CN108887293A - A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof - Google Patents
A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof Download PDFInfo
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- CN108887293A CN108887293A CN201810822067.1A CN201810822067A CN108887293A CN 108887293 A CN108887293 A CN 108887293A CN 201810822067 A CN201810822067 A CN 201810822067A CN 108887293 A CN108887293 A CN 108887293A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/16—Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/50—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids the nitrogen atom being doubly bound to the carbon skeleton
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/50—1,3-Diazoles; Hydrogenated 1,3-diazoles
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- A—HUMAN NECESSITIES
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
- A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
- A01N47/14—Di-thio analogues thereof
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
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- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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Abstract
The invention discloses a kind of high-efficiency low-toxicity chemical pesticide new products and preparation method thereof, as made by the component of following weight ratio:20-30 parts of frutus cnidii, 15-30 parts of mulberry leaf, 12-20 parts of purple perilla, 2-5 parts of acid sodium of isocyanide dichloride urea, 2-8 parts of eugenol, 2-6 parts of nitrile bacterium azoles, 3-7 parts of kresoxim-methyl, 1-3 parts of potassium nitrate, 20-60 parts of chitosan, 0.5-1 parts of sodium carboxymethylcellulose, 16-22 parts of Mancozeb, 5-10 parts of chlorogenic acid, 10-15 parts of iprodione, 5-15 parts of cyprodinil, 15-25 parts of oxazole, 1-3 parts of bacillus subtilis, 0.1-1 parts of imazalil, 1-3 parts of Noni fruit, 10-20 parts of ethanol extraction, 1-5 parts of suspending agent, 2-6 parts of water dispersible granules, 1-3 parts of smoke agent, 10-15 parts and Tween 80 0.5-1 parts of ultra-low volume spray agent, the present invention relates to grape Prevention Technique fields.A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof reduces and substitutes dosage form easy to pollute, achievees the purpose that be reduced synergy, safety and environmental protection, improve the guard time of medicament, can play efficient protective action with a variety of grape major target pest and disease damages.
Description
Technical field
The present invention relates to grape Prevention Technique field, specially a kind of high-efficiency low-toxicity chemical pesticide new product and its preparation side
Method.
Background technique
As the improvement of people's living standards, the demand to fruit is more and more, quality requirements are higher and higher, oenin
The morbidity of mildew occurs, and reduces the quality of grape, influences orchard worker's income, and Chinese Grape producing region, which has, occurs grape leafhopper
Harm, adult and nymph inhale juice in leaf back, are killed blade face and small white dirt is presented, and leaf color is pale when serious, so that shrivelled de-
It falls, the major targets pest and disease damage such as anthracnose, gray mold, mealybug is accompanied by wine-growing, need at present a kind of efficiently new
Medicament newly administered and prevented and treated to insect pest and grape illness and reduce substitution missible oil, wettable powder etc. easily by mixed combination product
Pollute bring pollution problem.
Summary of the invention
(One)The technical issues of solution
In view of the deficiencies of the prior art, the present invention provides a kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, solutions
Current pesticide control of having determined can not be administered and be prevented and treated to a variety of insect pest diseases, and the additive in pesticide control is easy to soil again
The problem of ground pollutes.
(Two)Technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:A kind of high-efficiency low-toxicity chemical pesticide new product,
As made by the component of following weight ratio:20-30 parts of frutus cnidii, 15-30 parts of mulberry leaf, 12-20 parts of purple perilla, isocyanide dichloride urea
Sour sodium 2-5 parts, 2-8 parts of eugenol, 2-6 parts of nitrile bacterium azoles, 3-7 parts of kresoxim-methyl, 1-3 parts of potassium nitrate, 20-60 parts of chitosan, carboxylic first
0.5-1 parts of base sodium cellulosate, 16-22 parts of Mancozeb, 5-10 parts of chlorogenic acid, 10-15 parts of iprodione, 5-15 parts of cyprodinil,
15-25 parts of oxazole, 1-3 parts of bacillus subtilis, 0.1-1 parts of imazalil, 1-3 parts of Noni fruit, 10-20 parts of ethanol extraction,
1-5 parts of suspending agent, 2-6 parts of water dispersible granules, 1-3 parts of smoke agent, 10-15 parts of ultra-low volume spray agent and 0.5-1 parts of Tween 80.
