KR20140039394A - Composition of insecticide or fungicide comprising the mixtured herbal medicine by alcohol aging - Google Patents

Abstract

The present invention relates to a composition of an insecticide or a fungicide comprising an aged alcohol of a herbal medicine mixture of Sophora flavescens, tobacco leaf, chamomile, purslane, Persicaria blume, Persicaria hydropiper, Huttuynia cordata, pepper, sugar, and alcohol. The composition of an insecticide or a fungicide has a superior efficacy to control various kinds of pests or fungi damaging crops, and therefore, can be used as an eco-friendly composition of an insecticide or a fungicide unlike an existing synthetic composition of an insecticide or a fungicide causing an environmental pollution, a harmful effect on a human body, a crop tolerance, an ecosystem disturbance, etc. [Reference numerals] (AA) Step of mixing the 30-70 by weight of tabacco, the 20-50 by weight of camomile, the 80-120 of purslane, the 30-70 by weight of yeogwi , the 30-70 by weight of huttuynia cordata, the 5-20 by weight of red pepper, the 350-550 by weight of sugar, and 300-500 by weight of alcohol based on the 100 by weight of ginseng; (BB) Step of aging a herbal medicine mixture at 11-20째C for 10-20 days; (CC) Step of obtaining filtered water solution by filtering the aged materials

Description

Composition of Insecticide or fungicide comprising the mixtured herbal medicine by alcohol aging

The present invention relates to an insecticide or fungicide composition containing an alcohol aging of a herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, moxa, eochocho, pepper, sugar and alcohol.

In modern agriculture, almost all are using synthetic pesticides to control pests or plant diseases caused by fungi. However, due to the excessive use of chemical pesticides for a long time, ecosystem disturbance such as soil microbial and natural enemy degradation, water pollution, and environmental problems such as soil and pesticide residues of agricultural products have emerged as a big social issue. There is an urgent need for natural pesticides or pesticides which are low toxic, non-toxic, and non-toxic for realization. In addition, chemical pesticides, which have been used for decades, are resistant to pests and fungi that cause plant diseases, and over time they can only be controlled by using more pesticides or more deadly pesticides. In addition to making the environmental problem more serious, it also creates serious social problems that can be fatal to humans who consume crops directly. Accordingly, studies on biopesticides using natural insecticides or fungicides to replace chemical pesticides are being actively conducted. Well-known plant insecticides include pyrethrin and rotenone isolated from Lonchcarpus nicou , a component of the pesticide country, and Melia azedarach var. Limonoids compounds isolated from japonica MAKINO, subtripinnata, and neem tree are also popular as insecticides (J. Agric. Food Chem., 2003, 51, 369-374).

On the other hand, although the pesticide or fungicide component is present in a trace amount in the natural state, its content is often increased when the plant extract or the plant is aged. The aging process is a method of inducing the structural change of the active ingredient by infiltrating the aged material into water or alcohol or making the extraction of the active ingredient smooth. As compared with the fermentation requiring the microorganism and the medium, aging is mainly performed at a low temperature (4 ~ 50 ° C) of water as a solvent. For example, a plant called Baekguyong contains a small amount of pulsatilla saponin D, which is an anti-cancer component. However, when the Baekguyong is matured, the hyderaginin glycoside contained in Baekguyong It has been confirmed that the content of the full-tattilasapotin D is increased by 2 to 3 times as the flour is converted into full-tilasapotin D (US Patent No. 7682638).

The inventors of the present invention while studying the insecticide or fungicide composition using natural products, when using the alcohol aging of the herbal mixture containing wild ginseng, tobacco leaf, wild chrysanthemum, purslane, moxa, eochocho, pepper, sugar and alcohol as a plant control agent The present invention could be completed by revealing the enhanced control against pests and fungi.

Among the compositions constituting the herbal mixture, Korean Patent Application Publication No. 2012-0072269 discloses a pesticide composition containing tobacco leaves, and Korean Patent No. 1128264 discloses an insecticide composition containing Eoseongcho. In addition, Korean Patent No. 514978 discloses an insecticide composition containing licorice, and Korean Patent Publication No. 1989-0009271 discloses a fungicidal composition containing onion, but the composition of the present invention and the preceding art. Since the overall composition and effects of the techniques are different, the above prior arts can be said to be different from the present invention.

