CN104397053B - Preparation method for botanical pesticide for specially killing cabbage caterpillars during organic vegetable planting - Google Patents
Preparation method for botanical pesticide for specially killing cabbage caterpillars during organic vegetable planting Download PDFInfo
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- CN104397053B CN104397053B CN201410753998.2A CN201410753998A CN104397053B CN 104397053 B CN104397053 B CN 104397053B CN 201410753998 A CN201410753998 A CN 201410753998A CN 104397053 B CN104397053 B CN 104397053B
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- 235000013311 vegetables Nutrition 0.000 title claims abstract description 37
- 241000255969 Pieris brassicae Species 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000575 pesticide Substances 0.000 title abstract description 15
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract description 14
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 4
- 238000007789 sealing Methods 0.000 claims abstract 2
- 239000002917 insecticide Substances 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 7
- 239000012141 concentrate Substances 0.000 claims description 4
- 241000907661 Pieris rapae Species 0.000 abstract description 12
- 241000196324 Embryophyta Species 0.000 abstract description 10
- 239000003814 drug Substances 0.000 abstract description 8
- 240000000233 Melia azedarach Species 0.000 abstract description 6
- 206010059866 Drug resistance Diseases 0.000 abstract description 2
- 241000545405 Tripterygium Species 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract description 2
- 230000000857 drug effect Effects 0.000 abstract description 2
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- 241000173529 Aconitum napellus Species 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 229930182470 glycoside Natural products 0.000 abstract 1
- 150000002338 glycosides Chemical class 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 9
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- ZSBXGIUJOOQZMP-JLNYLFASSA-N Matrine Chemical compound C1CC[C@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-JLNYLFASSA-N 0.000 description 5
- 230000000749 insecticidal effect Effects 0.000 description 5
- 229930014456 matrine Natural products 0.000 description 5
- 239000000047 product Substances 0.000 description 5
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- 231100000614 poison Toxicity 0.000 description 4
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- 238000012360 testing method Methods 0.000 description 4
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- 235000013399 edible fruits Nutrition 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
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- 239000008488 toosendanin Substances 0.000 description 3
- CULUKMPMGVXCEI-NXEZZACHSA-N (-)-N-Methylcytisine Natural products C12=CC=CC(=O)N2C[C@H]2CN(C)C[C@H]1C2 CULUKMPMGVXCEI-NXEZZACHSA-N 0.000 description 2
- XVPBINOPNYFXID-JARXUMMXSA-N 85u4c366qs Chemical compound C([C@@H]1CCC[N@+]2(CCC[C@H]3[C@@H]21)[O-])N1[C@@H]3CCCC1=O XVPBINOPNYFXID-JARXUMMXSA-N 0.000 description 2
- 208000004998 Abdominal Pain Diseases 0.000 description 2
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- CULUKMPMGVXCEI-UHFFFAOYSA-N N-methylcystisine Natural products C12=CC=CC(=O)N2CC2CN(C)CC1C2 CULUKMPMGVXCEI-UHFFFAOYSA-N 0.000 description 2
- 208000002193 Pain Diseases 0.000 description 2
- 208000005374 Poisoning Diseases 0.000 description 2
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- AAGFPTSOPGCENQ-UHFFFAOYSA-N Sophocarpin I Natural products C1CCC2CN3C(=O)C=CCC3C3C2N1CCC3 AAGFPTSOPGCENQ-UHFFFAOYSA-N 0.000 description 2
- IGXQFUGORDJEST-UHFFFAOYSA-N Sophocarpine Natural products O=C1C=CCC2C3CCCC4CCCC(CN12)C34 IGXQFUGORDJEST-UHFFFAOYSA-N 0.000 description 2
- VQYBAEAOOJBSTR-QHSBEEBCSA-N Sophoranol Chemical compound C([C@@H]12)CCC(=O)N1C[C@@]1(O)[C@H]3[C@@H]2CCCN3CCC1 VQYBAEAOOJBSTR-QHSBEEBCSA-N 0.000 description 2
- VQYBAEAOOJBSTR-AYRXBEOTSA-N Sophoranol Natural products O=C1N2[C@H]([C@@H]3[C@@H]4[C@](O)(C2)CCCN4CCC3)CCC1 VQYBAEAOOJBSTR-AYRXBEOTSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
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- 230000006872 improvement Effects 0.000 description 2
