CN104305541A - Red bean velvet healthcare functional fabric - Google Patents
Red bean velvet healthcare functional fabric Download PDFInfo
- Publication number
- CN104305541A CN104305541A CN201410611744.7A CN201410611744A CN104305541A CN 104305541 A CN104305541 A CN 104305541A CN 201410611744 A CN201410611744 A CN 201410611744A CN 104305541 A CN104305541 A CN 104305541A
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- Prior art keywords
- fabric
- red bean
- refining
- agent
- bleaching
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- Granted
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- 239000004744 fabric Substances 0.000 title claims abstract description 148
- 240000001417 Vigna umbellata Species 0.000 title claims abstract description 46
- 235000011453 Vigna umbellata Nutrition 0.000 title claims abstract description 46
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 54
- 238000007670 refining Methods 0.000 claims abstract description 41
- 238000004061 bleaching Methods 0.000 claims abstract description 36
- 238000001035 drying Methods 0.000 claims abstract description 36
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- 239000002270 dispersing agent Substances 0.000 claims abstract description 22
- 238000012986 modification Methods 0.000 claims abstract description 22
- 238000012545 processing Methods 0.000 claims abstract description 21
- 238000005406 washing Methods 0.000 claims abstract description 18
- 239000004902 Softening Agent Substances 0.000 claims abstract description 16
- 229920000742 Cotton Polymers 0.000 claims abstract description 14
- 210000004209 hair Anatomy 0.000 claims abstract description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 25
- 230000036541 health Effects 0.000 claims description 23
- 230000008569 process Effects 0.000 claims description 23
- 230000004048 modification Effects 0.000 claims description 21
- 238000002156 mixing Methods 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 20
- 230000002421 anti-septic effect Effects 0.000 claims description 19
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 16
- 206010013786 Dry skin Diseases 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 15
- 230000000740 bleeding effect Effects 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 15
- 238000004043 dyeing Methods 0.000 claims description 13
- 239000000243 solution Substances 0.000 claims description 13
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- 150000001768 cations Chemical class 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- 238000009940 knitting Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 238000003801 milling Methods 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 10
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 10
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 8
- 230000003115 biocidal effect Effects 0.000 claims description 8
- 235000017550 sodium carbonate Nutrition 0.000 claims description 8
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000004132 cross linking Methods 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 239000012153 distilled water Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000012805 post-processing Methods 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 229920002545 silicone oil Polymers 0.000 claims description 5
- 235000019982 sodium hexametaphosphate Nutrition 0.000 claims description 5
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 5
- 238000010025 steaming Methods 0.000 claims description 5
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 239000001488 sodium phosphate Substances 0.000 claims description 4
- 229910000162 sodium phosphate Inorganic materials 0.000 claims description 4
- 235000011008 sodium phosphates Nutrition 0.000 claims description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 2
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 2
- 229910000397 disodium phosphate Inorganic materials 0.000 claims description 2
- 235000019800 disodium phosphate Nutrition 0.000 claims description 2
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 13
- 238000010382 chemical cross-linking Methods 0.000 abstract description 7
- 239000003431 cross linking reagent Substances 0.000 abstract description 7
- 230000008859 change Effects 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 2
- 239000003242 anti bacterial agent Substances 0.000 abstract 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 abstract 1
- 229910052731 fluorine Inorganic materials 0.000 abstract 1
- 239000011737 fluorine Substances 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 230000000149 penetrating effect Effects 0.000 abstract 1
- 238000007781 pre-processing Methods 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 238000004513 sizing Methods 0.000 abstract 1
- 238000009941 weaving Methods 0.000 abstract 1
- 239000000835 fiber Substances 0.000 description 13
- 238000010998 test method Methods 0.000 description 11
- 230000000845 anti-microbial effect Effects 0.000 description 10
- 238000010186 staining Methods 0.000 description 10
- 238000010586 diagram Methods 0.000 description 5
- 210000002268 wool Anatomy 0.000 description 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000007547 defect Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 241000222122 Candida albicans Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 238000006424 Flood reaction Methods 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 229940095731 candida albicans Drugs 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000007730 finishing process Methods 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 235000007183 paleface Nutrition 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 238000010340 saliva test Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/14—Other fabrics or articles characterised primarily by the use of particular thread materials
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C11/00—Teasing, napping or otherwise roughening or raising pile of textile fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C3/00—Stretching, tentering or spreading textile fabrics; Producing elasticity in textile fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/34—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass antimicrobial or antibacterial
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Coloring (AREA)
Abstract
The invention relates to a red bean velvet healthcare functional fabric. The red bean velvet healthcare functional fabric is characterized by adopting the following technology (1) weaving into the fabric through all cotton combing yarns, processing through weak positive ion softening agent S200 after refining, bleaching and dying, performing napping processing on the front side and rear side through a sanding machine after preprocessing open width drying before napping and enabling the fabric speed to be 16 to 18 meters per minute and the rotary speed of a carbon brush hair roller to be 1800 to 2000 turns per minute; (2) sorting the red beam fabric in antibacterial agent, wherein the antibacterial agent comprises components of 1.5 to 5 % o.w.f (On weight the fabric) of nano-modification titanium dioxide, 2 to 5 % o.w.f of penetrating agent and 1 to 3 % of dispersing agent; (3) performing tentering sizing sorting; (4) performing organic silicon and organic fluorine sorting. The red bean velvet healthcare functional fabric has the advantages of not needing to adding extra chemical crosslinking agent, having an anti-bacterial function, being good in antibacterial performance, high in washing fastness, free of color change and fluffy and soft.
