CN104370661A - Microecological preparation for grain production safety assurance and preparation method thereof - Google Patents
Microecological preparation for grain production safety assurance and preparation method thereof Download PDFInfo
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- CN104370661A CN104370661A CN201410564730.4A CN201410564730A CN104370661A CN 104370661 A CN104370661 A CN 104370661A CN 201410564730 A CN201410564730 A CN 201410564730A CN 104370661 A CN104370661 A CN 104370661A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Micro-Organisms Or Cultivation Processes Thereof (AREA)
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Abstract
The invention relates to a modern agriculture biotechnology, particularly a microecological preparation for grain production safety assurance and a preparation method thereof. The method can effectively enhance the production efficiency of the microecological preparation for grain production safety assurance, maximally ensures the activity of the microecological preparation, and improves the large-scale industrialized development of the production of the microecological preparation for grain production safety assurance. The microecological preparation for grain production safety assurance is prepared from the following raw materials in parts by weight by a certain preparation method: 100-150 parts of lactobacillus, 120-200 parts of bacillus, 130-180 parts of Bacillus pumilus, 550-700 parts of ammonium phytate, 80-200 parts of coated urea, 60-150 parts of phosphate fertilizer, 60-150 parts of ammonium dihydrogen phosphate, 20-35 parts of chitin, 3-30 parts of kurarinone and 20-50 parts of glauconite.
Description
One, technical field:
The present invention relates to Modern Agricultural Biotechnology, be specifically related to safe plant protection probiotics of a kind of grain-production and preparation method thereof.
Two, background technology:
In background technology, the factor affecting China's grain-production safety is at present of a great variety, and the factors such as different harmful organism, man-made disaster, environmental hazard are particularly outstanding.Recently, a file in national environmental protection portion has caused the strong interest of the domestic public to grain Land pollution.This part of file is pointed out: there are 3.6 ten thousand hectares of arable soil heavy metals exceeding standards in China, and the grain contamination caused every year is thus up to 1,200 ten thousand tons, and direct economic loss is more than 20,000,000,000 yuan.The behind of soil pollution is Food Security.For having a large population and a few land, and be difficult to the China of Irrrigation, day by day serious soil pollution is material injury 1,800,000,000 mu of arable land red lines, perhaps can bring new crisis in food to China always.The profile formulation of Ministry of Land and Resources is similar: at present the whole nation till the land area more than 10% by heavy metal contamination, about 1.5 hundred million mu altogether; In addition, the arable land of polluting because of sewage irrigation has 32,500,000 mu; Take up an area because solid waste is stored up and ruin field about have 2,000,000 mu, wherein majority concentrates on area that are fairly developed economically.Just because of this, in order to ensure grain-production safety, repair impaired soil resource, we need the preparation method innovating the safe plant protection probiotics of a kind of novel grain-production, in core technology, outstanding behaviours is can the temperature prepared of intelligent regulation and control probiotics and domestication adaptive ability, thus ensure its safety in utilization and maturity to greatest extent, the preparation of the safe plant protection probiotics of grain-production is made to realize standardization, resistance, adaptability, practicality, and easy and simple to handle, upgrading synergism is remarkable.
Three, summary of the invention:
The present invention is in order to solve the weak point in above-mentioned background technology; safe plant protection probiotics of a kind of grain-production and preparation method thereof is provided; it effectively can improve grain-production safe plant protection probiotics production efficiency; and ensure that it is active to greatest extent, improve the mass-producing of the safe plant protection probiotics production of grain-production, industrialization development.
For achieving the above object, the technical solution used in the present invention is: the safe plant protection probiotics of a kind of grain-production, is characterized in that: described preparation comprises following raw material: milk-acid bacteria 100 ~ 150 parts, genus bacillus 120 ~ 200 parts, bacillus pumilus 130 ~ 180 parts, phytic acid ammonium 550 ~ 700 parts, 80 ~ 200 parts, coated urea, 60 ~ 150 parts, phosphate fertilizer, phosphorus ammonium 60 ~ 150 parts, chitin 20 ~ 35 parts, kurarinone 3 ~ 30 parts, glaukonine 20 ~ 50 parts.
Also comprise following weight part auxiliary material: xanthohumic acid 60 ~ 100 parts, 20 ~ 50 parts, amino acid, bone meal 20 ~ 50 parts, rare earth 0.8 ~ 2 part, medical stone 10 ~ 50 parts.
The preparation method of described a kind of grain-production safe plant protection probiotics is: first phytic acid ammonium processed, then order adds coated urea, phosphate fertilizer, phosphorus ammonium, chitin, kurarinone, xanthohumic acid, amino acid, bone meal, rare earth, medical stone is added when fully stirring, wherein temperature of reaction is 80 DEG C, reaction times is 8 hours, be sequentially added into and ensure Antagonism and synergy, finally add glaukonine, milk-acid bacteria, genus bacillus, bacillus pumilus, be mixed into granular, adopt digital quantization drying, air-dry rear packaging.