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- 210000004185 liver Anatomy 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- CULUKMPMGVXCEI-VHSXEESVSA-N n-methylcytisine Chemical compound C12=CC=CC(=O)N2C[C@@H]2CN(C)C[C@H]1C2 CULUKMPMGVXCEI-VHSXEESVSA-N 0.000 description 2
- 229930015582 oxymatrine Natural products 0.000 description 2
- 239000002574 poison Substances 0.000 description 2
- 231100000572 poisoning Toxicity 0.000 description 2
- 230000000607 poisoning effect Effects 0.000 description 2
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- AAGFPTSOPGCENQ-JLNYLFASSA-N sophocarpine Chemical compound C1CC[C@H]2CN3C(=O)C=CC[C@@H]3[C@@H]3[C@H]2N1CCC3 AAGFPTSOPGCENQ-JLNYLFASSA-N 0.000 description 2
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- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- XBZYWSMVVKYHQN-MYPRUECHSA-N (4as,6as,6br,8ar,9r,10s,12ar,12br,14bs)-10-hydroxy-2,2,6a,6b,9,12a-hexamethyl-9-[(sulfooxy)methyl]-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-icosahydropicene-4a-carboxylic acid Chemical compound C1C[C@H](O)[C@@](C)(COS(O)(=O)=O)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C XBZYWSMVVKYHQN-MYPRUECHSA-N 0.000 description 1
- 241000208838 Asteraceae Species 0.000 description 1
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- 241000345998 Calamus manan Species 0.000 description 1
- 241000208365 Celastraceae Species 0.000 description 1
- 241000675108 Citrus tangerina Species 0.000 description 1
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- 241000238631 Hexapoda Species 0.000 description 1
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- 241001093501 Rutaceae Species 0.000 description 1
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- 241001263604 Stellera chamaejasme Species 0.000 description 1
- 241000830536 Tripterygium wilfordii Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
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- 238000009825 accumulation Methods 0.000 description 1
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- 235000013871 bee wax Nutrition 0.000 description 1
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- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
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- 230000004345 fruit ripening Effects 0.000 description 1
- 208000027692 gas pain Diseases 0.000 description 1
- 235000021384 green leafy vegetables Nutrition 0.000 description 1
- 208000035861 hematochezia Diseases 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
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- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a preparation method for a botanical pesticide for specially killing cabbage caterpillars during organic vegetable planting. The preparation method comprises the following steps: 1), preparing raw materials, wherein the raw materials comprise the following components in parts by weight: 10-15 parts of radix sophorae flavescentis, 7-10 parts of melia toosendan, 12-19 parts of melia toosendan bark, 10-15 parts of tripterygium glycosides, 18-24 parts of raw kusnezoff monkshood roots, 4-6 parts of radix euphorbiae lantu, 6-8 parts of pericarpium citri reticulatae and 13 parts of tobacco; 2), adding 3 to 4 times of water by weight in the raw materials, decocting in a sealing manner at the temperature of 90-100 DEG C for 100 to 120 minutes, filtering, and concentrating the filtrate to be 1/3-1/4 of the original used water amount to obtain the botanical pesticide for specially killing pierisrapae linne. The botanical pesticide can targetedly and specially kill cabbage caterpillars by scientific compatibility of the traditional Chinese medicine components, and is high in permeability, conducive to plant uptake, low in cost, free of three-evil, residue, pollution and drug resistance, high in drug adsorption, and long in drug effect duration.
Description
Technical field
The present invention relates to a kind of agricultural planting Pesticidal technology, specifically a kind of middle-size and small-size (family) farm is in organic vegetable kind
The method and apparatus preparing special for killing cabbage worm vegetable insecticide during plant.
