CN104364242A - 哌嗪的制备方法 - Google Patents

哌嗪的制备方法 Download PDF

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Publication number
CN104364242A
CN104364242A CN201380029522.8A CN201380029522A CN104364242A CN 104364242 A CN104364242 A CN 104364242A CN 201380029522 A CN201380029522 A CN 201380029522A CN 104364242 A CN104364242 A CN 104364242A
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CN
China
Prior art keywords
reaction
ammonia
catalyst
weight
deoa
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201380029522.8A
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English (en)
Chinese (zh)
Inventor
R·布切迪德
J-P·梅尔德
U·艾贝尔
R·多斯塔莱克
N·沙兰德
B·施泰因
M·约德克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN104364242A publication Critical patent/CN104364242A/zh
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C07D295/023—Preparation; Separation; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
CN201380029522.8A 2012-06-06 2013-05-29 哌嗪的制备方法 Pending CN104364242A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12171084.2 2012-06-06
EP12171084 2012-06-06
PCT/EP2013/061104 WO2013182468A1 (de) 2012-06-06 2013-05-29 Verfahren zur herstellung von piperazin

Publications (1)

Publication Number Publication Date
CN104364242A true CN104364242A (zh) 2015-02-18

Family

ID=48536904

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380029522.8A Pending CN104364242A (zh) 2012-06-06 2013-05-29 哌嗪的制备方法

Country Status (5)

Country Link
EP (1) EP2858978A1 (enExample)
JP (1) JP2015525214A (enExample)
CN (1) CN104364242A (enExample)
IN (1) IN2014DN09263A (enExample)
WO (1) WO2013182468A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111925341A (zh) * 2020-08-11 2020-11-13 山东达民化工股份有限公司 一种哌嗪的制备方法
CN114195738A (zh) * 2021-12-27 2022-03-18 江苏康恒化工有限公司 一种无溶剂合成哌嗪的方法

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IN2014DN10837A (enExample) * 2012-07-13 2015-09-04 Basf Se

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400539A (en) * 1981-09-30 1983-08-23 Union Carbide Corporation Process for the manufacture of ethylenediamine
WO2006114417A2 (de) * 2005-04-26 2006-11-02 Basf Aktiengesellschaft Verfahren zur herstellung von ethylenaminen
CN101489673A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
CN101489979A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
CN101489980A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
US20110137030A1 (en) * 2009-12-03 2011-06-09 Basf Se Catalyst and process for preparing an amine

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL137371C (enExample) 1963-08-02
BE757840A (fr) 1969-10-23 1971-04-22 Basf Ag Procede de preparation d'amines a partir d'alcools
NL169595C (nl) 1970-05-21 1982-08-02 Shell Int Research Werkwijze voor de bereiding van aminen en van smeerolien en vloeibare motorbrandstoffen die deze bevatten.
DE3611230A1 (de) 1986-04-04 1987-10-08 Basf Ag Polybutyl- und polyisobutylamine, verfahren zu deren herstellung und diese enthaltende kraft- und schmierstoffzusammensetzungen
DE19859776B4 (de) 1998-12-23 2008-06-19 Basf Se Verfahren zur Herstellung von Aminen
DE10153411A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
DE10153410A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
US7196033B2 (en) 2001-12-14 2007-03-27 Huntsman Petrochemical Corporation Advances in amination catalysis
EP2225030B1 (de) 2007-12-21 2012-04-18 Basf Se Verfahren zur herstellung eines amins
CN101903095B (zh) 2007-12-21 2013-07-10 巴斯夫欧洲公司 制备胺的方法
US8293945B2 (en) 2007-12-21 2012-10-23 Basf Se Method for producing an amine
SG174379A1 (en) 2009-04-08 2011-10-28 Basf Se Method for producing 1,6-hexanediol by hydrogenation of oligo- and polyesters
HUE026565T2 (hu) 2010-06-15 2016-06-28 Basf Se Eljárás egy ciklikus tercier metil-amin elõállítására
EP2627644B1 (de) 2010-10-14 2014-12-10 Basf Se Verfahren zur herstellung eines zyklischen tertiären amins
CN102304101A (zh) 2011-05-26 2012-01-04 绍兴兴欣化工有限公司 哌嗪与n-烷基哌嗪联产工艺

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400539A (en) * 1981-09-30 1983-08-23 Union Carbide Corporation Process for the manufacture of ethylenediamine
WO2006114417A2 (de) * 2005-04-26 2006-11-02 Basf Aktiengesellschaft Verfahren zur herstellung von ethylenaminen
CN101489673A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
CN101489979A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
CN101489980A (zh) * 2006-07-14 2009-07-22 巴斯夫欧洲公司 生产胺的方法
US20110137030A1 (en) * 2009-12-03 2011-06-09 Basf Se Catalyst and process for preparing an amine

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111925341A (zh) * 2020-08-11 2020-11-13 山东达民化工股份有限公司 一种哌嗪的制备方法
CN114195738A (zh) * 2021-12-27 2022-03-18 江苏康恒化工有限公司 一种无溶剂合成哌嗪的方法

Also Published As

Publication number Publication date
JP2015525214A (ja) 2015-09-03
EP2858978A1 (de) 2015-04-15
WO2013182468A1 (de) 2013-12-12
IN2014DN09263A (enExample) 2015-07-10

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Effective date of abandoning: 20171222