Preferably, made by the component of following weight ratio:24-26 parts of frutus cnidii, 20-25 parts of mulberry leaf, purple perilla 15-18
Part, 3-5 parts of isocyanide dichloride urea acid sodium, 4-6 parts of eugenol, 3-5 parts of nitrile bacterium azoles, 4-6 parts of kresoxim-methyl, 1-2 parts of potassium nitrate, chitosan
40-50 parts, it is 0.7-0.9 parts of sodium carboxymethylcellulose, 18-20 parts of Mancozeb, 6-8 parts of chlorogenic acid, 12-14 parts of iprodione, phonetic
7-12 parts of collarium amine, 17-22 parts of oxazole, 1-3 parts of bacillus subtilis, 0.4-0.6 parts of imazalil, 1-3 parts of Noni fruit, extraction
Take 14-17 parts of ethyl alcohol, 2-4 parts of suspending agent, 3-5 parts of water dispersible granules, 1-3 parts of smoke agent, 12-14 parts of ultra-low volume spray agent and
0.5-1 parts of Tween 80.
Preferably, made by the component of following weight ratio:25 parts of frutus cnidii, 22 parts of mulberry leaf, 16 parts of purple perilla, dichloro are different
4 parts of nitrile urea acid sodium, 5 parts of eugenol, 4 parts of nitrile bacterium azoles, 5 parts of kresoxim-methyl, 2 parts of potassium nitrate, 45 parts of chitosan, sodium carboxymethylcellulose
0.8 part, 19 parts of Mancozeb, 7 parts of chlorogenic acid, 13 parts of iprodione, 10 parts of cyprodinil, 20 parts of oxazole, bacillus subtilis
2 parts of bacterium, 2 parts of Noni fruit, 15 parts of ethanol extraction, 3 parts of suspending agent, 4 parts of water dispersible granules, 2 parts of smoke agent, surpasses 0.5 part of imazalil
13 parts and 0.8 part of Tween 80 of low-gallonage spraying agent.
A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, includes the following steps:
(1)Noni fruit, frutus cnidii, mulberry leaf, purple perilla and sweet wormwood are taken, is cleaned, the water of 8-11 times of volume is added, extraction is boiled in heating
Twice, 2-3 hours each, it is spare to be condensed into total extract for combined extract after extraction;
(2)It takes chitosan to be added in 40-50 °C of warm water, dissolves by heating, obtain chitosan solution, keep the temperature, it is spare;
(3)Take isocyanide dichloride urea acid sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80 that total extract is added
It in liquid, pours into stirring mixer and is mixed using the revolving speed of 5000-6500r/min, it is standby to obtain mixed liquor after mixing 15-30 minutes
With;
(4)Take Mancozeb, chlorogenic acid, iprodione, cyprodinil, oxazole, bacillus subtilis, imazalil that pure water is added
Mixed liquor is poured into after being stirred, using obtaining dispersion liquid after 1000-2000r/min blender mixing 5-10;
(5)Take ethanol extraction, water dispersible granules, suspending agent, smoke agent ultra-low volume spray agent and chitosan solution that dispersion is added
Be uniformly mixed in liquid before reagent liquid it is spare;
(6)Liquid takes supernatant before reagent after standing 10-12 hours, and potassium nitrate is added, and dissolution mixes to get new product.
Preferably, liquid is stood using room temperature standing before the reagent.
Preferably, the step(3)Standard atmospheric pressure is used when stirring mixer hybrid working.
Preferably, it is 1.06-1.12 that the chitosan solution, which is concentrated into 30 DEG C of relative densities,.
Preferably, the water dispersible granules are one or more of dried starch, zeolite powder, coal ash powder and ammonium sulfate.
Preferably, the suspending agent is by effective component, dispersing agent, thickener, antiprecipitant, defoaming agent, antifreezing agent and water
It constitutes.
Preferably, described be smoke agent is Mobucin smoke agent.