USP 7682638 (Use of hederagenin 3-O- alpha -L-rhamnopyranosyl (1-2) - [beta -D-glucopyranosyl (1-4)] -? - L-arabinopyranoside or an extract from pulsatillae radix containing the same as a therapeutic agent for solid tumors, March 23, 2010. Registration) Korean Laid-Open Patent No. 2012-0072269 (Pesticide manufacturing method using natural materials, published on July 3, 2012) Korean Registered Patent No. 1128264 (Natural insecticide to induce insecticide and its manufacturing method, registered on March 13, 2012) Korean Registered Patent No. 514978 (Chicken Red Scabicidal Insecticide Composition, Registered 2005.09.07.) Korean Patent Publication No. 1989-0009271 (A method for sterilizing fungicides and phytopathogenic fungi, published 1989.08.01.)

Carpinella, M.C. et al., Antifeedant and insecticide properties of a limonoid from Meliaceae [Meliaceae] with potential use for pest management, J. Agric. Food Chem., 2003, 51, 369-374.

It is an object of the present invention to provide an insecticide or fungicide composition containing an alcohol aging product of a herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, vulgaris, red pepper, red pepper, sugar and alcohol.

The present invention relates to an insecticide or fungicide composition containing an alcohol aging of a herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, moxa, eochocho, pepper, sugar and alcohol.

Alcohol medicinal product of the herbal mixture is based on 100 parts by weight of ginseng, 30 to 70 parts by weight, 20 to 50 parts by weight of wild chrysanthemum, 80 to 120 parts by weight of purslane, 30 to 70 parts by weight, 30 to 70 parts by weight of eoseongcho , 5 to 20 parts by weight of red pepper, 350 to 550 parts by weight of sugar and 300 to 500 parts by weight of alcohol may be filtrate obtained by mixing with alcohol.

In addition, one or more herbal medicines selected from the group consisting of castor, licorice and onion skin may be added to the herbal mixture. Preferably, the herbal mixture may be mixed with at least one herb selected from the group consisting of 30 to 70 parts by weight, licorice licorice 1 to 15 parts by weight and onion peel 40 to 80 parts by weight based on 100 parts by weight of ginseng. have.

Shochu may be used as the alcohol.

Alcohol aging of the herbal mixture may be aged for 10 to 20 days at 11 ~ 20 ℃.

The insecticide or fungicide composition may be diluted in water of 400 to 2000 times the weight of the composition.

In addition, the insecticide or fungicide composition may further contain a phytonutrient, a pesticide or a mixture of two or more thereof.

The composition includes aphids, meadowsweet aphids, black aphids, peach aphids, cotton aphids, spotted mite, greenhouse dust, whiskers, blue worms, oysters, green chestnut moths, deep-moth moths, slugs, larvae, moths, sheer beetles, pears Seaweed Moth, Pear Tree, Little Pear, Pear Moth, Creeper Moth, Rice Creeper Moth, Rice Creeper Moth, Rice Creeper Moth, Rice Creeper Moth, Rice Cactus, Rice Weevil, Rice Clover, Chinese Cabbage Moth, Chinese Cabbage One or more pests selected from the group consisting of seminar rooms, moths, moth larvae, or the plant pathogen Fusarium oxysporum, Cylindrocarpon destructans , root rot bacteria), Botrytis cinerea, gray mold pathogen), Colle Saturday kyum geuloh Eos tree forest death (Colletotrichum gloeosporioides , anthrax causative), Sclerotium ( Sclerotium) cepivorum, black rot pathogen gyunhaekbyeong), Loti's Clermont Clermont Nias to Tio Room (Sclerotinia sclerotiorum , causative organism), Penicillium hirsutum , causative bacteria of blue mold), Pectobacterium carotovorum , a causative agent), Rhizoctonia solani , causative agent), Pythium ultimum , causative agent), Pythium debaryanum , a causative agent of the genus Agrobacterium ) and Rhizopus sp., which can be used as a control against one or more plant disease strains selected from the group consisting of.

Therefore, the present invention preferably,

On the basis of 100 parts by weight of ginseng, 30 to 70 parts by weight of tobacco leaves, 20 to 50 parts by weight of wild chrysanthemum, 80 to 120 parts by weight of purslane, 30 to 70 parts by weight of vulture, 30 to 70 parts by weight of eoseongcho, 5 to 20 parts by weight of red pepper, Mixing 350 to 550 parts by weight of sugar and 300 to 500 parts by weight of alcohol;

Aging the herbal mixture at 11-20 ° C. for 10-20 days; And

Filtering the aging to obtain a filtrate;

It provides a method for producing an alcohol aging of the herbal mixture comprising a.

Hereinafter, the present invention will be described in more detail.

When the herbal mixture is mixed and aged each herbal medicine beyond the herbal mixing ratio disclosed above, the insecticidal effect may be lowered.