Description
Technical field
The present invention relates to a kind of red bean suede shell fabric with health care function, belong to the antimicrobial health care function finishing technique field of fabric.
Background technology
Along with the raising of social development and people's living standard, the comfortableness of fabric and to be functionally more and more subject to people's attention.As the underwear fabric worn next to the skin, its comfortableness requires higher, not only requires to have super soft feel, and all has higher requirement to its anti-microbial property, skin-friendly.But antimicrobial product mostly in the market is chemical fibre and is mixed into through functionalization or floods antiseptic and obtain anti-microbial property.Because chemical fibre fabric snugness of fit is poor, be not suitable as underwear fabric raw material; And natural fiber dipping antiseptic finishing technique mostly is adds chemical cross-linking agent by antiseptic and be bonded in fiber surface, the color and luster of product and style are brought and has a strong impact on.Owing to adding chemical cross-linking agent, fabric is hardened, snugness of fit difference and washing easily come off, and anti-microbial property is unstable.This problem seriously constrains the popularization carrying out antibacterial functionalized arrangement in underwear fabric, and especially the antibacterial functionalized of natural fiber woven underwear fabric still lacks effective treatment process.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of red bean suede shell fabric with health care function is provided, without the need to adding additional chemical crosslinking agent, make fabric have antibacterial functions, and anti-microbial property is excellent, washing fastness is high, colourless change, the fluffy softness of cloth cover.
According to technical scheme provided by the invention, described red bean suede shell fabric with health care function, is characterized in that, adopt following processing step:
(1) making of red bean velvet fabric:
A, raw material adopt 100% cotton combed yarn, and fineness of yarn is that 32 ~ 40 English prop up, and yarn twist factor is 325 ~ 330;
B, knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, yarn is woven into fabric by the double knit weft machine of pin number 24 pins/inch;
C, refining, bleaching: refining and bleaching are carried out to the fabric that step (b) obtains;
The condition of described refining is: refining liquid component is: the knitting refining agent 729 of 3 ~ 7g/L, 1 ~ 5g/L soda ash, and surplus is water; Refining bath raio is 10 ~ 20:1, and refining temperature is 90 ~ 100 DEG C, and refining time is 45 ~ 50min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 1% ~ 40%, and bleaching bath ratio is 5 ~ 20:1, and the temperature of bleaching is 10 ~ 45 DEG C, and bleaching time is 5 ~ 15min;
D, dyeing: the fabric after step (c) process is dyeed;
E, dyeing post processing: adopt weak cation softening agent S200 process, the addition of weak cation softening agent S200 is 3.5 ~ 4.5% of fabric weight, and bath raio is 5 ~ 30:1, is rolled after normal temperature dipping 1 ~ 5min, pick-up is 50% ~ 80%, then 140 DEG C ~ 180 DEG C oven dry;
F, open width dry finishing: the fabric after step (e) being processed is 25 ~ 35% through dewatering to moisture content, and arrange in open width drying and setting machine, temperature is 150 ~ 165 DEG C, and the speed of a motor vehicle is 15 ~ 16m/min;
Pretreatment before g, napping: fabric is successively through overboard, decatize, drying and processing, the alkaline aqueous solution of overboard solution to be concentration be 0.01 ~ 1mol/L, bath raio is 50 ~ 100:1, and fabric soaks 1 ~ 50min in overboard solution, the temperature of drying and processing is 60 ~ 90 DEG C, and drying time is 3 ~ 10min; Then carry out decatize, steam temperature is 50 ~ 105 DEG C, and steam pressure during decatize is 2MPa ~ 10MPa, and steaming time is 5 ~ 60min;
H, napping process: the fabric after step (f) being processed carries out double-edged napping processing on roughing-up machine, and the speed of a motor vehicle of fabric is 16 ~ 18m/min, the rotating speed of carbon brush hair roller is 1800 ~ 2000 turns/min;
