CN109265250A - A kind of preparation method of fruit tree antifreezing agent - Google Patents

A kind of preparation method of fruit tree antifreezing agent Download PDF

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Publication number
CN109265250A
CN109265250A CN201811293331.3A CN201811293331A CN109265250A CN 109265250 A CN109265250 A CN 109265250A CN 201811293331 A CN201811293331 A CN 201811293331A CN 109265250 A CN109265250 A CN 109265250A
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powder
fulvic acid
hours
grams
biochemical fulvic
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卢国政
卢凤纯
卢凤超
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a kind of preparation methods of fruit tree antifreezing agent, it be according to unit of weight proportion following group be grouped as, 13.5% biochemical fulvic acid fine powder, 20% potassium dihydrogen phosphate, 30% brown sugar, 20% xanthan rubber powder, 8% cellulose powder, 2% ginger powder, 2% compound sodium nitrophenolate, 1% zinc sulfate, 2% ferrous sulfate, 1% boric acid, 0.5% sodium permanganate;First ultra-fine grinding will be carried out after mixing evenly after potassium dihydrogen phosphate, brown sugar, zinc sulfate, ferrous sulfate, boric acid, potassium permanganate, compound sodium nitrophenolate, ginger powder compounding, xanthan rubber powder, cellulose powder, biochemical fulvic acid fine powder compounding are mixed into superfines, then it is stirred 10 minutes with blender, it is packed with 500 grams -1000 grams of packaging bag, obtains fruit tree antifreezing agent.The beneficial effects of the present invention are: compatibility is reasonable, simple process, without secondary toxic action.Product category pulvis solid, it is small in size, it is convenient for packed and transported.