Background technology
The phenomenon abusing chemical pesticide in China's green leaf vegetable is quite serious.Country expressly provides the chemical pesticide prohibitting the use of
Peasant still use, therefore due in agricultural product the exceeded poisoning causing of high-toxic pesticide residual quantity occur repeatedly.According to statistics, entirely
The world has 3,000,000 pesticide intoxication persons every year, China have every year tens thousand of to 100,000 pesticide intoxication persons.Chemical pesticide residual is exceeded to be caused
Food poisoning at any time all it may happen that.Meanwhile, long-term chemical pesticide remains in people's cylinder accumulation, leads to be difficult to discover
Chronic poisoning and " three cause " effect.Meanwhile, chemical pesticide residual also results in soil fail, environmental pollution.At present, open energetically
Send out pesticide made of Chinese medicinal herbs, progressively substituting chemical pesticide is a new breakthrough in World Agrochemicals history.
Cabbage butterfly (Classification system：Pierisrapae Linne), also known as Pieris rapae, become 12～20 millimeters of polypide length, vegetable powder
Butterfly belongs to complete metamorphosiss and develops.Main host plants are in Cruciferae, Compositae, Convolvulaceae etc. 9 section plant, Cruciferae vegetable of mainly causing harm
Dish, especially with cabbage mustard, Caulis et Folium Brassicae capitatae, Brassica oleracea L. var. botrytis L. etc. aggrieved than more serious.
All there is the not good defect of insecticidal effect in the existing at present vegetable insecticide for Pieris rapae.
Content of the invention
The technical problem to be solved in the present invention is to provide a kind of middle-size and small-size (family) farm in organic vegetable planting process
The method preparing vegetable insecticide, this vegetable insecticide is used in particular for special for killing cabbage worm.
In order to solve above-mentioned technical problem, the present invention provides a kind of plant of organic vegetable planting process special for killing cabbage worm to kill
The preparation method of worm agent, follows the steps below successively：
1), preparation raw material：
With Radix Sophorae Flavescentiss 10-15 part, Fructus Toosendan 7-10 part, Fructus Toosendan skin (Cortex Meliae) 12-19 part, Radix Tripterygii Wilfordii 10-15 part, Radix Aconiti Kusnezoffii
18-24 part, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4-6 part, Pericarpium Citri Reticulatae 6-8 part, 13 parts of constitutive materials of Nicotiana tabacum L.；Described part is weight portion；
2), add the water of 3～4 times of weight in the feed, seal 100～120 points of decoction at a temperature of 90～100 DEG C
Clock；Filter, gained filtrate concentrates the 1/3～1/4 of most former water consumption, obtains the vegetable insecticide of special for killing cabbage worm.
Improvement as the preparation method of the vegetable insecticide of the machine growing vegetables process special for killing cabbage worm of the present invention：Concentrate and be
Concentrated at 90～110 DEG C.
Improvement further as the preparation method of the vegetable insecticide of the machine growing vegetables process special for killing cabbage worm of the present invention：
Step 1) be：With 13 parts of Radix Sophorae Flavescentiss, 10 parts of Fructus Toosendan, 19 parts of Fructus Toosendan skin, 15 parts of Radix Tripterygii Wilfordii, 24 parts of Radix Aconiti Kusnezoffii, 6 parts of the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), Pericarpium Citri Reticulatae 8
Part and 13 parts of constitutive materials of Nicotiana tabacum L..
In raw material, the source of every composition is described as follows：
Radix Sophorae Flavescentiss, (scientific name：Sophora flavescens) for pulse family Radix Sophorae Flavescentiss belong to plant.It is distributed in Russia, Japan, print
The ground such as each provinces and regions in north and south of degree, Korea and China's Mainland, are grown on the area of 1500 meters of height above sea level, give birth in hillside, sand ground, grass more
In slope, spinney and near field, at present not yet by artificial introducing and planting.Indication：Heat clearing and damp drying, parasite killing, diuresis.For
Cure hematodiarrhoea, have blood in stool, jaundice urine retention, red and white leukorrhea.Matrine can be extracted, matrine is a kind of high-efficient broad-spectrum insecticide, not
All there is good insecticidal effect with area to the insect of the crops such as vegetable, fruit tree, Folium Camelliae sinensis, Semen Tritici aestivi, Oryza sativa L..And aqueous matrine solution
It is safe to people and animals, to crop no poisoning, noresidue, free from environmental pollution, using rear no bad smell, do not affect the matter of product
Amount and local flavor.Adopt (main matrine containing matrine, oxymatrine oxymatrine, sophor-anol based on Radix Sophorae Flavescentiss
Sophoranol, N-methylcytisine N-methylcytisine and SopHocarpine sophocarpine etc.), with other medium-height grass
Prescription supplemented by medicine, can make multiple have that insecticidal action is strong, noresidue, the plant to people and animals' low toxicity, environmentally safe
Insecticide.