In addition, among the components that can be mixed in the herbal mixture, onion pulp may be included instead of onion peel, but it is preferable to use onion peel which is a by-product of onion. Onion peel is a by-product that is discarded after trimming to use onion as a food ingredient, and it has a cost-saving effect. Also, onion peel contains 30 times as much quercetin as the main ingredient of onion flesh. have.

Alcohol fermentation of the herbal mixture is most preferably aged for 10 to 20 days at 11 ~ 20 ℃, it is preferable to extend the ripening period at a temperature lower than 11 ℃, and further aged at a temperature higher than 20 ℃ It is desirable to shorten it.

As alcohol used for alcohol aging of the herbal mixture, it is most preferable to use shochu, and the shochu may use 30 to 40 degrees shochu (alcohol content 30 to 40% (v / v)). Moreover, 30-40% (v / v) ethanol aqueous solution or another kind of distilled alcohol can also be used.

Alcohol fermentation of the herbal mixture may be used after the aging, the filtrate obtained by removing the solid content, when the removed solid content to 100 parts by weight, 10 to 20 parts by weight of sugar and 20 to 30 parts by weight of soju After the mixture is prepared, the mixture may be re-aged at 11-20 ° C. for 10-20 days. Through this process, the active ingredient remaining in the solid content of the herbal medicine may be used again in the aging process.

In addition, the alcohol aging of the herbal mixture may contain a natural pesticide extract, pesticide or a mixture of two or more thereof.

The natural product extract may include extracts such as mulberry, wormwood, garlic, rhubarb, tansy, gosam, celandine. Among them, especially the fruit of the mulberry tree has excellent insecticidal effect, and is known to contain a large amount of theophylline component that acts on the insect pests. The composition of the present invention may also contain nem oil extracted and purified from the mulberry fruit, which has an insect control effect (an insect's decline in an insect's pests, growth retardation, reproductive dysfunction, repellent effect, .

In addition, the alcohol aging of the herbal mixture may contain a phytonutrient added. As a phytonutrient which can be added to the alcohol aging of the herbal mixture of the present invention, conventionally used plant nutritional fertilizers may be used. As the above-mentioned fertilizer, organic fertilizer, compound fertilizer, nitrogen fertilizer, phosphoric acid fertilizer, calcium fertilizer, lime fertilizer, lactic acid fertilizer, sulfuric acid fertilizer, magnesium fertilizer, trace element fertilizer, organic fertilizer and manure fertilizer can be used. The composition of the insecticide composition and the plant nutrients of the present invention is mixed, it can be used as a phytonutrient useful for the growth of plants while having excellent control effect against the various pests.

Pesticides that may be added to the alcohol aging of the herbal mixture of the present invention may include conventionally used pesticides. Preferably, the pesticide may be carbamate, organic phosphate, organic chlorine pesticide, phenylpyrazole, pyrethroid, neonicotinoid, spinosin, avermectin, milbimecin, larval hormone analogue, Alkyl halides, organotin compounds, nereistoxin analogues, benzoylurea, diacylhydrazines, insecticides of METI acaricides, chloropicrine, pimetrozine, phlonicamid, clopentesine, hexiatia , Ethoxazole, diafenthiuron, propargite, tetradipon, chlorfenapyr, DNOC, buprofezin, cyromazine, amitraz, hydrmethylmone, acequinosyl, fluacrypyrim, rotenone or these Pesticides such as derivatives of can be used.

In addition, the insecticide or fungicide composition containing the alcohol aging of the herbal mixture may be used in admixture with other commonly used active ingredients or excipients, and may be used by further adding pigments, surfactants, and preservatives. have.

The insecticide or fungicide composition may be sprayed on the plant using a spray method.

In addition, the alcohol aging of the herbal mixture may be used immediately after alcohol aging, and after evaporating the alcohol component, it may be powdered and mixed with various insecticides or fungicide compositions.

Alcohol medicinal product of the herbal mixture can be used through various methods depending on the form, application purpose, and application field, such as a method of diluting with water, spraying method, and the like. It can use suitably according to a site | part, application object, etc. However, the insecticide or fungicide composition containing the alcohol aging of the herbal mixture of the present invention does not particularly limit the amount used or the method of application.

In addition, the present invention may provide a foliar spraying agent, irrigation spraying agent, phytonutrient, seed coating agent, soil improving agent, composting agent containing the pesticide or fungicide composition.