Description

A kind of preparation method of fruit tree antifreezing agent
Technical field
The present invention relates to a kind of planting fruit trees industry field, specifically a kind of preparation method of fruit tree antifreezing agent.
Background technique
The planting fruit trees in China, it is wide in variety, area is big, but cold spell in later spring and cold current, freezing colored bone all occur for annual spring Pistil, seriously affects pollination and as a result, the serious time even has no harvest, this is a great problem of orchard worker's puzzlement.
Summary of the invention
Problem to be solved by this invention is that the presence of the polar current for cold spell in spring, and temperature drops to subzero 2-3 DEG C, the flower that a bud just ready to burst The freezing jelly of bone pistil is black, cannot normally pollinate as a result, the severe cold time causes to have no harvest, after spraying fruit tree antifreezing agent provided by the invention 3-5 DEG C of fruit tree cold tolerance can be improved, can effectively solve this universal problem.The present invention provides a kind of fruit tree antifreezing agent Preparation method, the present invention are using 200 times of liquid after this agent dissolution, and 1-2 days implementation branches and leaves flower bones spray before the presence of the polar current, Good maintenance action is played to flower bone pistil, to make fruit tree normally bloom, pollinate, result.This preparation is all made of food-grade Raw material composition, without any toxic side effect, and effectively maintenance nutrition flower bone.Pistil makes fruit tree stable and high yields.
The technical solution of the present invention is as follows: a kind of proportion of fruit tree antifreezing agent is, it is according to the as follows of unit of weight proportion Group is grouped as, 13.5% biochemical fulvic acid fine powder, 20% potassium dihydrogen phosphate, 30% brown sugar, 20% xanthan rubber powder, 8% cellulose powder, 2% ginger powder, 2% compound sodium nitrophenolate, 1% zinc sulfate, 2% ferrous sulfate, 1% boric acid, 0.5% sodium permanganate.
The preparation method of the fruit tree antifreezing agent the following steps are included:
First step, in the following order by 20% potassium dihydrogen phosphate, 30% brown sugar, 1% zinc sulfate, 2% sulphur It is carried out after mixing evenly after sour ferrous iron, 1% boric acid, 0.5% potassium permanganate, 2% compound sodium nitrophenolate, 2% ginger powder compounding Ultra-fine grinding is crushed into 80 targeted fine powders with ultrafine crusher, and the ultra-fine grinding is to use using ultrafine crusher Winnowing type pulverizer is completed, and the machine controls fineness by control air volume;
Second step mixes 20% xanthan rubber powder, 8% cellulose into the 80 mesh superfines that first step obtains Powder, 13.5% biochemical fulvic acid fine powder compounding, then with blender stir 10 minutes, with 500 grams -1000 grams of packaging bag Packaging, obtains fruit tree antifreezing agent.
The biochemical fulvic acid fine powder is extracted after fermenting according to the following component of unit of weight proportion: 53.6% Sawdust, 10% wheat bran, 12% corn flour, 0.8% microelement, 0.6% vitamin, 6% monoammonium phosphate, 6% dregs of beans, 10% soybean oil, 1% strain, the proportion of water are the 55% of the above total weight proportion.
The microelement refers to the single-item combination or any combination of zinc, iron, manganese, boric acid.
The vitamin refer to vitamin B, vitamin C, vitamin D, vitamin E single-item combination or any group It closes.
The strain refer to photosynthetic bacteria, nitrogen-fixing bacteria, ferment bacterium, lactic acid bacteria, bacillus subtilis, bacillus licheniformis, It is phosphobacteria, bacillus megaterium, bacillusmusilaginosiengineering, actinomyces, aspergillus oryzae, aspergillus niger, trichoderma harzianum, muscardine, green Stiff bacterium, Bifidobacterium.
The preparation method of the biochemical fulvic acid fine powder the following steps are included:
One), fermentation process: by 53.6% sawdust, 10% wheat bran, 12% corn flour, 0.8% microelement, 0.6% vitamin, 6% monoammonium phosphate, 6% dregs of beans, 10% soybean oil in carbon-nitrogen ratio 1:25 ratio be uniformly mixed 1% strain is added afterwards, said mixture is packed into ventilative woven bag, fermentation plant is put into and ferments, fermentation plant Temperature is at 30 DEG C -40 DEG C;
Mixture temperature rises to 40 DEG C -50 DEG C after 24 hours, after mixture temperature is raised to 60 DEG C, 72 hours after 48 hours Mixture temperature is raised to 70 DEG C -73 DEG C, keeps the temperature 48 hours at this time, and temperature is begun to decline, and after -96 hours, mixes within about 72 hours Object temperature drops to 30 DEG C -40 DEG C of room temperature, then after keeping the temperature -96 hours 72 hours, and fermentation process is completed;