(Three)Beneficial effect
The present invention provides a kind of high-efficiency low-toxicity chemical pesticide new products and preparation method thereof.Has following beneficial effect:
The high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, can be with by adding Noni fruit and ethanol extraction in a medicament
The anthracnose for effectively preventing grape uses suspending agent, water dispersible granules, smoke agent, ultra-low volume spray agent etc. in pesticide control
Environment-friendly agent product and dosage form reduce and substitute the dosage forms easy to pollute such as missible oil, wettable powder, reach decrement synergy, safety collar
The guard time of medicament can be improved in the purpose of guarantor, the present invention, can also be to downy mildew, anthracnose, gray mold, leafhopper, mealybug
Equal grapes major target pest and disease damage plays efficient protective action.
The high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, water dispersible granules, good dispersion, suspensibility are high, steady
The features such as qualitative good, easy to use, avoids wettable powder and generates dust, and suspending agent packed and transported is inconvenient, and storage is also easy to produce
The disadvantages of precipitating, agglomeration, poor fluidity, viscous wall.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Case study on implementation one:A kind of high-efficiency low-toxicity chemical pesticide new product, as made by the component of following weight ratio:Snake
24 parts of machine tool, 20 parts of mulberry leaf, 15 parts of purple perilla, 3 parts of isocyanide dichloride urea acid sodium, 4 parts of eugenol, 3 parts of nitrile bacterium azoles, 4 parts of kresoxim-methyl, nitre
1 part of sour potassium, 40 parts of chitosan, 0.7 part of sodium carboxymethylcellulose, 18 parts of Mancozeb, 6 parts of chlorogenic acid, 12 parts of iprodione, phonetic bacterium
7 parts of cyclammonium, 1 part of bacillus subtilis, 0.4 part of imazalil, 1 part of Noni fruit, 14 parts of ethanol extraction, suspends at 17 parts of oxazole
2 parts of agent, 3 parts of water dispersible granules, 1 part of smoke agent, 12 parts of ultra-low volume spray agent and 0.5 part of Tween 80.
A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, includes the following steps:
(1)Noni fruit, frutus cnidii, mulberry leaf, purple perilla and sweet wormwood are taken, is cleaned, the water of 8-11 times of volume is added, extraction is boiled in heating
Twice, 2-3 hours each, it is spare to be condensed into total extract for combined extract after extraction;
(2)It takes chitosan to be added in 40-50 °C of warm water, dissolves by heating, obtain chitosan solution, keep the temperature, it is spare;
(3)Take isocyanide dichloride urea acid sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80 that total extract is added
It in liquid, pours into stirring mixer and is mixed using the revolving speed of 5000-6500r/min, it is standby to obtain mixed liquor after mixing 15-30 minutes
With;
(4)Take Mancozeb, chlorogenic acid, iprodione, cyprodinil, oxazole, bacillus subtilis, imazalil that pure water is added
Mixed liquor is poured into after being stirred, using obtaining dispersion liquid after 1000-2000r/min blender mixing 5-10;
(5)Take ethanol extraction, water dispersible granules, suspending agent, smoke agent ultra-low volume spray agent and chitosan solution that dispersion is added
Be uniformly mixed in liquid before reagent liquid it is spare;
(6)Liquid takes supernatant before reagent after standing 10-12 hours, and potassium nitrate is added, and dissolution mixes to get new product.
Liquid is stood before reagent is stood using room temperature.
Step(3)Standard atmospheric pressure is used when stirring mixer hybrid working.
It is 1.06-1.12 that chitosan solution, which is concentrated into 30 DEG C of relative densities,.
Case study on implementation two:A kind of high-efficiency low-toxicity chemical pesticide new product, as made by the component of following weight ratio:With
Made by the component of lower weight ratio:25 parts of frutus cnidii, 22 parts of mulberry leaf, 16 parts of purple perilla, 4 parts of isocyanide dichloride urea acid sodium, cloves
5 parts of phenol, 4 parts of nitrile bacterium azoles, 5 parts of kresoxim-methyl, 2 parts of potassium nitrate, 45 parts of chitosan, 0.8 part of sodium carboxymethylcellulose, Mancozeb 19
Part, 7 parts of chlorogenic acid, 13 parts of iprodione, 10 parts of cyprodinil, 20 parts of oxazole, 2 parts of bacillus subtilis, imazalil 0.5
Part, 2 parts of Noni fruit, 15 parts of ethanol extraction, 3 parts of suspending agent, 4 parts of water dispersible granules, 2 parts of smoke agent, ultra-low volume spray agent 13
Part and 0.8 part of Tween 80.