The alcohol aging of the herbal mixture of the present invention, preferably, sorghum, mung beans, rice, barley, wheat barley, sesame, both large, kidney beans, perilla, red beans, soybeans, red beans, corn, oats, buckwheat, tangerines, quince, Chestnut, peach, persimmon, apricot, bank, plum, citron, whiskey, apple, pear, jujube, grape, orange, watermelon, melon, strawberry, cucumber, pumpkin, loofah, tomato, pumpkin, gourd, cherry tomato, paprika, bokbunja , Melon, lettuce, cabbage, buttercup, leek, freshly, garland chrysanthemum, cabbage, radish, burdock, onion, garlic, radish, burdock, lotus, potato, sweet potato, carrot, bellflower, duckling, hemp, taro, green onion, mountain garlic, It can be used as a control agent for one plant selected from ginseng and nocturnal ganoderma.

In addition, the alcohol aging of the herbal mixture of the present invention can be used as a control against wilting disease, root rot disease, black rot fungal disease, ash fungus, anthrax, fungal disease, blue mold disease, root disease, diarrhea disease, and sores of these plants.

The present invention relates to an insecticide or fungicide composition containing an alcohol aging of a herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, vulgaris, eosungcho, red pepper, sugar and alcohol, the insecticide or fungicide composition, As it has excellent efficacy in controlling various pests or fungi that damage crops, it is an environmentally friendly insecticide or fungicide composition, unlike conventional synthetic insecticide or fungicide composition that involves environmental pollution, human hazard, crop resistance, and ecosystem disturbance. Can be used as

Figure 1 is a flow chart showing the steps of preparing the alcohol aging of the herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, vulgaris, eosungcho, red pepper, sugar and alcohol of the present invention.

Hereinafter, preferred embodiments of the present invention will be described in detail. However, the present invention is not limited to the embodiments described herein but may be embodied in other forms. Rather, these embodiments are provided so that this disclosure will be thorough and complete, and will fully convey the concept of the invention to those skilled in the art.

< Example  One. You , Tobacco leaf , Chrysanthemum, purslane, Devil Of herbal mixtures of fish, fish, peppers, sugar and alcohol Aging  Manufacturing>

Ginseng, tobacco leaves, wild chrysanthemum, purslane, mole, eoseongcho, pepper, sugar, shochu, onion peel, castor and licorice were mixed under the conditions of Table 1 and aged for 14 days at 20 ℃.

Condition Weight (kg) You Tobacco leaf Chrysanthemum purslane Devil Sophora pepper Sugar Soju onion
skin very
Cary licorice Example 1-1 100 70 49.75 120 70 70 20 456.5 375 - - - Examples 1-2 100 70 37.5 120 50 66.25 12.5 437.5 375 62.5 - - Example 1-3 100 70 47.5 100 70 61.75 19.5 437.5 375 - 50 - Examples 1-4 100 70 49.5 120 70 70 20 437.5 388 - - 6.25 Examples 1-5 100 50 47.5 118 50 30 10.75 437.5 375 62.5 50 - Examples 1-6 100 70 37.5 100 70 70 15.5 437.5 375 - 50 6.25 Examples 1-7 100 70 37.5 120 55 55 12.5 437.5 375 62.5 - 6.25 Examples 1-8 100 50 37.5 100 50 50 12.5 437.5 375 62.5 50 6.25 Examples 1-9 100 50 20 118 50 50 12.5 437.5 375 40 70 8.25 Example 1-10 100 70 37.5 80 50 50 12.5 437.5 375 80 30 8.75 Example 1-11 100 50 37.5 100 30 70 12.5 437.5 375 67.75 50 One Examples 1-12 100 50 37.5 120 50 30 12.6 437.5 375 62.5 41.25 15 Examples 1-13 100 50 37.5 100 58 50 5 437.5 375 62 50 6.25 Examples 1-14 100 50 37.5 100 50 50 12.5 332.5 480 62.5 50 6.25 Examples 1-15 100 50 37.5 100 50 50 12.5 512.5 300 62.5 50 6.25

< Comparative Example  1.Alcohols of the Herbal Compounds to be Compared Aging  Manufacturing>

Noodles, tobacco leaves, wild chrysanthemum, purslane, mole, eoseongcho, red pepper, sugar, shochu, onion peel, castor and licorice were mixed under the conditions of Table 2 and aged for 14 days at 20 ℃.

