are mixed, add water stirring, uses ball mill ball grinding stirring, obtains liquid glaze slurries;
(2) glazing: china clay unpainted clay idol surface liquid glaze slurries being coated equably biscuiting, and dry;
(3) fire: kiln put into by the unpainted clay idol by glazing and after drying, and fires with oxydizing flame, when temperature is increased to 1290-1300 DEG C, start cooling, temperature is incubated when being down to 1070-1090 DEG C, close flame, when kiln temperature is down to room temperature, take out the ceramic fired.
7. spill the method for cooking of golden peacock blue glaze as claimed in claim 6, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, the 80-120 weight part that adds water stirs.
8. spill the method for cooking of golden peacock blue glaze as claimed in claim 6, wherein, in step (1), based on mixture total weight amount 100 weight part of glass powder, zinc oxide, silica powder, titanium dioxide, aluminum oxide and nickel sesquioxide, 100 weight parts that add water stir.
9. spill the method for cooking of golden peacock blue glaze as claimed in claim 6, wherein, in step (1), be milled to below particle diameter 200 order with ball mill.
10. spill the method for cooking of golden peacock blue glaze as claimed in claim 6, wherein, in step (3), when temperature is increased to 1297 DEG C, start cooling, be incubated when temperature is down to 1080 DEG C.
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| CN107311613A (en) * | 2017-07-26 | 2017-11-03 | 贵州省旅游产品研发中心（有限合伙） | A kind of tooth boat pottery underglaze colour manufacture craft |
| CN109081589B (en) * | 2018-08-29 | 2022-03-29 | 江苏高淳陶瓷股份有限公司 | Feather-shaped transmutation glaze and preparation method thereof |
| CN110092581B (en) * | 2019-05-25 | 2020-11-24 | 景德镇陶瓷大学 | Preparation method of blue photon glaze |
| CN110066112B (en) * | 2019-05-25 | 2020-11-24 | 景德镇陶瓷大学 | Preparation method of red photon glaze |
| CN114956560B (en) * | 2022-06-17 | 2023-11-03 | 景德镇欧神诺陶瓷有限公司 | Crystal glaze, preparation method thereof and crystal glaze ceramic product |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1040570A (en) * | 1988-08-19 | 1990-03-21 | 北京市建筑材料科学研究所 | The preparation method of lead-free gluzed enamel |
| CN101973788A (en) * | 2010-10-26 | 2011-02-16 | 陕西科技大学 | Preparation method of phase-separation peacock blue glaze |
| CN102659453A (en) * | 2012-04-01 | 2012-09-12 | 江苏拜富科技有限公司 | Crystal glaze and its preparation method and use method |
-
2013
- 2013-08-19 CN CN201310361888.7A patent/CN104418610B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1040570A (en) * | 1988-08-19 | 1990-03-21 | 北京市建筑材料科学研究所 | The preparation method of lead-free gluzed enamel |
| CN101973788A (en) * | 2010-10-26 | 2011-02-16 | 陕西科技大学 | Preparation method of phase-separation peacock blue glaze |
| CN102659453A (en) * | 2012-04-01 | 2012-09-12 | 江苏拜富科技有限公司 | Crystal glaze and its preparation method and use method |
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