A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, includes the following steps:
(1)Noni fruit, frutus cnidii, mulberry leaf, purple perilla and sweet wormwood are taken, is cleaned, the water of 8-11 times of volume is added, extraction is boiled in heating
Twice, 2-3 hours each, it is spare to be condensed into total extract for combined extract after extraction;
(2)It takes chitosan to be added in 40-50 °C of warm water, dissolves by heating, obtain chitosan solution, keep the temperature, it is spare;
(3)Take isocyanide dichloride urea acid sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80 that total extract is added
It in liquid, pours into stirring mixer and is mixed using the revolving speed of 5000-6500r/min, it is standby to obtain mixed liquor after mixing 15-30 minutes
With;
(4)Take Mancozeb, chlorogenic acid, iprodione, cyprodinil, oxazole, bacillus subtilis, imazalil that pure water is added
Mixed liquor is poured into after being stirred, using obtaining dispersion liquid after 1000-2000r/min blender mixing 5-10;
(5)Take ethanol extraction, water dispersible granules, suspending agent, smoke agent ultra-low volume spray agent and chitosan solution that dispersion is added
Be uniformly mixed in liquid before reagent liquid it is spare;
(6)Liquid takes supernatant before reagent after standing 10-12 hours, and potassium nitrate is added, and dissolution mixes to get new product.
Liquid is stood before reagent is stood using room temperature.
Step(3)Standard atmospheric pressure is used when stirring mixer hybrid working.
It is 1.06-1.12 that chitosan solution, which is concentrated into 30 DEG C of relative densities,.
Case study on implementation three:A kind of high-efficiency low-toxicity chemical pesticide new product, as made by the component of following weight ratio:Snake
26 parts of machine tool, 25 parts of mulberry leaf, 18 parts of purple perilla, 5 parts of isocyanide dichloride urea acid sodium, 6 parts of eugenol, 5 parts of nitrile bacterium azoles, 6 parts of kresoxim-methyl, nitre
2 parts of sour potassium, 50 parts of chitosan .9 parts of sodium carboxymethylcellulose, 20 parts of Mancozeb, 8 parts of chlorogenic acid, 14 parts of iprodione, phonetic bacterium
12 parts of cyclammonium, 3 parts of bacillus subtilis, 0.6 part of imazalil, 3 parts of Noni fruit, 17 parts of ethanol extraction, suspends at 22 parts of oxazole
4 parts of agent, 5 parts of water dispersible granules, 3 parts of smoke agent, 14 parts of ultra-low volume spray agent and 0.5-1 parts of Tween 80.
A kind of high-efficiency low-toxicity chemical pesticide new product and preparation method thereof, includes the following steps:
(1)Noni fruit, frutus cnidii, mulberry leaf, purple perilla and sweet wormwood are taken, is cleaned, the water of 8-11 times of volume is added, extraction is boiled in heating
Twice, 2-3 hours each, it is spare to be condensed into total extract for combined extract after extraction;
(2)It takes chitosan to be added in 40-50 °C of warm water, dissolves by heating, obtain chitosan solution, keep the temperature, it is spare;
(3)Take isocyanide dichloride urea acid sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80 that total extract is added
It in liquid, pours into stirring mixer and is mixed using the revolving speed of 5000-6500r/min, it is standby to obtain mixed liquor after mixing 15-30 minutes
With;
(4)Take Mancozeb, chlorogenic acid, iprodione, cyprodinil, oxazole, bacillus subtilis, imazalil that pure water is added
Mixed liquor is poured into after being stirred, using obtaining dispersion liquid after 1000-2000r/min blender mixing 5-10;
(5)Take ethanol extraction, water dispersible granules, suspending agent, smoke agent ultra-low volume spray agent and chitosan solution that dispersion is added
Be uniformly mixed in liquid before reagent liquid it is spare;
(6)Liquid takes supernatant before reagent after standing 10-12 hours, and potassium nitrate is added, and dissolution mixes to get new product.
