CN104322576A - Grape downy mildew prevention and treatment medicine - Google Patents

Grape downy mildew prevention and treatment medicine Download PDF

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Publication number
CN104322576A
CN104322576A CN201410539059.8A CN201410539059A CN104322576A CN 104322576 A CN104322576 A CN 104322576A CN 201410539059 A CN201410539059 A CN 201410539059A CN 104322576 A CN104322576 A CN 104322576A
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parts
downy mildew
sodium
garpe
pesticide control
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CN201410539059.8A
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Chinese (zh)
Inventor
李燕
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JURONG MANYUANCHUN FAMILY FARM
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JURONG MANYUANCHUN FAMILY FARM
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Abstract

The invention discloses a grape downy mildew prevention and treatment medicine. The medicine is prepared by using the following components, by weight, 5 parts of sodium dichloroisocyanurate, 2-8 parts of eugenol, 2-6 parts of myclobutanil, 1-5 parts of kresoxim methyl, 20-30 parts of Fructus Cnidii, 15-25 parts of mulberry leaf, 12-20 parts of Perilla frutescens, 10-20 parts of Artemisia carvifolia, 0.2-0.6 parts of potassium nitrate, 40-60 parts of chitosan, 0.2-0.8 parts of carboxymethylcellulose sodium and 0.03-0.07 parts of Tween 80. Compared with medicines in the prior art, the grape downy mildew prevention and treatment medicine prepared in the invention has the advantages of protruding effect, long persistent period, reduction of the use frequency, raw material saving and environmental pollution reduction.

