CN104356832A - Preparation method of flexible gigging natural stone paint - Google Patents

Preparation method of flexible gigging natural stone paint Download PDF

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Publication number
CN104356832A
CN104356832A CN201410697335.3A CN201410697335A CN104356832A CN 104356832 A CN104356832 A CN 104356832A CN 201410697335 A CN201410697335 A CN 201410697335A CN 104356832 A CN104356832 A CN 104356832A
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CN
China
Prior art keywords
raw
stirring
flexible
mineral varnish
true mineral
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410697335.3A
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Chinese (zh)
Inventor
刘志伟
赵雅文
孙晨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
First New Material Science & Technology Development Co Ltd
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First New Material Science & Technology Development Co Ltd
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Filing date
Publication date
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Priority to CN201410697335.3A priority Critical patent/CN104356832A/en
Publication of CN104356832A publication Critical patent/CN104356832A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/28Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

Abstract

The invention discloses a preparation method of a flexible gigging natural stone paint, belonging to the field of preparation of paints. The method uses a pure acrylic emulsion, an assistant, a thickener, water and colored sand as the raw materials and uses a mixing plant with a dispersion disk for treatment. The method comprises the following steps: adding the raw material water into a reaction kettle of the mixing plant; adding the raw material assistant, and dispersing by stirring; after uniformly dispersing the assistant, adding the raw material pure acrylic emulsion, and dispersing by stirring; after uniformly dispersing the pure acrylic emulsion, adding the raw material thickener, and stirring to obtain a slurry; and adding the raw material colored sand into the slurry, and stirring uniformly to obtain the flexible gigging natural stone paint. The specific amounts of raw materials are added in the specific sequence, and dispersed by stirring to obtain the paint. Since the raw materials are reasonably proportioned, the prepared paint has the advantages of favorable flexibility and favorable stone-simulating effect, can well repair the crack in the base layer, and achieves the effect of compact and persistent natural stone.