Fructus Toosendan, (scientific name：Melia toosendan) for Meliaceae deciduous tree toosendanin mature fruit.Mainly originate in
The southern various places of China, superior with the product person in Sichuan, therefore also known as Fructus Toosendan.Fructus Toosendan is cold in nature, bitter in the mouth, is the one of qi-activating drug
Kind.There are soothing liver-QI promoting the circulation of QI to relieve pain, the drug effect of anthelmintic.For chest side of body, abdominal distention, colic, abdominal pain due to worm stagnation.But also be to make efficiently
The important source material of no residual hazard free of contamination novel plant pesticide.Fructus Toosendan bitter cold settles, and mainly enters Liver Channel, catharsis liver-heat, OK
Gas pain relieving, controls the stagnation of QI and has demonstrate,proving of heat especially suitable.
Fructus Toosendan skin (Cortex Meliae) is dry bark and the root bark of Meliaceae plant Fructus Toosendan, also known as Melia azedarach L., gloomy tree, pale reddish brown tree, hardship
Chinaberry skin etc..Fructus Toosendan is widely distributed, mainly originates in the ground such as China Sichuan, Hunan, Hubei, Henan, Guangxi, Guizhou, Yunnan.At present
Extract chinaberry alkane type triterpenoid, lignanoids from Fructus Toosendan, flavonoid and other phenolic compounds wherein belong to triterpenoid compound
Toosendanin (TSN) there is anti-inflammation heat-clearing and toxic substances removing and the effect of anti-Enterozoa.
Radix Tripterygii Wilfordii, is Caulis Fibraureae, beeswax rattan, cabbageworm medicine, red medicine, water thick grass, Classification system again：Tripterygium
Wilfordii, is Celastraceae, the root of tripterygium plant Radix Tripterygii Wilfordii, liana shrub, and main product is in Fujian, Zhejiang, Anhui, Henan
Etc. ground.Be born in the shade how wet hillside, mountain valley, in the bushes of small stream side.The more shady and cool hillside of happiness, deep with slant acidity, soil layer
Sand soil or yellow soil the most preferably grow.Bitter in the mouth, pungent, cool in nature, poison greatly.Return liver and kidney channel.Effect removing toxic substances parasite killing.
Radix Aconiti Kusnezoffii, Chinese medicine name.Tuber for Ranunculaceae herbaceos perennial Aconitum carmichjaelii Debx. (wild species) or Aconitum kusnezoffii Reichb.Autumn stem
Excavation when leaf is withered, removes fibrous root and silt, is dried.Radix Aconiti Kusnezoffii used in the market mostly is wild product, China northern territory
Mainly take from ranunculaceae plant Aconitum kusnezoffii Reichb, the tuber of Aconitum carmichjaelii Debx. is then mainly taken from southern areas.There is expelling wind and removing dampness, dispelling cold by warming the meridian,
The effect of reducing swelling and alleviating pain.
The Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) (Classification system：Stellera chamaejasme Linn.), the another name river Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), continuous poison, Radix Stellerae etc., be
Thymelaeceae stellera, perennial herb or shrub.The toxicity of the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) is larger, can be with parasite killing.
Pericarpium Citri Reticulatae, is the mature peel of rutaceae orange and its variety.Evergreen dungarunga of tangerine or shrub, cultivate in mound
Mound, low mountain zone, rivers and lakes bank or Plain.It is distributed in each department on the south the Changjiang river.During 10 to December fruit maturation, take fruit
Real, strip peel, dry in the shade or aeration-drying.Being slit into 3 to 4 lobes when Pericarpium Citri Reticulatae strips more.Volatile oil contained by Pericarpium Citri Reticulatae has fragrant stomach invigorating
Effect with the wind dispelling therapeutic method to keep the adverse QI flowing downwards.