(2) antibiotic finish: the red bean velvet fabric that step (1) obtains is arranged in antiseptic; The composition of described antiseptic is: nano modification titanium dioxide: 1.5 ~ 5%o.w.f, bleeding agent: 2 ~ 5%o.w.f, dispersant: 1 ~ 3 %o.w.f; Stir 5 ~ 30 minutes at normal temperatures by after nano modification titanium dioxide, bleeding agent and dispersant, mixing speed is 150 ~ 300 revs/min, and fabric is processed 1 ~ 5min in antiseptic, and bath raio is 5 ~ 40:1, and treatment temperature is 140 ~ 190 DEG C;
(3) stentering forming arranges: the red bean velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 ~ 190 DEG C, and the speed of a motor vehicle of fabric is 15 ~ 25m/min, and upper overfeed ratio is 25 ~ 35%;
(4) organosilicon, Organic fluoride arrange: described silicone finish adopts block amino-silicone oil softening agent S200, consumption is 3.5 ~ 4.5% of fabric weight; bath raio is 5 ~ 20:1; be rolled after fabric is flooded 1 ~ 5min at normal temperatures; pick-up is 50% ~ 80%, then dries 5 ~ 15 minutes at 120 ~ 140 DEG C; Described Organic fluoride arranges and adopts HS1100 type self-cross linking type Organic fluoride finishing agent, consumption is 1.5 ~ 3.5% of fabric weight, be rolled after fabric is flooded 1 ~ 3min at normal temperatures, pick-up is 50% ~ 80%, after 3 ~ 10 minutes, 1 ~ 5min is baked in 120 ~ 160 DEG C again at 80 ~ 100 DEG C of preliminary dryings.
Further, the process dyeed in described step (1) operation d is: fabric normal temperature enters dye, and programming rate is 1 ~ 1.5 DEG C/min, is warming up to 65 ~ 70 DEG C, and insulation 50 ~ 60min, bath raio is 10:1 ~ 20:1.
Further, described bleeding agent is bleeding agent XP50 or XP70.
Further, described dispersant is dispersing agent C F.
Further, described overboard solution is one or more the aqueous solution in NaOH, potassium hydroxide, sodium carbonate, sodium acid carbonate, sodium hydrogen phosphate, dibastic sodium phosphate or sodium phosphate.
Further, in described step (2), the preparation method of nano modification titanium dioxide is: added by 2 ~ 15g titanium dioxide powder in 1L distilled water, add 1 ~ 4g sodium hexametaphosphate dispersant again, vigorous stirring 5 ~ 20 minutes, mixing speed is 50 ~ 150 revs/min to be made to be uniformly dispersed, and obtains mixed solution; Adopt concentration to be that the hydrochloric acid of 0.01 ~ 0.5mol/L regulates the pH value of mixed solution to be after 10 ~ 11, add 3 ~ 10g odium stearate, stirring reaction 3 ~ 10 hours, mixing speed is 30 ~ 100 revs/min; Filter, adopt alcohol and water washing respectively, in 110 ~ 150 DEG C of dryings 5 ~ 45 minutes, ball mill grinds, grinding rotating speed is 200 ~ 1000 revs/min, and milling time is 30 ~ 100 minutes, obtains nano-titanium dioxide powder; Be added to the water by nano-titanium dioxide powder, and add the PEG of 5 ~ 10g, vigorous stirring reaction 1 ~ 6 hour, mixing speed is 200 ~ 1000 revs/min; After filtration, respectively with water and ethanol washing, then in 80 ~ 120 DEG C of dryings 3 ~ 10 hours; Grind on dispersion mill, grinding rotating speed is 200 ~ 1000 revs/min, and milling time is 30 ~ 100 minutes, obtains nano modification titanium dioxide again.
The manufacture craft of red bean suede shell fabric with health care function of the present invention, at the uniform fine hair of surface coverage one deck of fabric, anti-microbial property is excellent, washing good stability, and cloth pale face becomes, soft fluffy.The present invention overcomes prior art textile and carry out with natural fibre blended fabric the defect that antibacterial functionalized arrangement is easy to change, washing fastness is low, fabric hardens, and provides a kind of antibacterial functionalized treatment process of cotton fabric environment-friendly energy-saving without the need to adding additional chemical crosslinking agent.Fabric anti-microbial property excellence after treatment, high, the colourless change of washing fastness, the fluffy softness of cloth cover, show good application prospect as underwear fabric.