Condition Weight (kg) You Tobacco leaf Chrysanthemum purslane Devil Sophora pepper Sugar Soju onion
skin very
Cary licorice Comparative Example 1-1 - 70 49.75 120 120 120 20 456.5 375 - - - Comparative Example 1-2 200 - 49.75 100 60 70 20 456.5 375 - - - Comparative Example 1-3 100 85 - 119.75 70 100 25 456.5 375 - - - Comparative Example 1-4 100 90 100 - 70 120 19.75 456.5 375 - - - Comparative Example 1-5 100 70 49.75 190 - 70 20 456.5 375 - - - Comparative Example 1-6 100 140 49.75 120 70 - 20 456.5 375 - - - Comparative Example 1-7 100 70 49.75 120 90 70 - 456.5 375 - - - Comparative Example 1-8 100 - - 100 100 100 99.75 456.5 375 - - - Comparative Example 1-9 100 100 100 - - 100 99.75 456.5 375 - - - Comparative Example 1-10 100 100 100 100 99.75 - - 456.5 375 - - - Comparative Example 1-11 - - - 125 125 125 124.75 456.5 375 - - - Comparative Example 1-12 125 125 125 - - - 124.75 456.5 375 - - - Comparative Example 1-13 250 249.75 - - - - - 456.5 375 - - - Comparative Example 1-14 - 250 249.75 - - - - 456.5 375 - - - Comparative Example 1-15 - - 250 249.75 - - - 456.5 375 - - - Comparative Example 1-16 - - - 250 249.75 - - 456.5 375 - - - Comparative Example 1-17 - - - - 250 249.75 - 456.5 375 - - - Comparative Example 1-18 - - - - - 250 249.75 456.5 375 - - - Comparative Example 1-19 120 78 80 80 79.75 - - 456.5 375 62.5 - - Comparative Example 1-20 90 90 90 90 89.75 - - 456.5 375 - 50 - Comparative Example 1-21 100 100 100 100 93.5 - - 456.5 375 - - 6.25 Comparative Example 1-22 - - 122.25 105 105 105 - 456.5 375 62.5 - - Comparative Example 1-23 - - 124.75 75 125 125 - 456.5 375 - 50 - Comparative Example 1-24 - - 124.75 125 125 118.75 - 456.5 375 - - 6.25

< Experimental Example  One. You , Tobacco leaf , Chrysanthemum, purslane, Devil Of herbal mixtures of fish, fish, peppers, sugar and alcohol Aging  Checking the effect of apple tree leaf against spotted mite>

On September 5, 2011, 50 apples (group 1) of the lower branches of the apple tree were taken, and 20 spotted mites per leaf were inoculated at the base of the leaves (total 1000), and other branches separated by 5m were taken. They were inoculated with spotted mites in the same way.

After 10 days, at 10 am by spraying water on the lower part of the leaves of the mite treatment, evenly moisten the leaves and dilute the composition of Example 1 and Comparative Example 1 with 1000 times the weight of water, respectively using a pesticide sprayer Sprayed thickly. 10 g of each dilution was sprayed on the same conditions at 10 o'clock the next day. After 72 hours of spraying, each leaf was picked up, and the number of spotted mites remaining on the apple tree leaves under a magnifying glass was examined and shown in Table 3 below. On the other hand, no sample was treated in the control group.

Condition Number of individuals of the spotted mite remaining on apple tree leaves (horses) Example 1-1 34 Examples 1-2 26 Example 1-3 31 Examples 1-4 22 Examples 1-5 28 Examples 1-6 32 Examples 1-7 34 Examples 1-8 12 Examples 1-9 15 Example 1-10 13 Example 1-11 16 Examples 1-12 12 Examples 1-13 16 Examples 1-14 15 Examples 1-15 19 Comparative Example 1-1 395 Comparative Example 1-2 377 Comparative Example 1-3 383 Comparative Example 1-4 362 Comparative Example 1-5 373 Comparative Example 1-6 395 Comparative Example 1-7 364 Comparative Example 1-8 473 Comparative Example 1-9 484 Comparative Example 1-10 456 Comparative Example 1-11 565 Comparative Example 1-12 528 Comparative Example 1-13 634 Comparative Example 1-14 614 Comparative Example 1-15 623 Comparative Example 1-16 632 Comparative Example 1-17 641 Comparative Example 1-18 624 Comparative Example 1-19 533 Comparative Example 1-20 542 Comparative Example 1-21 525 Comparative Example 1-22 564 Comparative Example 1-23 545 Comparative Example 1-24 557 Control group 977

   The results of Table 3 showed that the composition of Example 1 of the present invention exhibits high insecticidal properties.

< Experimental Example  2. You , Tobacco leaf , Chrysanthemum, purslane, Devil Of herbal mixtures of fish, fish, peppers, sugar and alcohol Aging Mustard radish  Checking the effectiveness of anti-

If the mustard seeds are grown in a field, the risk of the insect pests is very large. In this experiment, we observed the effect of aged ginkgo biloba on the pests and diseases of mustard radish.