Nicotiana tabacum L., (scientific name：Nicotiana tabacum) it is Solanaceae annual herb plant, all there is cultivation all parts of the country.Cigarette
The main insecticidal constituent of grass is nicotine, and Nicotiana tabacum L. always just uses as insecticide among the people, to preventing and treating diseases and pests of agronomic crop effect
Significantly.
The invention belongs to the vegetable insecticide of special for killing cabbage worm；The scientific compatibility by Chinese medicine ingredients for the present invention, orientation is specially
Killing cabbage worm, permeability is strong, is conducive to the absorption of plant, low cost, the no three disasters, noresidue, pollution-free, no Drug resistance, Pharmaceutical
Absorption affinity is strong, duration of efficacy is long.
The specifically used method of the vegetable insecticide of the special for killing cabbage worm of the present invention is as follows：
By the vegetable insecticide of special for killing cabbage worm of the present invention and water according to 1:3～5 weight ratio is diluted, by gained
The full vegetable plot of diluent sprays, and consumption is 200～1000 grams of vegetable insecticide/mus, once sprays in the high-incidence season of Pieris rapae,
As illumination is good, a few hours or once dead because stomach function regulating of tagging absorbs to two days Pieris rapae.
Specific embodiment
Embodiment 1, a kind of vegetable insecticide of special for killing cabbage worm, its preparation method is to follow the steps below successively：
1), preparation raw material：
With 13 parts of Radix Sophorae Flavescentiss, 10 parts of Fructus Toosendan, 19 parts of Fructus Toosendan skin (Cortex Meliae), 15 parts of Radix Tripterygii Wilfordii, 24 parts of Radix Aconiti Kusnezoffii, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 6
Part, 8 parts of Pericarpium Citri Reticulatae, 13 parts of constitutive materials of Nicotiana tabacum L.；
2), add the water of 3 times of weight in the feed, decoct 120 minutes at a temperature of 100 DEG C；Gained filtrate is concentrated into
The 1/3 of former water consumption；After being cooled to room temperature, obtain the vegetable insecticide of special for killing cabbage worm.
Embodiment 2, a kind of vegetable insecticide of special for killing cabbage worm, its preparation method is to follow the steps below successively：
1), preparation raw material：
With 15 parts of Radix Sophorae Flavescentiss, 8 parts of Fructus Toosendan, 15 parts of Fructus Toosendan skin (Cortex Meliae), 13 parts of Radix Tripterygii Wilfordii, 20 parts of Radix Aconiti Kusnezoffii, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 5
Part, 7 parts of Pericarpium Citri Reticulatae, 13 parts of constitutive materials of Nicotiana tabacum L..
Step 2) with embodiment 1.
Embodiment 3, a kind of vegetable insecticide of special for killing cabbage worm, its preparation method is to follow the steps below successively：
1), preparation raw material：
With 10 parts of Radix Sophorae Flavescentiss, 7 parts of Fructus Toosendan, 12 parts of Fructus Toosendan skin (Cortex Meliae), 10 parts of Radix Tripterygii Wilfordii, 18 parts of Radix Aconiti Kusnezoffii, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4
Part, 6 parts of Pericarpium Citri Reticulatae, 13 parts of constitutive materials of Nicotiana tabacum L..
Step 2) with embodiment 1.
Experiment 1, the vegetable insecticide to above-described embodiment 1～embodiment 3 gained carry out respectively following for Pieris rapae
Virulence test：
By vegetable insecticide be diluted to 3 times, 5 times (times of weight), using the culture dish of diameter 9cm, in each culture dish
Filter paper on pad, places the two-sided Cabbage Mustard Leaves (remarks being all moistened with vegetable insecticide after dilution：Daily replacing once this Cabbage Mustard Leaves, often
Secondary make Cabbage Mustard Leaves basic confluent cultures ware), it is then placed in 10 Pieris rapae, be placed in constant incubator (25 DEG C of temperature, humidity
85%) behind 12 hours, 24 hours, 48 hours, record the death condition of Pieris rapae,
Each experiment is repeated 10 times, and takes its meansigma methods；The results are shown in Table 1.