Liquid is stood before reagent is stood using room temperature.
Step(3)Standard atmospheric pressure is used when stirring mixer hybrid working.
It is 1.06-1.12 that chitosan solution, which is concentrated into 30 DEG C of relative densities,.
The embodiment of the present invention and the comparison of common glucose pesticide control are as follows:
Common glucose pesticide control | Embodiment one | Embodiment two | Embodiment three | |
7 days preventive effects after medicine(%) | 55.87 | 94.46 | 95.77 | 93.21 |
14 days preventive effects after medicine(%) | 50.23 | 91.17 | 92.34 | 91.01 |
21 days preventive effects after medicine(%) | 42.37 | 85.78 | 89.64 | 87.13 |
Average duration is decomposed in pollution(It) | 30 | 12 | 7 | 11 |
Preventive effect type | It is single | It is a variety of | It is a variety of | It is a variety of |
From above table as can be seen that the time of the preventive effect of the invention compared with common pesticide control in the market is longer, type is prevented and treated
More, substitute missible oil, the protection medicament easy to pollute such as wettable powder makes medicament pollutant decomposes more rapidly after use, reach
To decrement synergy, the purpose of safety and environmental protection.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (10)
1. a kind of high-efficiency low-toxicity chemical pesticide new product, it is characterised in that:As made by the component of following weight ratio:Cnidium monnieri
20-30 parts sub-, 15-30 parts of mulberry leaf, 12-20 parts of purple perilla, 2-5 parts of isocyanide dichloride urea acid sodium, 2-8 parts of eugenol, nitrile bacterium azoles 2-6
Part, 3-7 parts of kresoxim-methyl, 1-3 parts of potassium nitrate, 20-60 parts of chitosan, 0.5-1 parts of sodium carboxymethylcellulose, Mancozeb 16-22
Part, 5-10 parts of chlorogenic acid, 10-15 parts of iprodione, 5-15 parts of cyprodinil, 15-25 parts of oxazole, bacillus subtilis 1-3
Part, 0.1-1 parts of imazalil, 1-3 parts of Noni fruit, 10-20 parts of ethanol extraction, 1-5 parts of suspending agent, 2-6 parts of water dispersible granules, smog
1-3 parts of agent, 10-15 parts of ultra-low volume spray agent and 0.5-1 parts of Tween 80.
2. a kind of high-efficiency low-toxicity chemical pesticide new product according to claim 1, it is characterised in that:It is preferred that following parts by weight
Made by the component of ratio:24-26 parts of frutus cnidii, 20-25 parts of mulberry leaf, 15-18 parts of purple perilla, 3-5 parts of isocyanide dichloride urea acid sodium, fourth
Fragrant phenol 4-6 parts, 3-5 parts of nitrile bacterium azoles, 4-6 parts of kresoxim-methyl, 1-2 parts of potassium nitrate, 40-50 parts of chitosan, sodium carboxymethylcellulose
0.7-0.9 parts, 18-20 parts of Mancozeb, 6-8 parts of chlorogenic acid, 12-14 parts of iprodione, 7-12 parts of cyprodinil, oxazole
17-22 parts, 1-3 parts of bacillus subtilis, 0.4-0.6 parts of imazalil, 1-3 parts of Noni fruit, 14-17 parts of ethanol extraction, suspending agent
2-4 parts, 3-5 parts of water dispersible granules, 1-3 parts of smoke agent, 12-14 parts of ultra-low volume spray agent and 0.5-1 parts of Tween 80.