The mixture effective component content obtained after fermentation are as follows: 28% fulvic acid, 14% nucleotide, 9.3% ammonia Base acid, 30% small peptide, total effective component content are 81.3%.
Two), extracted: the mixture that the first step is obtained after everfermentation is added in extraction cylinder, adds in the ratio of 1:6 The clear water for entering 55%, after being sufficiently stirred 6 hours, by agitated mixture be put into liquid-solid separating centrifuge carry out solid-liquor separation, divide It separates out the liquid come to be put into reverse extracter, by 40 nanometers of pottery magnetic filter stick, it is yellow rotten that the biochemistry that solid content is 15% is made Sour stoste;
Three) it, is spray-dried: the biochemical fulvic acid stoste that the solid content that second step obtains is 15% is passed through into screw pump It squeezes into spray drying tower, is atomized biochemical fulvic acid stoste by atomizer, it is fast then to carry out 250 DEG C of air-heater again Speed evaporation moisture content, makes biochemical fulvic acid stoste become 120 targeted fine powders eventually by air-introduced machine and cyclone, obtains biochemical yellow rotten Sour fine powder.
Biochemical fulvic acid fine powder is produced using biology hair effect technology, with molecular weight is small, physiological is high, active group is tired More features, predominant amount are fulvic acid, nucleotide, small peptide ammino acid in combination with a variety of effective ingredients, and contained Huang is rotten Acid have closing blade face stomata improve the drought resisting of fruit tree cold-resistant function, have repair and reconstruction function to plant cell, through cell wall into The potassium dihydrogen phosphate being recycled into compatibility in a subtle way is that full nutrition flower bone improves itself cold tolerance, brown sugar and bonding in compatibility Film forming agent xanthan rubber powder, cellulose powder form protective film, and brown sugar is improved the physiological function of thermal energy, to improve the cold-resistant of fruit tree Ability, flower bone pistil can smoothly spend cold current in the environment of 4-5 nanometers of formation of fever protective film, normally bloom, award Powder, result.Ginger powder is also warm material described in Chinese medicine pharmacopeia, also has and generates the freeze proof function of thermal energy raising fruit tree.It is a variety of Microelement and compound sodium nitrophenolate are mainly the anti-adversity for improving fruit tree, enhance the cold tolerance of itself.Permanganic acid in compatibility Potassium has the stronger function of killing surface bacteria fungi.A good environment can be created after spraying to fruit tree, it is freeze proof to improve Function.Film forming is integrated, thermal energy is improved, nutrition, sterilizes degeneration-resistant comprehensive function, to reach antifreeze, guarantor is colored, fruit retention Effect.
The beneficial effects of the present invention are: compatibility is reasonable, simple process, without secondary toxic action.Product category pulvis solid, volume It is small, it is convenient for packed and transported.
Specific embodiment
Embodiment one
First step, in the following order by 200 grams of potassium dihydrogen phosphates, 300 grams of brown sugar, 10 grams of zinc sulfate, 20 grams of sulfuric acid Ultra-fine grinding is carried out after mixing evenly after ferrous iron, 10 grams of boric acid, 5 grams of potassium permanganate, 20 grams of compound sodium nitrophenolates, 20 grams of ginger powder compoundings, 80 targeted fine powders are crushed into ultrafine crusher, the ultra-fine grinding using ultrafine crusher is crushed using winnowing type Machine is completed, and the machine controls fineness by control air volume;
Second step mixes 200 grams of xanthan rubber powders, 80 grams of celluloses into the 80 mesh superfines that first step obtains Powder, 135 grams of biochemical fulvic acid fine powder compoundings, are then stirred 10 minutes with blender, with 500 grams -1000 grams of packaging bag packet Dress, obtains fruit tree antifreezing agent.
Embodiment two,
First step, in the following order by 100 grams of potassium dihydrogen phosphates, 150 grams of brown sugar, 5 grams of zinc sulfate, 10 grams of sulfuric acid Asias Ultra-fine grinding is carried out after mixing evenly after iron, 5 grams of boric acid, 2.5 grams of potassium permanganate, 10 grams of compound sodium nitrophenolates, 10 grams of ginger powder compoundings, is used Ultrafine crusher is crushed into 80 targeted fine powders, and the ultra-fine grinding is using winnowing type pulverizer using ultrafine crusher It completes, the machine controls fineness by control air volume;