The phytic acid ammonium that described phytic acid ammonium is weathered coal, brown coal, cinder generate through sorting, purification, fermentation, extraction process with the weight ratio of 2:1:1, leaching process is: by weathered coal, brown coal, cinder with the weight ratio of 2:1:1 respectively with 50 DEG C of water cleaning and dipping, again respectively with temperature fire 60 DEG C carry out for time the water treatment of 160 minutes, extracting pressure controls as 345MPa, and the time is 6h; Then 45% ethanol adding 5 times amount respectively carries out room temperature lixiviate, and total immersion carries 3 times, each 10 hours, merge vat liquor, filter liquor, the filter liquor of 3 times merges, and reclaims ethanol to obtaining medicinal extract without alcohol taste, the ethyl acetate of medicinal extract with 90% after the water suspendible of 2 times amount carries out three extractions, until extraction liquid is colourless, combined ethyl acetate extraction liquid, is concentrated into paste, drying, obtains dry powder; By the dry powder blend obtained respectively.
Compared with prior art, the advantage that the present invention has and effect as follows: the present invention can effectively utilize milk-acid bacteria, genus bacillus, bacillus pumilus, these probioticss, play the effect of repairing and protecting, thus play an important role safely to grain-production to soil; And the harm of objectionable impurities to plant can be removed, thus significantly improve quality and the efficiency of grain-production.
Four, embodiment:
Applicant proves by detecting, and the total composition of organic active substance content that phytic acid ammonium after treatment contains should be greater than (N+P2O5+K2O) content (in butt), % >=45; Trace element and other effective constituent % >=25 of mushroom, total cadmium (in Cd), mg/kg≤3; Total mercury (in Hg), mg/kg≤5; Total lead (in Pb), mg/kg≤100; Total chromium (in Cr), mg/kg≤300; Total arsenic (in As), mg/kg≤30; And be best containing various trace elements, the material that can meet above-mentioned requirements after process is as grain-production safe plant protection probiotics high-quality resource, also can be used for biological organic fertilizer preparation.
During practical application, formula of the present invention can according to the kind of farm crop, local geography, fertility, weather condition are optimized combination, if tree class probiotics content 26%, nitrogen content 12%, phosphorus 12%, potassium 16%, iron 1.8%, zinc 1.2%, greengrocery nitrogen content 18%, phosphorus 18%, potassium 13%, molybdenum 0.3%, boron 0.29%, grain class nitrogen content 20%, phosphorus 20%, potassium 13%, manganese 1.6%.
Embodiment one:
A kind of grain-production safe plant protection probiotics is made up of the raw material of following weight part: milk-acid bacteria 120kg, genus bacillus 150kg, bacillus pumilus 160, phytic acid ammonium 580kg, coated urea 90kg, phosphate fertilizer 80kg, phosphorus ammonium 80kg, chitin 22kg, 5kg, glaukonine 20kg, xanthohumic acid 70kg, amino acid 20kg, bone meal 20kg, rare earth 1kg, medical stone 12kg.
Described phytic acid ammonium comprises the phytic acid ammonium for weathered coal, brown coal, cinder generate through sorting, purification, fermentation, extraction process with the weight ratio of 2:1:1, leaching process is: by weathered coal, brown coal, cinder with the weight ratio of 2:1:1 respectively with 50 DEG C of water cleaning and dipping, again respectively with temperature fire 60 DEG C carry out for time the water treatment of 160 minutes, extracting pressure controls as 345MPa, and the time is 6h; Then 45% ethanol adding 5 times amount respectively carries out room temperature lixiviate, and total immersion carries 3 times, each 10 hours, merge vat liquor, filter liquor, the filter liquor of 3 times merges, and reclaims ethanol to obtaining medicinal extract without alcohol taste, the ethyl acetate of medicinal extract with 90% after the water suspendible of 2 times amount carries out three times, until extraction liquid is colourless, combined ethyl acetate extraction liquid, is concentrated into paste, drying, obtains dry powder; By the dry powder blend obtained respectively.
Grain-production safe plant protection probiotics is preparation method comprise the following steps: first make phytic acid ammonium as required, then adding coated urea, phosphate fertilizer, phosphorus ammonium, adding chitin, kurarinone, xanthohumic acid, amino acid, bone meal, rare earth, medical stone when fully stirring.Wherein temperature of reaction is 80 DEG C, and the reaction times is 8 hours, is sequentially added into and ensures Antagonism and synergy, finally add glaukonine, milk-acid bacteria, genus bacillus, bacillus pumilus, be mixed into granular, adopts digital quantization drying, air-dry rear packaging.