Description

The preparation method of the true mineral varnish of flexible plucking
Technical field
The present invention relates to paint vehicle production field, particularly relate to a kind of preparation method of the true mineral varnish of flexible plucking for external wall.
Background technology
Along with the Great span of China's economic, development of real estate also reaches unprecedented growth height, in mega structure exterior wall market, stone materials effect is widely accepted because decorating elegant, for a long time by high-end construction market as first-selected finishing material, but stone material also has a lot of deficiency while having so many advantages, specific as follows: 1, stone material deadweight is very heavy, this is very high to basic level requirement, and basic unit's cost can be made so greatly to improve.
(1) good stone material price is very high, and every square meter is mostly more than 200 yuan/square meter, and the lower stone material quality of price is very poor.
(2) very heavyly there is potential safety hazard because of deadweight in stone material always, along with various places Highrise buildings stone material drops the report successively of the event of hurting sb.'s feelings, the security of stone material has been pulled to the teeth of the storm place, and a lot of local government has ordered regulation exterior wall not use stone material.
(3) stone material is because being pure resource products, and along with continuous exploitation, product can be fewer and feweri, more can aggravate the raising of price like this.
(4) stone material is because being that pure natural generates, and the colour consistency of stone material is difficult to be consistent, and finally there will be shade and differs.
The how could decorative effect of existing elegant, can safety be ensured again? so imitative stone materials product arises at the historic moment, imitative stone material product not only has very high emulation to stone material, and safety and environmental protection, price is well below stone material, the release of imitative stone material product is accepted by middle and high end client rapidly, and application prospect is very optimistic.
Summary of the invention
Based on the problem existing for above-mentioned prior art, the invention provides a kind of can cost far below building stones, have very high emulation and the preparation method of the true mineral varnish of flexible plucking of safety and environmental protection to stone material.
For solving the problems of the technologies described above, the invention provides the preparation method of the true mineral varnish of a kind of flexible plucking, by mass percentage, pure-acrylic emulsion with 38% ~ 40%, the auxiliary agent of 1% ~ 1.5%, the thickening material of 0.5% ~ 1%, the water of 5% ~ 10% and 50% ~ 55% color sand be raw material, adopt the whipping device with dispersion impeller to process, comprise the following steps:
The water in described raw material is added in the reactor of described whipping device;
The auxiliary agent added in described raw material carries out dispersed with stirring;
The pure-acrylic emulsion added after described auxiliary agent is uniformly dispersed in described raw material carries out dispersed with stirring;
After described pure-acrylic emulsion is uniformly dispersed, the thickening material added in described raw material obtains slurry after stirring;
Namely the true mineral varnish of flexible plucking is obtained after the color sand added in described slurry in described raw material stirs.
Beneficial effect of the present invention is: be raw material by the pure-acrylic emulsion of specific consumption, auxiliary agent, thickening material, water and color sand, the true mineral varnish of flexible plucking is defined by specific addition sequence dispersion stirring, because the usage ratio of its pure-acrylic emulsion, auxiliary agent, thickening material, water and color sand is reasonable, the paint vehicle degree of flexibility made is good and have preferably imitative stone effect, be specially adapted to exterior wall and imitate stone plucking, can well make up basic unit's crackle, reach fine and close, permanent as new true stone effect.
Embodiment
Be clearly and completely described the technical scheme in the embodiment of the present invention below, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on embodiments of the invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to protection scope of the present invention.
Below in conjunction with specific embodiment, method of the present invention is described further.
The embodiment of the present invention provides the preparation method of the true mineral varnish of a kind of flexible plucking, by mass percentage, pure-acrylic emulsion with 38% ~ 40%, the auxiliary agent of 1% ~ 1.5%, the thickening material of 0.5% ~ 1%, the water of 5% ~ 10% and 50% ~ 55% color sand be raw material, adopt the whipping device with dispersion impeller to process, comprise the following steps:
The water in described raw material is added in the reactor of described whipping device;
The auxiliary agent added in described raw material carries out dispersed with stirring;
The pure-acrylic emulsion added after described auxiliary agent is uniformly dispersed in described raw material carries out dispersed with stirring;