Second step mixes 100 grams of xanthan rubber powders, 40 grams of celluloses into the 80 mesh superfines that first step obtains Powder, 67.5 grams of biochemical fulvic acid fine powder compoundings, are then stirred 10 minutes with blender, with 500 grams -1000 grams of packaging bag packet Dress, obtains fruit tree antifreezing agent.
Embodiment three,
First step, in the following order by 300 grams of potassium dihydrogen phosphates, 450 grams of brown sugar, 15 grams of zinc sulfate, 30 grams of sulfuric acid Superfine powder is carried out after mixing evenly after ferrous iron, 15 grams of boric acid, 7.5 grams of potassium permanganate, 30 grams of compound sodium nitrophenolates, 30 grams of ginger powder compoundings It is broken, 80 targeted fine powders are crushed into ultrafine crusher, the ultra-fine grinding is using winnowing type using ultrafine crusher Pulverizer is completed, and the machine controls fineness by control air volume;
Second step mixes 300 grams of xanthan rubber powders, 120 grams of celluloses into the 80 mesh superfines that first step obtains Powder, 202.5 grams of biochemical fulvic acid fine powder compoundings, are then stirred 10 minutes with blender, with 500 grams -1000 grams of packaging bag packet Dress, obtains fruit tree antifreezing agent.
Application method: being dissolved when use with 200 times of water, after 2 hours, is stirred 10-15 minutes, can be used to fruit tree spray It applies, sprays after doing in the protective film of branches and leaves 4-5 meters of bon e formation of flower, be not readily dissolved in water, flower bone can be played within 2 weeks feeding Shield effect flows to come in first 1-2 days to spray in cold spell in later spring, and effect is best, can resist subzero 2-3 DEG C of low temperature, make fruit tree just Normally opened flower, pollination, result.
Acute toxicological experiment has done to biochemical fulvic acid fine powder in Hebei Academy of Medical Science, with more than human normal dosage 240 times on small white mouse carry out stomach-filling experiments, any adverse reaction is had no after 7 days.Other compatibility raw materials are all made of food-grade Raw material is prepared, and is perfectly safe to people and animals.
Done a large amount of experiment and demonstration over 5 years throughout the country: Sichuan Province Renshou County is that loquat cultivates big county, there is 40 Remaining ten thousand mu, loquat was bloomed before the Spring Festival, after the Spring Festival as a result, on the occasion of hypothermic phase, there is cold current every year, is generated and is frozen flower and freeze young fruit Phenomenon, or even cause to have no harvest.Since 2014, with " Ji is contained ammonia peptide antifreezing agent and is sprayed, and the flower bone phase sprays one time before the Spring Festival, Young fruit period sprays 2 time, and algid stage is spent safely in Loquat-Shaped Cake, high yield good harvest, and output increased 10% or more, and quality is also changed It is kind.Animal Community in Zhanjiang, Guangdong, 2016 are south vegetable north transportations, the main producing region across season vegetables, but every year can all have around the Spring Festival it is cold Inflow is invaded, and makes capsicum, cucumber, banana all can be by different excessive freeze injuries, since using fruit tree antifreezing provided by the invention Freeze injury problem is resolved after agent, is invaded in spite of cold wave, vegetables banana all can be safe and sound.Hebei province Jinzhou City, Xinji City, Shenzhou City be apple, pears, peach main growing area, but it is annual by the end of March -4 month at the beginning of will have a cold wave invasion, freezing colored bone, Pistil causes the underproduction or total crop failure, we have done the antifreeze experiment of apple, pears, peach in three cities respectively within this 2 years.At subzero 3 DEG C In the case of, fruit tree yields positive results as usual.
Effect standard determines: using fruit tree antifreezing agent provided by the invention, selecting best spraying time can be effectively controlled fruit The generation for setting freeze injury does not have freeze injury in flower bone, pistil, fruit branch, yields positive results as usual, this is just solved in subzero 3 DEG C of cold wave The orchard worker that determined most worry because caused by freeze injury have no harvest trouble and worry.
The above-described embodiments are merely illustrative of preferred embodiments of the present invention, not to structure of the invention Think and range is defined, without departing from the design concept of the invention, those skilled in the art are to the present invention The various improvement made of technical solution, protection scope of the present invention should all be fallen into.