We prepared 30 pots with four pairs of leaves by planting mustard in a flowerpot containing 100g of gardening soil. Three fields were made in 2m intervals in the field, and 30 pieces of mustard radish were placed 30cm apart for each group. In addition, after diluting the composition of Example 1 and Comparative Example 1 with 1000 times the weight of water in mustard radish between 10 am and 11 am on a sunny day having a temperature of 25 to 27 ° C., 10 g each was used by using a pesticide sprayer. Sprayed. Thereafter, the composition was sprayed in the same manner twice more at two day intervals. After 7 days of the last spray was confirmed the state of each mustard and the results are shown in Table 4 below.

Condition Number of edible canards (mustard) Example 1-1 21 Examples 1-2 20 Example 1-3 21 Examples 1-4 22 Examples 1-5 19 Examples 1-6 20 Examples 1-7 21 Examples 1-8 25 Examples 1-9 26 Example 1-10 29 Example 1-11 25 Examples 1-12 27 Examples 1-13 28 Examples 1-14 24 Examples 1-15 25 Comparative Example 1-1 11 Comparative Example 1-2 12 Comparative Example 1-3 10 Comparative Example 1-4 10 Comparative Example 1-5 11 Comparative Example 1-6 10 Comparative Example 1-7 12 Comparative Example 1-8 8 Comparative Example 1-9 8 Comparative Example 1-10 9 Comparative Example 1-11 6 Comparative Example 1-12 5 Comparative Example 1-13 4 Comparative Example 1-14 3 Comparative Example 1-15 4 Comparative Example 1-16 4 Comparative Example 1-17 3 Comparative Example 1-18 4 Comparative Example 1-19 8 Comparative Example 1-20 7 Comparative Example 1-21 6 Comparative Example 1-22 8 Comparative Example 1-23 8 Comparative Example 1-24 5 Control group One

Checking the results of Table 4, it was found that the control effect on the mustard radish of the composition of Example 1 of the present invention is significantly better than that of Comparative Example 1 or the control, in particular, onion peel, castor and licorice all Added cases were found to have higher pesticidal activity.

< Experimental Example  3. You , Tobacco leaf , Chrysanthemum, purslane, Devil Of antifungal activity of herbal mixtures mixed with, fish vinegar, red pepper, sugar and alcohol>

After diluting the alcohol aging of the herbal mixtures prepared in Example 1 and Comparative Example 1 with 1000-fold weight of water, it was confirmed that the mycelial growth was inhibited by replacing with various phytopathogens.

To this end, after sterilizing the medium of PDA (potato dextrose agar), mixed with 200 μl of the culture solution containing mycelia and spores of each pathogen in a medium at 50 ° C., the medium is completely hardened, and then the herbal medicine prepared in Example 1 and Comparative Example 1 After diluting the alcohol aging of the mixture with 1000 times the weight of water, 10 μl of the diluting solution was put on a paper disc (diameter 8 mm) and placed on a petri dish mixed with pathogens, and then grown at 28 ° C. for 7 days at which various pathogens were well grown. Incubated. Thereafter, the effect of the diluent on various pathogens was investigated with a low support diameter, which is shown in Tables 5-9.

Condition Growth jersey degree Example 1-1 Examples 1-2 Example 1-3 Examples 1-4 Examples 1-5 Examples 1-6 Examples 1-7 Botrytis cinerea +++ +++ ++ ++++ + ++ + Colletotrichum gloeosporioides ++ ++ ++ +++ +++ +++ ++ Cylindrocarpon destructans ++ +++ +++ ++++ +++ ++ + Pectobacterium carotovorum ++ + ++ +++ + +++ ++ Rhizoctonia solani +++ ++ ++ ++++ +++ ++ ++ Pythium ultimum +++ +++ +++ ++ ++ ++ + Pythium debaryanum ++ + ++ +++ ++ +++ +++ Sclerotium cepivorum +++ ++ ++++ ++ + ++ ++ Sclerotinia sclerotiorum +++ +++ + +++ ++ + + Pythium myriotylum ++ ++ +++ ++ ++ ++ ++ Penicillium hirstum +++ +++ ++ +++ + ++ + Rhizopus sp. ++ ++ +++ ++ ++ ++ ++ Note)-no activity; +, 10 mm or less; ++, 10.1-20 mm;
+++, 20.1-30; ++++, 30.1 mm or more