3. a kind of high-efficiency low-toxicity chemical pesticide new product according to claim 1, it is characterised in that:It is preferred that following parts by weight
Made by the component of ratio:25 parts of frutus cnidii, 22 parts of mulberry leaf, 16 parts of purple perilla, 4 parts of isocyanide dichloride urea acid sodium, 5 parts of eugenol, nitrile
4 parts of bacterium azoles, 5 parts of kresoxim-methyl, 2 parts of potassium nitrate, 45 parts of chitosan, 0.8 part of sodium carboxymethylcellulose, 19 parts of Mancozeb, green original
Sour 7 parts, 13 parts of iprodione, 10 parts of cyprodinil, 20 parts of oxazole, 2 parts of bacillus subtilis, 0.5 part of imazalil, Noni fruit
2 parts, 15 parts of ethanol extraction, 3 parts of suspending agent, 4 parts of water dispersible granules, 2 parts of smoke agent, 13 parts of ultra-low volume spray agent and tween
800.8 part.
4. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product, it is characterised in that:Include the following steps:
Noni fruit, frutus cnidii, mulberry leaf, purple perilla and sweet wormwood are taken, is cleaned, the water of 8-11 times of volume is added, heating boils extraction twice,
2-3 hours every time, it is spare to be condensed into total extract for combined extract after extraction;
It takes chitosan to be added in 40-50 °C of warm water, dissolves by heating, obtain chitosan solution, keep the temperature, it is spare;
Take isocyanide dichloride urea acid sodium, eugenol, nitrile bacterium azoles, kresoxim-methyl, sodium carboxymethylcellulose and Tween 80 that total extract is added
In, it pours into stirring mixer and is mixed using the revolving speed of 5000-6500r/min, it is spare to obtain mixed liquor after mixing 15-30 minutes;
Take Mancozeb, chlorogenic acid, iprodione, cyprodinil, oxazole, bacillus subtilis, imazalil that pure water is added and stirs
Mixed liquor is poured into after mixing mixing, using obtaining dispersion liquid after 1000-2000r/min blender mixing 5-10;
Noni fruit, ethanol extraction, water dispersible granules, suspending agent, smoke agent ultra-low volume spray agent and chitosan solution is taken to be added
Be uniformly mixed in dispersion liquid before reagent liquid it is spare;
Liquid takes supernatant before reagent after standing 10-12 hours, and potassium nitrate is added, and dissolution mixes to get new product.
5. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:It is described
Liquid is stood before reagent is stood using room temperature.
6. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:It is described
Step(3)Standard atmospheric pressure is used when stirring mixer hybrid working.
7. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:It is described
It is 1.06-1.12 that chitosan solution, which is concentrated into 30 DEG C of relative densities,.
8. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:It is described
Water dispersible granules are one or more of dried starch, zeolite powder, coal ash powder and ammonium sulfate.
9. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:It is described
Suspending agent is made of effective component, dispersing agent, thickener, antiprecipitant, defoaming agent, antifreezing agent and water.
10. a kind of preparation method of high-efficiency low-toxicity chemical pesticide new product according to claim 4, it is characterised in that:Institute
Stating as smoke agent is Mobucin smoke agent.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110352986A (en) * | 2019-07-04 | 2019-10-22 | 福建农林大学 | Composition and application containing bacillus subtilis and iprodione |
WO2022118257A1 (en) * | 2020-12-02 | 2022-06-09 | Adama Makhteshim Ltd. | Dithiocarbamate fungicide composition |
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CN104322576A (en) * | 2014-10-13 | 2015-02-04 | 句容市满园春家庭农场 | Grape downy mildew prevention and treatment medicine |
CN105010022A (en) * | 2015-06-30 | 2015-11-04 | 云南天质网络科技有限公司 | Prevention and treatment method for grape botrytis cinerea |
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2018
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104322576A (en) * | 2014-10-13 | 2015-02-04 | 句容市满园春家庭农场 | Grape downy mildew prevention and treatment medicine |
CN105010022A (en) * | 2015-06-30 | 2015-11-04 | 云南天质网络科技有限公司 | Prevention and treatment method for grape botrytis cinerea |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110352986A (en) * | 2019-07-04 | 2019-10-22 | 福建农林大学 | Composition and application containing bacillus subtilis and iprodione |
WO2022118257A1 (en) * | 2020-12-02 | 2022-06-09 | Adama Makhteshim Ltd. | Dithiocarbamate fungicide composition |
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