Embodiment two:
A kind of grain-production safe plant protection probiotics is made up of the raw material of following weight part: milk-acid bacteria 130kg, genus bacillus 160kg, bacillus pumilus 140kg, phytic acid ammonium 650kg, coated urea 150kg, phosphate fertilizer 140kg, phosphorus ammonium 120kg, chitin 30kg, kurarinone 25kg, glaukonine 40kg, xanthohumic acid 80kg, amino acid 45kg, bone meal 35kg, rare earth 1.6kg, medical stone 40kg.
Described phytic acid ammonium comprises the phytic acid ammonium for weathered coal, brown coal, cinder generate through sorting, purification, fermentation, extraction process with the weight ratio of 2:1:1, leaching process is: by weathered coal, brown coal, cinder with the weight ratio of 2:1:1 respectively with 50 DEG C of water cleaning and dipping, again respectively with temperature fire 60 DEG C carry out for time the water treatment of 160 minutes, extracting pressure controls as 345MPa, and the time is 6h; Then 45% ethanol adding 5 times amount respectively carries out room temperature lixiviate, and total immersion carries 3 times, each 10 hours, merge vat liquor, filter liquor, the filter liquor of 3 times merges, and reclaims ethanol to obtaining medicinal extract without alcohol taste, the ethyl acetate of medicinal extract with 90% after the water suspendible of 2 times amount carries out three times, until extraction liquid is colourless, combined ethyl acetate extraction liquid, is concentrated into paste, drying, obtains dry powder; By the dry powder blend obtained respectively.
Grain-production safe plant protection probiotics is preparation method comprise the following steps: first make phytic acid ammonium as required, then adding coated urea, phosphate fertilizer, phosphorus ammonium, adding chitin, kurarinone, xanthohumic acid, amino acid, bone meal, rare earth, medical stone when fully stirring.Wherein temperature of reaction is 80 DEG C, and the reaction times is 8 hours, is sequentially added into and ensures Antagonism and synergy, finally add glaukonine, milk-acid bacteria, genus bacillus, bacillus pumilus, be mixed into granular, adopts digital quantization drying, air-dry rear packaging.
Digital quantization drying in above-described embodiment is: be 10%-18% by the water content of the various batch materials of Digital Control, waits after reaching various batch materials physics absorbent drying to water content 18%-20% and packs.
five, test example
1, test objective
Verify that the safe plant protection probiotics of the grain-production of development and production of the present invention is to the effect of wheat growth and effect of increasing production, and the impact on objectionable impurities in Farming soil, on wheat paddock, large scale application provides scientific basis.
2, test method
2011 little is arranged in six groups, Cao Jiapo village of Zhi Bao township, Heyang County, Cao builds in loyal contracted field and implements, plot experiment area is 8 mu, 8 mu of ground are divided into four groups, first three groups is often organized and is all used the safe plant protection probiotics of grain-production, last group is blank group, manually will use soil trencher sowing processed.
3, processing mode
Within 2011, use the safe plant protection probiotics of grain-production of development and production of the present invention to make base fertilizer, use liquid fertilizer seed soaking, dial fertile 1 time of joint phase spray, fertile 1 time of spray in flowering period.To wash be 600 times in the seed soaking used, and pulls out to dry for subsequent use after two hours, sprays dilution 800 times, select to become a fine day, without mist, calm time spray, consumption every mu 250ML is the best.
4, physiological index determining
Flowering period measures leaf water content, chlorophyll content.The relative number of seedling determination white root, blade, measures the height in each period, the assay of heavy metal in soil.
5, analytical results
Table 1: the safe plant protection probiotics of grain-production of development and production of the present invention is on the impact of wheat yield
Table 2: the grain-production safe plant protection probiotics of development and production of the present invention uses the content balance of each heavy metal species in the soil of front and back
6, conclusion: from table 1, use the safe plant protection probiotics of the grain-production of development and production of the present invention, per mu yield on average increases by 42.2%.
From table 2, after using the safe plant protection probiotics of the grain-production of development and production of the present invention, the copper in soil, zinc, lead, cadmium content reduce all in a short time.The plantation of producing for grain security provides good edaphic condition.
7, conclusion: the safe plant protection probiotics of grain-production of development and production of the present invention is natural bioactive preparation, nuisanceless, pollution-free, have no side effect, three acid included can remove the harm of objectionable impurities to plant, soil is had to the effect of repairing health care, for environmentally friendly product, meet the international green environment propensity to consume, can promote the use of.