Condition Growth jersey degree Examples 1-8 Examples 1-9 Example 1-10 Example 1-11 Examples 1-12 Examples 1-13 Examples 1-14 Examples 1-15 Botrytis cinerea ++++ +++ ++++ ++++ + +++ ++++ + Colletotrichum gloeosporioides ++++ +++ +++ +++ +++ +++ +++ ++ Cylindrocarpon destructans +++ ++ ++ ++++ ++++ + + + Pectobacterium carotovorum ++++ + + +++ + ++++ ++ ++++ Rhizoctonia solani +++ ++++ +++ ++++ +++ ++ + + Pythium ultimum +++ +++ ++ ++ ++++ ++ ++ ++ Pythium debaryanum ++++ +++ ++++ + ++ +++ + ++++ Sclerotium cepivorum ++++ ++ +++ ++++ + ++ ++ ++ Sclerotinia sclerotiorum +++ +++ +++ +++ ++ ++++ + ++ Pythium myriotylum ++++ ++ + ++ ++ ++ ++++ ++ Penicillium hirstum ++++ +++ +++ +++ +++ ++++ ++ +++ Rhizopus sp. +++ ++ +++ ++ ++ ++ ++ Note)-no activity; +, 10 mm or less; ++, 10.1-20 mm;
+++, 20.1-30; ++++, 30.1 mm or more

Condition Growth jersey degree Comparative Example 1-1 Comparative Example 1-2 Comparative Example 1-3 Comparative Example 1-4 Comparative Example 1-5 Comparative Example 1-6 Comparative Example 1-7 Comparative Example 1-8 Botrytis cinerea + - + + + - + - Colletotrichum gloeosporioides ++ + - + - - - + Cylindrocarpon destructans - + + - - - + - Pectobacterium carotovorum - - - + ++ - - + Rhizoctonia solani + - + + - - - - Pythium ultimum + - ++ + - - + + Pythium debaryanum - - + - - - - - Sclerotium cepivorum ++ - + + + - - - Sclerotinia sclerotiorum - - - - - + + + Pythium myriotylum + - + + - - - - Penicillium hirstum + - + - ++ - + - Rhizopus sp. + - + + - - - - Note)-no activity; +, 10 mm or less; ++, 10.1-20 mm;
+++, 20.1-30; ++++, 30.1 mm or more

Condition Growth jersey degree Comparative Example 1-9 Comparative Example 1-10 Comparative Example 1-11 Comparative Example 1-12 Comparative Example 1-13 Comparative Example 1-14 Comparative Example 1-15 Comparative Example 1-16 Botrytis cinerea + - - - - - - - Colletotrichum gloeosporioides - - - - - - + - Cylindrocarpon destructans - - + - + - - - Pectobacterium carotovorum - - - - - - - - Rhizoctonia solani + - - - - - - + Pythium ultimum - - + + - + - - Pythium debaryanum - + - - - - - - Sclerotium cepivorum - - - - - - + - Sclerotinia sclerotiorum - + - - + - - - Pythium myriotylum - - + - - - - - Penicillium hirstum - - - - - + + - Rhizopus sp. - - - - - - - - Note)-no activity; +, 10 mm or less; ++, 10.1-20 mm;
+++, 20.1-30; ++++, 30.1 mm or more

Condition Growth jersey degree Comparative Example 1-17 Comparative Example 1-18 Comparative Example 1-19 Comparative Example 1-20 Comparative Example 1-21 Comparative Example 1-22 Comparative Example 1-23 Comparative Example 1-24 Botrytis cinerea - - + - - - - - Colletotrichum gloeosporioides - + + - - + - - Cylindrocarpon destructans - - - - + - + + Pectobacterium carotovorum + - + - - - - - Rhizoctonia solani - + - + - - + - Pythium ultimum + - - - + - - + Pythium debaryanum + - + - - + - - Sclerotium cepivorum - - - + - - + - Sclerotinia sclerotiorum - - - - - + - - Pythium myriotylum + - - - + - - - Penicillium hirstum - - - - - + - + Rhizopus sp. - - - - - - - - Note)-no activity; +, 10 mm or less; ++, 10.1-20 mm;
+++, 20.1-30; ++++, 30.1 mm or more

Referring to Tables 5 to 9, it can be seen that the alcohol aging of the herbal mixture of the present invention has a significantly superior control effect against fungi causing various plant diseases compared to the aging of the comparative example, in particular, onion peel, castor And both licorice was found to have higher antifungal activity. As a result, the composition of the present invention was found to exhibit excellent antagonism, such as rot, root rot, black rot fungal disease, gray mold, anthrax, fungal disease, blue mold disease, root disease, dizziness disease, incurable disease.

< Experimental Example  4. Confirm the Control Effect of Apple Tree Anthraci>

In order to determine the composition of apple trees anthrax control effect of the present invention directly in September 2011 PDB by 10 each in an apple tree orchard (potato dextrose broth) 2 days cultured Collet Sat tree kyum geuloh Eos Forest Death (Colletotrichum in gloeosporioides , anthrax causative) 10 g of strain cultures were sprayed (sprayed on apple leaves). After 7 days, the compositions of Example 1 and Comparative Example 1 were diluted in 1000 times the weight of water, sprayed three times at 100 g per tree at 15 day intervals, and anthrax occurred in each tree 30 days after the last spraying. The degree was confirmed. As a result, it was confirmed that the anthrax control effect of the apple tree sprayed with the composition of the present invention as shown in Table 10 is more excellent.