After described pure-acrylic emulsion is uniformly dispersed, the thickening material added in described raw material obtains slurry after stirring;
Namely the true mineral varnish of flexible plucking is obtained after the color sand added in described slurry in described raw material stirs.
In aforesaid method, the mixing speed that the auxiliary agent added in described raw material carries out dispersed with stirring is 400 revs/min;
Auxiliary agent adds with the speed of 50 kg/minute, and mixing speed is 600 revs/min;
Thickening material adds with the speed of 10 kg/minute, and mixing speed is 800 revs/min, and the churning time after thickening material adds is 5 ~ 10 minutes;
Color sand adds with the speed of 200 kg/minute, and stirring velocity is 600 revs/min.
In aforesaid method, state auxiliary agent and adopt: pH value regulator, film coalescence aid and dispersion agent.Thickening material adopts: any one or several in polyurethane associative thickener, alkali swelling type thickening material, Mierocrystalline cellulose.Color sand adopts the color sand of 40-120#.
The method can preparation cost low, the high and true mineral varnish of flexible plucking that the feature of environmental protection is good of imitative stone emulation property, well can make up basic unit's crackle, reach fine and close, permanent as new true stone effect.
Concrete, the step that the present invention prepares the true mineral varnish of flexible plucking is:
The water in raw material is added in the reactor of whipping device;
The auxiliary agent in raw material is added successively under 400 revs/min of states;
Add the pure-acrylic emulsion in raw material with the speed of 50 kg/minute after auxiliary agent is uniformly dispersed, can when starting to add pure-acrylic emulsion, mixing speed with regard to raising whipping device is 600 revs/min, just completes whipping process, carry out subsequent disposal after pure-acrylic emulsion adds completely;
Slowly add the thickening material in raw material after emulsion dispersion is even with the speed of 10 kg/minute, the mixing speed improving whipping device after adding thickening material is 800 revs/min, and churning time is 5 to 10 minutes, obtains slurry after stirring;
In slurry after above-mentioned obtaining (solid content generally obtaining slurry is 63%), the color sand in raw material is slowly added with the speed of 200 kg/minute, the rotating speed improving whipping device is 600 revs/min, namely obtains the true mineral varnish of flexible plucking after stirring.
The true mineral varnish of flexible plucking that the present embodiment obtains can be used in exterior wall construction, and construction technology is as follows:
(1) scope of application: be applicable to all kinds of skin faces such as concrete, plaster base, heat insulation base layer decoration.
(2) process characteristic:
(21) flexible plucking true mineral varnish technique is a kind of effect exactly liking lithotome, has natural colour, gives elegance, harmony, serious aesthetic feeling.Current more building all have employed true mineral varnish and fits up as the facing of top-grade building thing.
(22) the true mineral varnish of flexible plucking have water-fast, alkaline-resisting, nontoxic, tasteless, bonding force is strong, the advantage such as will never fade; True mineral varnish has good sticking power; True mineral varnish can extend the work-ing life of buildings.
(23) in heat insulation base layer, adopt true mineral varnish to replace stone decoration effect, there is easy construction, save time, safety, economy, the plurality of advantages such as environmental protection.
(3) coating structure:
Form the coating that flexible plucking imitates stone effect.
(4) preparation of construction
(41) auxiliary products:
Sequence number Name of product Effect
1 Flexible repairing material Make up basic unit's fine defects
2 Exterior wall alkali-resistant primer (transparent) Close body of wall alkalescence, improve ply adhesion
3 Environmental-protection decorative priming paint Partitioning slot color
4 The true mineral varnish of flexible plucking prepared by the present invention Decoration function
5 Environmental protection coating varnish Provide protection
Note: when basic unit's deviation is larger, by last process to basic unit carry out repairing levelling or adopt polymkeric substance plastering mortar (BS202/FBJ-02) carry out levelling finishing.
(42) major mechanical and service tool:
Air compressor machine and supporting pipe joint, funnel spray gun, spray gun, angle grinding machine, wire brush, trowel (scraper plate), operate on, thick stick chi, box chi, line bag (ink fountain), hair roller, brush, easy horizon equipment, thickness sand paper etc.
(5) operating condition:
(51) before base treatment, body of wall needs the maintenance of certain hour, and the curing time in general new cement wall surface winter is 28 days, and the curing time in summer is 14 days.Maintenance is less than 10 to the pH value of basic unit, after water ratio is less than 10%, then carries out processing base level.
(52) basic unit inspects for acceptance: the permissible variation (mm) of GB50210-2001 plastering quality and the method for inspection.
(53) basic unit should clean, surperficial free from dust, without laitance, oil stains-less, without rust staining, without mildew, without salt precipitate with without foreign material such as mosses.