Description

A kind of downy mildew of garpe pesticide control
Technical field
The present invention relates to a kind of downy mildew of garpe pesticide control, be applied to agriculture field.
Background technology
Downy mildew of garpe is a kind of global grape disease.All there is distribution each viny region of China, and especially occurring general in rainy humid area, is one of grape Major Diseases.Downy mildew of garpe main harm blade, also can infect the tender tissues such as young sprout young fruit.Blade is killed, the fleck that nascent faint yellow water stain shape blur margin is clear, expands as the irregular shape of brown or polygonal scab gradually later, and number spot is connected and becomes the large spot of irregular shape.During wet weather, produce white downy mildew shape thing in the scab back side, i.e. the sporangiophore of germ and sporangium.When falling ill serious, sick leaf is early withered caducous.The tender tip is injured, and forms water soaked spots, after become the scab of brown slightly depression, time moist, scab also produces white downy mildew.Young sprout distortion time seriously ill, growth stops, even withered.Tendril, cob, petiole sometimes also can be killed, and its symptom is similar to the tender tip.Young fruit is killed, fades in sick portion, and hardening sagging, the white downy mildew of upper life, very easy atrophy comes off.Be injured when fruit grain is medium-sized, sick portion brown is to dark-coloured, and soft corruption is caducous.No longer infect after fruit color.
At present, the pesticide control of downy mildew of garpe is of a great variety, mostly needs repeatedly to use different periods in morbidity, not only loaded down with trivial details, and repeatedly uses increase environmental pollution, and effect is undesirable.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the invention provides a kind of downy mildew of garpe pesticide control.
Technical scheme: for achieving the above object, the invention provides a kind of downy mildew of garpe pesticide control, its primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 2-8 part, nitrile bacterium azoles 2-6 part, kresoxim-methyl 1-5 part,
Frutus cnidii 20-30 part, mulberry leaf 15-25 part, purple perilla 12-20 part, sweet wormwood 10-20 part, potassium nitrate 0.2-0.6 part,
Shitosan 40-60 part, sodium carboxymethylcellulose 0.2-0.8 part, Tween 80 0.03-0.07 part.
As preferably, described downy mildew of garpe pesticide control primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 4-6 part, nitrile bacterium azoles 3-5 part, kresoxim-methyl 2-4 part,
Frutus cnidii 22-28 part, mulberry leaf 18-22 part, purple perilla 14-18 part, sweet wormwood 12-18 part, potassium nitrate 0.3-0.5 part,
Shitosan 45-55 part, sodium carboxymethylcellulose 0.4-0.6 part, Tween 80 0.04-0.06 part.
Preferred as another kind, described downy mildew of garpe pesticide control primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 5 parts, nitrile bacterium azoles 4 parts, kresoxim-methyl 3 parts,
Frutus cnidii 25 parts, 20 parts, mulberry leaf, purple perilla 16 parts, sweet wormwood 15 parts, 0.4 part, potassium nitrate,
Shitosan 50 parts, sodium carboxymethylcellulose 0.5 part, Tween 80 0.05 part.
Preferred as another kind, in described pesticide control, the concentration of isocyanide dichloride urea acid sodium is 4-8% (weight ratio).
Preferred as another kind, described downy mildew of garpe pesticide control is mainly made by following steps:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 6-10 times of volume, heating boils extraction twice, each 1-3 hour, and merge extract, being concentrated into 30 DEG C of relative densities is 1.04-1.10, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 40-50 DEG C of heating for dissolving, obtains chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 4000-6000r/min high speed dispersion 10-20 minute, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
Beneficial effect: relative to prior art, the downy mildew of garpe pesticide control of gained of the present invention, drug effect is given prominence to, and the lasting period is long, and can reduce the access times of medicine, economizes in raw materials, and reduces environmental pollution.
Embodiment
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1:
Prescription:
Isocyanide dichloride urea acid sodium 5g, eugenol 2g, nitrile bacterium azoles 2g, kresoxim-methyl 1g, frutus cnidii 20g, mulberry leaf 15g,
Purple perilla 12g, sweet wormwood 10g, potassium nitrate 0.2g, shitosan 40g, sodium carboxymethylcellulose 0.2g, Tween 80 0.03g.
Preparation method:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 6 times of volumes, heating boils extraction twice, each 1 hour, and merge extract, being concentrated into 30 DEG C of relative densities is 1.04, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 40 DEG C of heating for dissolving, obtain chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 4000r/min high speed dispersion 10 minutes, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
In gained pesticide control, the concentration of isocyanide dichloride urea acid sodium is 4% (weight ratio).
Embodiment 2:
Prescription:
Isocyanide dichloride urea acid sodium 5g, eugenol 8g, nitrile bacterium azoles 6g, kresoxim-methyl 5g, frutus cnidii 30g, mulberry leaf 25g,