Table 1, the mortality rate (%) of Pieris rapae
Comparative example 1, " 13 parts of Radix Sophorae Flavescentiss " in embodiment 1 are made into 25 parts, remaining is equal to embodiment 1.
Comparative example 2, " 13 parts of Nicotiana tabacum L. " in embodiment 1 is made into 18 parts, remaining is equal to embodiment 1.
Comparative example 3, " 13 parts of Nicotiana tabacum L. " in embodiment 1 is made into 8 parts, remaining is equal to embodiment 1.
Comparative example 4, " 13 parts of Radix Sophorae Flavescentiss, 13 parts of the Nicotiana tabacum L. " in embodiment 1 is made into " 20 parts of Radix Sophorae Flavescentiss, 20 parts of Nicotiana tabacum L. ", remaining
It is equal to embodiment 1.
Contrast experiment, the vegetable insecticide of above-mentioned comparative example 1～4 gained is carried out Pieris rapae according to testing 1 methods described
Virulence test, only carried out diluting 3 times of test, acquired results are as shown in table 2 below.
Table 2, the mortality rate (%) (3 times of dilution) of Pieris rapae
| 12 hours | 24 hours | 48 hours | |
| Comparative example 1 | 54% | 83% | 90% |
| Comparative example 2 | 55% | 82% | 90% |
| Comparative example 3 | 40% | 71% | 88% |
| Comparative example 4 | 52% | 75% | 88% |
| Embodiment 1 | 68% | 92% | 97% |
By the contrast of above-mentioned case, it is understood that：Proportion relation between every composition of the present invention is extremely important
's.Only optimal insecticidal effect could be obtained according to the formula that the present invention provides.
Last in addition it is also necessary to it is noted that listed above be only the present invention several specific embodiments.Obviously, this
Bright be not limited to above example, can also have many deformation.Those of ordinary skill in the art can be from present disclosure
The all deformation directly derived or associate, are all considered as protection scope of the present invention.
Claims (2)
1. the preparation method of the vegetable insecticide of organic vegetable planting process special for killing cabbage worm, is characterized in that carrying out successively following step
Suddenly：
1), preparation raw material：
With 13 parts of Radix Sophorae Flavescentiss, 10 parts of Fructus Toosendan, 19 parts of Fructus Toosendan skin, 15 parts of Radix Tripterygii Wilfordii, 24 parts of Radix Aconiti Kusnezoffii, 6 parts of the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), 8 parts of Pericarpium Citri Reticulatae and
13 parts of constitutive materials of Nicotiana tabacum L., described part is weight portion；
2), add the water of 3～4 times of weight in the feed, sealing decoction 100～120 minutes at a temperature of 90～100 DEG C；Cross
Filter, gained filtrate concentrates the 1/3～1/4 of most former water consumption, obtains the vegetable insecticide of special for killing cabbage worm.
2. the preparation method of the vegetable insecticide of organic vegetable planting process special for killing cabbage worm according to claim 1, it is special
Levying is：Described concentrate in 90～110 DEG C and concentrated.
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| CN105410058B (en) * | 2015-12-23 | 2017-12-08 | 云南省农业科学院园艺作物研究所 | A kind of cabbage caterpillar insecticide and preparation method thereof |
| CN105394098B (en) * | 2015-12-23 | 2017-11-03 | 云南省农业科学院园艺作物研究所 | A kind of method for preventing and treating cabbage caterpillar |
| CN105994417A (en) * | 2016-06-13 | 2016-10-12 | 南京信息工程大学 | Environment-friendly insecticide and preparation method and application thereof |
| CN106962422A (en) * | 2017-05-12 | 2017-07-21 | 还童（锦州）特殊医学用途配方食品有限公司 | Vegetable insecticide and preparation method thereof |
| CN108967452A (en) * | 2017-06-03 | 2018-12-11 | 黑龙江省小磨坊有机杂粮农业有限责任公司 | A kind of natural organic insecticide |
| CN108308207A (en) * | 2018-03-23 | 2018-07-24 | 夏文秀 | A kind of vegetable insecticide and preparation method thereof for vegetable cultivation |
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| CN102283260A (en) * | 2011-09-07 | 2011-12-21 | 杜肇南 | Biologic bactericide prepared from plant sources |
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