Claims (1)

1. a kind of preparation method of fruit tree antifreezing agent, it is characterised in that it is grouped as according to following group of unit of weight proportion: 13.5% biochemical fulvic acid fine powder, 20% potassium dihydrogen phosphate, 30% brown sugar, 20% xanthan rubber powder, 8% cellulose Powder, 2% ginger powder, 2% compound sodium nitrophenolate, 1% zinc sulfate, 2% ferrous sulfate, 1% boric acid, 0.5% permanganic acid Sodium.
The preparation method of the fruit tree antifreezing agent the following steps are included:
First step, in the following order by 20% potassium dihydrogen phosphate, 30% brown sugar, 1% zinc sulfate, 2% sulfuric acid it is sub- It is carried out after mixing evenly after iron, 1% boric acid, 0.5% potassium permanganate, 2% compound sodium nitrophenolate, 2% ginger powder compounding ultra-fine It crushes, is crushed into 80 targeted fine powders with ultrafine crusher;
Second step, into the 80 mesh superfines that first step obtains mix 20% xanthan rubber powder, 8% cellulose powder, 13.5% biochemical fulvic acid fine powder compounding, is then stirred 10 minutes with blender, with 500 grams -1000 grams of packaging bag packet Dress, obtains fruit tree antifreezing agent.
The biochemical fulvic acid fine powder is extracted after fermenting according to the following component of unit of weight proportion: 53.6% wood Bits, 10% wheat bran, 12% corn flour, 0.8% microelement, 0.6% vitamin, 6% monoammonium phosphate, 6% Dregs of beans, 10% soybean oil, 1% strain, the proportion of water are the 55% of the above total weight proportion.
The microelement refers to the single-item combination or any combination of zinc, iron, manganese, boric acid.
The vitamin refers to the single-item combination or any combination of vitamin B, vitamin C, vitamin D, vitamin E.
The strain refers to that photosynthetic bacteria, nitrogen-fixing bacteria, ferment bacterium, lactic acid bacteria, bacillus subtilis, bacillus licheniformis, phosphorus are thin Bacterium, bacillus megaterium, bacillusmusilaginosiengineering, actinomyces, aspergillus oryzae, aspergillus niger, trichoderma harzianum, muscardine, green muscardine fungus, Bifidobacterium;
The preparation method of the biochemical fulvic acid fine powder the following steps are included:
One), fermentation process: by 53.6% sawdust, 10% wheat bran, 12% corn flour, 0.8% microelement, 0.6% Vitamin, 6% monoammonium phosphate, 6% dregs of beans, 10% soybean oil be added after mixing in the ratio of carbon-nitrogen ratio 1:25 Said mixture is packed into ventilative woven bag, is put into fermentation plant and ferments, the temperature of fermentation plant exists by 1% strain 30℃-40℃;
Mixture temperature rises to 40 DEG C -50 DEG C after 24 hours, and mixture temperature is raised to 60 DEG C after 48 hours, mixes after 72 hours Object temperature is raised to 70 DEG C -73 DEG C, keeps the temperature 48 hours at this time, and temperature is begun to decline, and about 72 hours after -96 hours, mixture temperature Degree drops to 30 DEG C -40 DEG C of room temperature, then after keeping the temperature -96 hours 72 hours, and fermentation process is completed;
The mixture effective component content obtained after fermentation are as follows: 28% fulvic acid, 14% nucleotide, 9.3% amino acid, 30% small peptide, total effective component content are 81.3%.
Two), extracted: the mixture that the first step is obtained after everfermentation is added in extraction cylinder, is added in the ratio of 1:6 Agitated mixture after being sufficiently stirred 6 hours, is put into liquid-solid separating centrifuge and carries out solid-liquor separation, separation by 55% clear water Liquid out is put into reverse extracter, and by 40 nanometers of pottery magnetic filter stick, the biochemical fulvic acid that solid content is 15% is made Stoste;
Three) it, is spray-dried: the biochemical fulvic acid stoste that the solid content that second step obtains is 15% is squeezed by screw pump In spray drying tower, biochemical fulvic acid stoste is atomized by atomizer, then carries out 250 DEG C of air-heater rapid steaming again Shampoo part makes biochemical fulvic acid stoste become 120 targeted fine powders eventually by air-introduced machine and cyclone, obtains biochemical fulvic acid essence Powder.
CN201811293331.3A 2018-11-01 2018-11-01 A kind of preparation method of fruit tree antifreezing agent Pending CN109265250A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110896776A (en) * 2019-12-17 2020-03-24 中国热带农业科学院南亚热带作物研究所 Method for preventing frost of young macadimia nuts in high-altitude mountain areas

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Publication number Priority date Publication date Assignee Title
CN101253867A (en) * 2006-12-19 2008-09-03 王树禹 Cold-resistance spraying agent
CN104585239A (en) * 2015-02-02 2015-05-06 山西省农业科学院棉花研究所 Multifunctional fruit tree low temperature-resistant preparation and preparation method thereof
CN105130692A (en) * 2015-07-14 2015-12-09 广西乐业百农原生态食品开发有限公司 Biochemical fulvic acid fertilizer and preparation process thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101253867A (en) * 2006-12-19 2008-09-03 王树禹 Cold-resistance spraying agent
CN104585239A (en) * 2015-02-02 2015-05-06 山西省农业科学院棉花研究所 Multifunctional fruit tree low temperature-resistant preparation and preparation method thereof
CN105130692A (en) * 2015-07-14 2015-12-09 广西乐业百农原生态食品开发有限公司 Biochemical fulvic acid fertilizer and preparation process thereof

Non-Patent Citations (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110896776A (en) * 2019-12-17 2020-03-24 中国热带农业科学院南亚热带作物研究所 Method for preventing frost of young macadimia nuts in high-altitude mountain areas

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Application publication date: 20190125