Purple perilla 20g, sweet wormwood 20g, potassium nitrate 0.6g, shitosan 60g, sodium carboxymethylcellulose 0.8g, Tween 80 0.07g.
Preparation method:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 10 times of volumes, heating boils extraction twice, each 3 hours, and merge extract, being concentrated into 30 DEG C of relative densities is 1.10, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 50 DEG C of heating for dissolving, obtain chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 6000r/min high speed dispersion 20 minutes, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
In gained pesticide control, the concentration of isocyanide dichloride urea acid sodium is 8% (weight ratio).
Embodiment 3:
Prescription:
Isocyanide dichloride urea acid sodium 5g, eugenol 5g, nitrile bacterium azoles 4g, kresoxim-methyl 3g, frutus cnidii 25g, mulberry leaf 20g,
Purple perilla 16g, sweet wormwood 15g, potassium nitrate 0.4g, shitosan 50g, sodium carboxymethylcellulose 0.5g, Tween 80 0.05g.
Preparation method:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 8 times of volumes, heating boils extraction twice, each 2 hours, and merge extract, being concentrated into 30 DEG C of relative densities is 1.07, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 45 DEG C of heating for dissolving, obtain chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 5000r/min high speed dispersion 15 minutes, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
In gained pesticide control, the concentration of isocyanide dichloride urea acid sodium is 6% (weight ratio).
Embodiment 4:
Prescription:
Isocyanide dichloride urea acid sodium 5g, eugenol 4g, nitrile bacterium azoles 3g, kresoxim-methyl 2g, frutus cnidii 22g, mulberry leaf 18g,
Purple perilla 14g, sweet wormwood 12g, potassium nitrate 0.3g, shitosan 45g, sodium carboxymethylcellulose 0.4g, Tween 80 0.04g.
Preparation method:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 7 times of volumes, heating boils extraction twice, each 2 hours, and merge extract, being concentrated into 30 DEG C of relative densities is 1.05, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 42 DEG C of heating for dissolving, obtain chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 4500r/min high speed dispersion 12 minutes, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
In gained pesticide control, the concentration of isocyanide dichloride urea acid sodium is 5% (weight ratio).
Embodiment 5:
Prescription:
Isocyanide dichloride urea acid sodium 5g, eugenol 6g, nitrile bacterium azoles 5g, kresoxim-methyl 4g, frutus cnidii 28g, mulberry leaf 22g,
Purple perilla 18g, sweet wormwood 18g, potassium nitrate 0.5g, shitosan 55g, sodium carboxymethylcellulose 0.6g, Tween 80 0.06g.
Preparation method:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 9 times of volumes, heating boils extraction twice, each 2 hours, and merge extract, being concentrated into 30 DEG C of relative densities is 1.09, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 48 DEG C of heating for dissolving, obtain chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 5500r/min high speed dispersion 18 minutes, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
In gained pesticide control, the concentration of isocyanide dichloride urea acid sodium is 7% (weight ratio).
Experimental example downy mildew of garpe controlling experiment
In certain grape experiment field, get 5 pieces of areas and be 20m 2experiment field, be labeled as contrast 1 group respectively, contrast 2 groups, embodiment 3,4 and 5 groups, time of application be downy mildew of garpe morbidity mid-early stage.
Contrast 1 group and spray Ao Like frost Bel (50ml is watered 30 jin), only spray once;
Contrast 2 groups and spray Ao Like frost Bel (50ml is watered 30 jin), spray three times, sprayed once every 5 days;
Embodiment 3,4 and 5 groups sprays the embodiment of the present invention 3,4 and 5 gained pesticide control (being diluted to same concentrations) respectively, only sprays once.
All the other conditions of each piece of experimental field are identical.
Fertilizing method and regular maintenance management carries out all according to a conventional method, finally more each group after medicine 7 days, 14 days and 21 days time, to the control efficiency of downy mildew, the results are shown in Table 1.
Table 1 respectively organizes medicament to the control efficiency of downy mildew
Note: with contrast 1 group and compare, * P<0.05;
Can be drawn by upper table 1, compared with contrast 1 group, namely with only use compared with Yi Ao Like frost Bel, gained pesticide control of the present invention is used once, after medicine, the preventive effect of 7 days, 14 days and 21 days is significantly increased, and do not reduce significantly, show that medicament drug effect of the present invention is given prominence to, the lasting period is long.
Compared with contrast 2 groups, namely with use compared with three Ao Like frost Bels, gained pesticide control of the present invention, suitable to the control efficiency of downy mildew of garpe.Therefore, pesticide control of the present invention is only used once in downy mildew of garpe morbidity mid-early stage, can reach the effect that Ao Like frost Bel uses three times.So medicament of the present invention can reduce the access times of medicine, economizes in raw materials, and environmental pollution can be reduced.