Claims (4)
1. the safe plant protection probiotics of grain-production, is characterized in that: described preparation comprises following raw material: milk-acid bacteria 100 ~ 150 parts, genus bacillus 120 ~ 200 parts, bacillus pumilus 130 ~ 180 parts, phytic acid ammonium 550 ~ 700 parts, 80 ~ 200 parts, coated urea, 60 ~ 150 parts, phosphate fertilizer, phosphorus ammonium 60 ~ 150 parts, chitin 20 ~ 35 parts, kurarinone 3 ~ 30 parts, glaukonine 20 ~ 50 parts.
2. the safe plant protection probiotics of a kind of grain-production according to claim 1, is characterized in that: also comprise following weight part auxiliary material: xanthohumic acid 60 ~ 100 parts, 20 ~ 50 parts, amino acid, bone meal 20 ~ 50 parts, rare earth 0.8 ~ 2 part, medical stone 10 ~ 50 parts.
3. the preparation method of a kind of grain-production according to claim 1 safe plant protection probiotics: described preparation method is: first phytic acid ammonium processed, then order adds coated urea, phosphate fertilizer, phosphorus ammonium, chitin is added when fully stirring, kurarinone, xanthohumic acid, amino acid, bone meal, rare earth, medical stone, wherein temperature of reaction is 80 DEG C, reaction times is 8 hours, be sequentially added into and ensure Antagonism and synergy, finally add glaukonine, milk-acid bacteria, genus bacillus, bacillus pumilus, be mixed into granular, employing digital quantization is dry, air-dry rear packaging.
4. the preparation method of the safe plant protection probiotics of a kind of grain-production according to claim 3, it is characterized in that: the phytic acid ammonium that described phytic acid ammonium is weathered coal, brown coal, cinder generate through sorting, purification, fermentation, extraction process with the weight ratio of 2:1:1, leaching process is: by weathered coal, brown coal, cinder with the weight ratio of 2:1:1 respectively with 50 DEG C of water cleaning and dipping, again respectively with temperature fire 60 DEG C carry out for time the water treatment of 160 minutes, extracting pressure controls as 345MPa, and the time is 6h; Then 45% ethanol adding 5 times amount respectively carries out room temperature lixiviate, and total immersion carries 3 times, each 10 hours, merge vat liquor, filter liquor, the filter liquor of 3 times merges, and reclaims ethanol to obtaining medicinal extract without alcohol taste, the ethyl acetate of medicinal extract with 90% after the water suspendible of 2 times amount carries out three extractions, until extraction liquid is colourless, combined ethyl acetate extraction liquid, is concentrated into paste, drying, obtains dry powder; By the dry powder blend obtained respectively.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410564730.4A CN104370661A (en) | 2014-10-22 | 2014-10-22 | Microecological preparation for grain production safety assurance and preparation method thereof |
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| CN201410564730.4A CN104370661A (en) | 2014-10-22 | 2014-10-22 | Microecological preparation for grain production safety assurance and preparation method thereof |
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| CN104370661A true CN104370661A (en) | 2015-02-25 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107739232A (en) * | 2017-09-19 | 2018-02-27 | 武兴战 | A kind of high-activity biological film for carbon resource deposit and preparation method thereof |
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| CN101509013A (en) * | 2008-02-15 | 2009-08-19 | 马兰 | Micro-ecological formulation and preparation method thereof |
| CN101603016A (en) * | 2009-06-30 | 2009-12-16 | 孙建忠 | Live lactobacillus composite ecological microbial agent |
| CN102267847A (en) * | 2011-07-18 | 2011-12-07 | 武兴战 | Raw material composition and preparation method of sustained-release drought-resistant water-retention nutrient |
| CN102898208A (en) * | 2012-09-16 | 2013-01-30 | 浙江天地润珍珠有限公司 | Composite manure water preparation |
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2014
- 2014-10-22 CN CN201410564730.4A patent/CN104370661A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101509013A (en) * | 2008-02-15 | 2009-08-19 | 马兰 | Micro-ecological formulation and preparation method thereof |
| CN101603016A (en) * | 2009-06-30 | 2009-12-16 | 孙建忠 | Live lactobacillus composite ecological microbial agent |
| CN102267847A (en) * | 2011-07-18 | 2011-12-07 | 武兴战 | Raw material composition and preparation method of sustained-release drought-resistant water-retention nutrient |
| CN102898208A (en) * | 2012-09-16 | 2013-01-30 | 浙江天地润珍珠有限公司 | Composite manure water preparation |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107739232A (en) * | 2017-09-19 | 2018-02-27 | 武兴战 | A kind of high-activity biological film for carbon resource deposit and preparation method thereof |
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Application publication date: 20150225 |