Treatment Details Anthrax Trees (Trees) Example 1-1 3 Examples 1-4 4 Examples 1-8 One Example 1-10 2 Examples 1-12 2 Comparative Example 1-1 7 Comparative Example 1-4 8 Comparative Example 1-7 9 Comparative Example 1-10 8 Comparative Example 1-14 7 Comparative Example 1-20 8 Comparative Example 1-24 8  No treatment 10

Claims (10)

An insecticide or fungicide composition comprising an alcohol aging product of a herbal mixture of wild ginseng, tobacco leaf, wild chrysanthemum, purslane, moxa, eosungcho, red pepper, sugar and alcohol. The method of claim 1,
The alcohol aging of the herbal mixture is based on 100 parts by weight of ginseng, 30 to 70 parts by weight of tobacco leaves, 20 to 50 parts by weight of wild chrysanthemum, 80 to 120 parts by weight of purslane, 30 to 70 parts by weight, 30 to 70 parts by weight of eosungcho, 5 to 20 parts by weight of red pepper, 350 to 550 parts by weight of sugar and 300 to 500 parts by weight of alcohol and pesticide or fungicide composition characterized in that the filtrate obtained by aging with alcohol. 3. The method of claim 2,
To the herbal mixture, based on 100 parts by weight of ginseng, at least one herb selected from the group consisting of 30 to 70 parts by weight, licorice licorice 1 to 15 parts by weight and onion peel 40 to 80 parts by weight is mixed Insecticide or fungicide composition. The method of claim 1,
Insecticide or fungicide composition, characterized in that the alcohol is shochu. 5. The method according to any one of claims 1 to 4,
The alcohol aging of the herbal mixture is a pesticide or fungicide composition, characterized in that prepared by aging for 10 to 20 days at 11 ~ 20 ℃. 5. The method according to any one of claims 1 to 4,
The insecticide or fungicide composition is a pesticide or fungicide composition, characterized in that used in dilution in water 400-2000 times the weight of the composition. 5. The method according to any one of claims 1 to 4,
The composition, aphids, meadowsweet aphids, black aphids, peach aphids, cotton aphids, spotted mite, greenhouse dust, whiskers, blue worms, oysters, green beetle moths, deep-moth moths, slugs, larvae, moths, moths Pear pear moth, pear tree, small pear tree, pear worm, rice worm, rice worm moth, rice worm moth, rice worm moth, rice worm moth, rice rot, rice weevil, rice locust, chinese cabbage moth, chinese cabbage, tobacco One or more pests selected from the group consisting of castor moths, moths and moth larvae, or the plant pathogen Fusarium oxysporum ( caused causative agent), Cylindrocarpon destructans, causative agent of root rot ), Botrytis cinerea (Billtis fungi), Colletotrichum gloeosporioides , anthrax causative), Sclerotium ( Sclerotium) cepivorum , black rot nucleus causative organism , sclerotinia sclerotiorum ( sclerotinia bacillus causative agent), penicillium hirsutum (Pentobium bacterium), Pectobacterium carotovorum , Root cause causal), Rhizoctonia solani , Pythium ultimum , Pythium debaryanum , and Rhizopus sp. Insecticide or fungicide composition, characterized in that it is used as a control against one or more plant disease strains selected from the group consisting of purifying bacteria. On the basis of 100 parts by weight of ginseng, 30 to 70 parts by weight of tobacco leaves, 20 to 50 parts by weight of wild chrysanthemum, 80 to 120 parts by weight of purslane, 30 to 70 parts by weight of vulture, 30 to 70 parts by weight of eoseongcho, 5 to 20 parts by weight of red pepper, Mixing 350 to 550 parts by weight of sugar and 300 to 500 parts by weight of alcohol;
Aging the herbal mixture at 11-20 ° C. for 10-20 days; And
Filtering the aging to obtain a filtrate;
Method of producing an alcohol aging of the herbal mixture comprising a. 9. The method of claim 8,
The alcohol is a method of producing an alcohol aging of the herbal mixture, characterized in that the shochu. 9. The method of claim 8,
Herbal medicine characterized in that the mixture of one or more herbal medicines selected from the group consisting of 30 to 70 parts by weight, licorice licorice 1 to 15 parts by weight and onion peel 40 to 80 parts by weight based on 100 parts by weight of ginseng Process for the preparation of alcohol aging of the mixture.

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