(54) door and window installs by design requirements, and by checking and accepting.
(55) complete the installation of rainwater pipe clamp, equipment hole, pipeline, and by floating for hole surrounding sand-cement slurry, all metopes need dry.
(56) adopt double shelf or nacelle construction, national security code requirement should be met.
(57) before construction, protection is blocked to the position of not constructing.
(6) operating procedure:
(61) technical process:
Metope base treatment → scrape (smearing) Special flexible repairs material 1-2 time → roller coating exterior wall alkali-resistant primer, 1 time → roller coating environmental-protection decorative priming paint, 1-2 time → snap the line lattice, Continuous pressing device for stereo-pattern → true mineral varnish of flexible plucking of constructing, 2 times → spraying environmental protection coating varnish, 1-2 time.
(62) base treatment:
Thoroughly should remove the basic unit of loose, peeling, hollowing, efflorescence before base treatment, remove the pollutents such as floating ash, greasy dirt.
(63) blade coating Special flexible repairs material:
Special flexible is repaired material and is divided twice to construct, and first local is levelling, finishing door-window opening and negative and positive angle, second granted full.A blade coating thickness is no more than 1.0mm, and per pass is not less than 5 hours (when 25 DEG C) interval time.To local suitably (25 DEG C, dry 4-6 hour) polishing finishing after per pass putty blade coating, after polishing, remove floating ash.
Special flexible repairs material needs abundant dry solidification, is less than 10, after water ratio is less than 10%, can carries out the construction of next process to pH value.
(64) roller coating alkali-resistant sealing primer:
After the abundant dry solidification of putty layer, roller coating alkali-resistant sealing primer one time, requires that brushing evenly, never can have holiday phenomenon.Forbid being watered during the construction of exterior wall alkali-resistant primer, guarantee that priming paint is not polluted simultaneously.
(65) roller coating environmental-protection decorative priming paint:
Environmental-protection decorative prime must be even, can not excessively be watered, and the water generally can converting 5 ~ 10% is constructed.Imitative brickwork skill basecoat color used can select the color of dividing joint, reduces the fussy degree of technique.
(66) to construct the true mineral varnish of flexible plucking:
After the drying of environmental-protection decorative priming paint, the true mineral varnish of the flexible plucking of trowelling one time, the true mineral varnish of the flexible plucking of even roller coating after dry, notes, after material is evenly spread out, finally rolling towards a direction rewinding with plucking, avoiding causing grow diming phenomenon because of the equation of light.
Twice construction of the flexible true mineral varnish of plucking, last takes adhesive tape off as early as possible all over after plucking.
(67) environmental protection coating varnish is sprayed:
After the true mineral varnish of flexible plucking parches completely (general fine day at least keeps 3 days), environmental protection coating varnish can be sprayed, keep the flow of viscosity, air pressure, material consistent during construction, note pre-sag prevention phenomenon.General point 1-2, all over construction, is spaced apart 4 hours.
(7) construction precautions:
(71) label of auxiliary products should be checked before using, confirm errorless after can use.
(72) material of uncapping must be tight by bung after finishing using at every turn, and require to be finished in 12 hours.
(73) should do before constructing and carry out materials plan according to the scope of operation, reduce the supply of material batch, same face wall must use the true mineral varnish of same batch, to ensure consistency of colour.
(74) note abnormalities in construction process, must feed back in time and stop the construction of this road technique.
(75) linking of construction operation section should remain on dividing joint or negative and positive angle place, requires reasonable arrangement personnel and facility to the metope without lattice, keeps wet and touches wet linking, avoid occurring connecing stubble.To constructing, finished product position is blocked, and avoids crossed contamination.
(76) when the true mineral varnish of flexible plucking is constructed, require that metope temperature is not less than 5 DEG C, not higher than 40 DEG C, free air temperature is not higher than 35 DEG C (avoiding the wall construction of direct sunlight summer), humidity is not higher than 80%, wind-force is less than level Four, pay close attention to Changes in weather, rainy day or the weather being about to rain forbid construction.
(77) the true mineral varnish of flexible plucking store should more than 0 DEG C, less than 40 DEG C, shady and coolly dryly to locate, avoid sunlight directly to shine.
(78) other subitem finished product protection should be noted when the true mineral varnish of flexible plucking is constructed, prevent the pollution that cross-operation causes.
(79) painting tool should clean up with finishing in time and keep properly.
The above; be only the present invention's preferably embodiment, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.