Claims (5)

1. a downy mildew of garpe pesticide control, is characterized in that, its primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 2-8 part, nitrile bacterium azoles 2-6 part, kresoxim-methyl 1-5 part,
Frutus cnidii 20-30 part, mulberry leaf 15-25 part, purple perilla 12-20 part, sweet wormwood 10-20 part, potassium nitrate 0.2-0.6 part,
Shitosan 40-60 part, sodium carboxymethylcellulose 0.2-0.8 part, Tween 80 0.03-0.07 part.
2. downy mildew of garpe pesticide control according to claim 1, is characterized in that, its primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 4-6 part, nitrile bacterium azoles 3-5 part, kresoxim-methyl 2-4 part,
Frutus cnidii 22-28 part, mulberry leaf 18-22 part, purple perilla 14-18 part, sweet wormwood 12-18 part, potassium nitrate 0.3-0.5 part,
Shitosan 45-55 part, sodium carboxymethylcellulose 0.4-0.6 part, Tween 80 0.04-0.06 part.
3. downy mildew of garpe pesticide control according to claim 1, is characterized in that, its primarily of following weight ratio component made by:
Isocyanide dichloride urea acid 5 parts, sodium, eugenol 5 parts, nitrile bacterium azoles 4 parts, kresoxim-methyl 3 parts,
Frutus cnidii 25 parts, 20 parts, mulberry leaf, purple perilla 16 parts, sweet wormwood 15 parts, 0.4 part, potassium nitrate,
Shitosan 50 parts, sodium carboxymethylcellulose 0.5 part, Tween 80 0.05 part.
4. downy mildew of garpe pesticide control according to claim 1, is characterized in that, in described pesticide control, the concentration of isocyanide dichloride urea acid sodium is 4-8% (weight ratio).
5. the downy mildew of garpe pesticide control according to any one of claim 1-4, is characterized in that, they are mainly made by following steps:
(1) get frutus cnidii, mulberry leaf, purple perilla and sweet wormwood, clean, add the water of 6-10 times of volume, heating boils extraction twice, each 1-3 hour, and merge extract, being concentrated into 30 DEG C of relative densities is 1.04-1.10, obtains total extract;
(2) shitosan joins in a certain amount of pure water, and 40-50 DEG C of heating for dissolving, obtains chitosan solution, insulation, for subsequent use;
(3) get the acid of isocyanide dichloride urea sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80, mix with above-mentioned total extract and chitosan solution, 4000-6000r/min high speed dispersion 10-20 minute, obtains dispersion liquid;
(4) above-mentioned dispersion liquid is placed and is spent the night, and gets supernatant, adds potassium nitrate, dissolves, and mixing, to obtain final product.
CN201410539059.8A 2014-10-13 2014-10-13 Grape downy mildew prevention and treatment medicine Pending CN104322576A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104982465A (en) * 2015-07-08 2015-10-21 杨君 Compound for preventing white peony root leaf mould
CN105010436A (en) * 2015-06-26 2015-11-04 安徽禾众农业科技有限公司 Grape downy mildew prevention and control bacteriostat, and preparation method and application thereof
CN105123798A (en) * 2015-07-28 2015-12-09 魏琦 Method for preventing and treating loquat gray spot
CN108887293A (en) * 2018-07-24 2018-11-27 句容市茅山镇介文葡萄专业合作社 A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof
CN109315409A (en) * 2018-10-30 2019-02-12 张宗斌 The pharmaceutical composition for preventing and treating downy mildew of garpe

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101507433A (en) * 2008-11-10 2009-08-19 江苏省农业科学院 Compound bactericide capable of preventing and controlling grape downy mildew
CN101971812A (en) * 2010-11-08 2011-02-16 陕西汤普森生物科技有限公司 Eugenol-containing germicidal composition
CN103583521A (en) * 2012-08-14 2014-02-19 陕西美邦农药有限公司 Efficient sterilization composition
CN104012580A (en) * 2014-04-16 2014-09-03 辽宁农业职业技术学院 Traditional Chinese medicine preparation for preventing and treating plant downy mildew and preparation method of preparation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101507433A (en) * 2008-11-10 2009-08-19 江苏省农业科学院 Compound bactericide capable of preventing and controlling grape downy mildew
CN101971812A (en) * 2010-11-08 2011-02-16 陕西汤普森生物科技有限公司 Eugenol-containing germicidal composition
CN103583521A (en) * 2012-08-14 2014-02-19 陕西美邦农药有限公司 Efficient sterilization composition
CN104012580A (en) * 2014-04-16 2014-09-03 辽宁农业职业技术学院 Traditional Chinese medicine preparation for preventing and treating plant downy mildew and preparation method of preparation

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105010436A (en) * 2015-06-26 2015-11-04 安徽禾众农业科技有限公司 Grape downy mildew prevention and control bacteriostat, and preparation method and application thereof
CN104982465A (en) * 2015-07-08 2015-10-21 杨君 Compound for preventing white peony root leaf mould
CN105123798A (en) * 2015-07-28 2015-12-09 魏琦 Method for preventing and treating loquat gray spot
CN108887293A (en) * 2018-07-24 2018-11-27 句容市茅山镇介文葡萄专业合作社 A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof
CN109315409A (en) * 2018-10-30 2019-02-12 张宗斌 The pharmaceutical composition for preventing and treating downy mildew of garpe

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Application publication date: 20150204