Claims (5)

1. the preparation method of the true mineral varnish of flexible plucking, it is characterized in that, by mass percentage, pure-acrylic emulsion with 38% ~ 40%, the auxiliary agent of 1% ~ 1.5%, the thickening material of 0.5% ~ 1%, the water of 5% ~ 10% and 50% ~ 55% color sand be raw material, adopt the whipping device with dispersion impeller to process, comprise the following steps:
The water in described raw material is added in the reactor of described whipping device;
The auxiliary agent added in described raw material carries out dispersed with stirring;
The pure-acrylic emulsion added after described auxiliary agent is uniformly dispersed in described raw material carries out dispersed with stirring;
After described pure-acrylic emulsion is uniformly dispersed, the thickening material added in described raw material obtains slurry after stirring;
Namely the true mineral varnish of flexible plucking is obtained after the color sand added in described slurry in described raw material stirs.
2. the preparation method of the true mineral varnish of flexible plucking according to claim 1, is characterized in that,
The mixing speed that the described auxiliary agent added in described raw material carries out dispersed with stirring is 400 revs/min;
Described auxiliary agent adds with the speed of 50 kg/minute, and mixing speed is 600 revs/min;
Described thickening material adds with the speed of 10 kg/minute, and mixing speed is 800 revs/min, and it is 5 ~ 10 minutes that thickening material adds rear churning time;
Described color sand adds with the speed of 200 kg/minute, and stirring velocity is 600 revs/min.
3. the preparation method of the true mineral varnish of flexible plucking according to claim 1 and 2, is characterized in that, described auxiliary agent adopts: film coalescence aid, pH value regulator and dispersion agent.
4. the preparation method of the true mineral varnish of flexible plucking according to claim 1 and 2, is characterized in that, described thickening material adopts: any one or several in Mierocrystalline cellulose, polyurethane thickener, alkali swelling type thickening material.
5. the preparation method of the true mineral varnish of flexible plucking according to claim 1 and 2, is characterized in that, described color sand adopts the color sand of 40-120#.
CN201410697335.3A 2014-11-26 2014-11-26 Preparation method of flexible gigging natural stone paint Pending CN104356832A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410697335.3A CN104356832A (en) 2014-11-26 2014-11-26 Preparation method of flexible gigging natural stone paint

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Application Number Priority Date Filing Date Title
CN201410697335.3A CN104356832A (en) 2014-11-26 2014-11-26 Preparation method of flexible gigging natural stone paint

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104789074A (en) * 2015-05-06 2015-07-22 武汉德美涂料股份有限公司 Novel natural stone paint and preparation method thereof
CN105111872A (en) * 2015-09-11 2015-12-02 三棵树涂料股份有限公司 Elastic galling maishi paint and preparing method thereof
CN106752532A (en) * 2016-12-29 2017-05-31 三棵树涂料股份有限公司 A kind of antifouling weather-resistant type external wall elastic plucking paint and preparation method thereof
CN106866025A (en) * 2017-03-03 2017-06-20 富思特新材料科技发展股份有限公司 True mineral varnish of inorganic silicon and preparation method thereof
CN109825153A (en) * 2019-03-07 2019-05-31 南京淳彩建材有限公司 A kind of weather-proof lacquer and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102408203A (en) * 2011-08-18 2012-04-11 上海典佳节能环保科技有限公司 Preparation method of coating type natural color sand flexible face brick and construction technology thereof
CN103602197A (en) * 2013-11-29 2014-02-26 江门市华石涂料有限公司 Stone-like paint and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102408203A (en) * 2011-08-18 2012-04-11 上海典佳节能环保科技有限公司 Preparation method of coating type natural color sand flexible face brick and construction technology thereof
CN103602197A (en) * 2013-11-29 2014-02-26 江门市华石涂料有限公司 Stone-like paint and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104789074A (en) * 2015-05-06 2015-07-22 武汉德美涂料股份有限公司 Novel natural stone paint and preparation method thereof
CN105111872A (en) * 2015-09-11 2015-12-02 三棵树涂料股份有限公司 Elastic galling maishi paint and preparing method thereof
CN106752532A (en) * 2016-12-29 2017-05-31 三棵树涂料股份有限公司 A kind of antifouling weather-resistant type external wall elastic plucking paint and preparation method thereof
CN106866025A (en) * 2017-03-03 2017-06-20 富思特新材料科技发展股份有限公司 True mineral varnish of inorganic silicon and preparation method thereof
CN109825153A (en) * 2019-03-07 2019-05-31 南京淳彩建材有限公司 A kind of weather-proof lacquer and preparation method thereof

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Application publication date: 20150218

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