Accompanying drawing explanation
Fig. 1 is red bean suede shell fabric with health care function surface fine hair pictorial diagram.
Fig. 2 is red bean suede shell fabric with health care function local microscope figure.
Fig. 3 is that red bean velvet fabric antibacterial activity composition after antibiotic finish is attached to the schematic diagram of fiber surface.
Fig. 4 is that red bean velvet fabric antibacterial activity composition after antibiotic finish enters the schematic diagram of fibrous inside.
Fig. 5, Fig. 6 are red bean suede shell fabric with health care function anti-microbial property examining report.
Fig. 7 is the wearability examining report of red bean suede shell fabric with health care function.
Detailed description of the invention
Below in conjunction with concrete drawings and Examples, the invention will be further described.
Bleeding agent used in the present invention is XP-50 or XP-70 non-ionic surface active agent, and producer is German BASF Chemical Co., Ltd.; Dispersant used in the present invention is poly carboxylic acid derivative's dispersing agent C F, and producer is Suzhou Liansheng Chemicals Co., Ltd..
Embodiment 1: a kind of red bean suede shell fabric with health care function, adopts following processing step:
(1) making of red bean velvet fabric:
A, raw material adopt 100% cotton combed yarn, and fineness of yarn is that 32 English prop up, and yarn twist factor is 325;
B, knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, yarn is woven into fabric by the double knit weft machine of pin number 24 pins/inch;
C, refining, bleaching: refining and bleaching are carried out to the fabric that step (b) obtains;
The condition of described refining is: refining liquid component is: the knitting refining agent 729 of 3g/L, 1g/L soda ash, and surplus is water; Refining bath raio is 10:1, and refining temperature is 90 DEG C, and refining time is 50min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 1%, and bleaching bath is than being 5:1, and the temperature of bleaching is 10 DEG C, and bleaching time is 15min;
D, dyeing: the fabric after step (c) process is dyeed; The process of dyeing is: fabric normal temperature enters dye, and programming rate is 1 DEG C/min, is warming up to 65 DEG C, insulation 60min, and bath raio is 10:1;
E, dyeing post processing: adopt weak cation softening agent S200 process, the addition of weak cation softening agent S200 is 3.5% of fabric weight, and bath raio is 5:1, is rolled after normal temperature dipping 5min, and pick-up is 50%, then 140 DEG C of oven dry;
F, open width dry finishing: the fabric after step (e) being processed is 25% through dewatering to moisture content, and arrange in open width drying and setting machine, temperature is 150 DEG C, and the speed of a motor vehicle is 16m/min;
Pretreatment before g, napping: fabric is successively through overboard, decatize, drying and processing, the sodium hydrate aqueous solution of overboard solution to be concentration be 0.01mol/L, bath raio is 50:1, and fabric soaks 50min in overboard solution, the temperature of drying and processing is 60 DEG C, and drying time is 10min; Then carry out decatize, steam temperature is 50 DEG C, and steam pressure during decatize is 2MPa, and steaming time is 60min;
H, napping process: the fabric after step (f) being processed carries out double-edged napping processing on roughing-up machine, and the speed of a motor vehicle of fabric is 16m/min, the rotating speed of carbon brush hair roller is 1800 turns/min;
(2) antibiotic finish:
The preparation of a, nano modification titanium dioxide: 2g titanium dioxide powder is added in 1L distilled water, then add 1g sodium hexametaphosphate dispersant, vigorous stirring 20 minutes, mixing speed is 50 revs/min to be made to be uniformly dispersed, and obtains mixed solution; Adopt concentration to be that the hydrochloric acid of 0.01mol/L regulates the pH value of mixed solution to be after 10, add 3g odium stearate, stirring reaction 10 hours, mixing speed is 30 revs/min; Filter, adopt alcohol and water washing respectively, in 110 DEG C of dryings 45 minutes, ball mill grinds, grinding rotating speed is 200 revs/min, and milling time is 100 minutes, obtains nano-titanium dioxide powder; Be added to the water by nano-titanium dioxide powder, and add the PEG of 5g, vigorous stirring reacts 6 hours, and mixing speed is 200 revs/min; After filtration, respectively with water and ethanol washing, then in 80 DEG C of dryings 10 hours; Grind on dispersion mill, grinding rotating speed is 200 revs/min, and milling time is 100 minutes, obtains nano modification titanium dioxide again;
B, the red bean velvet fabric that step (1) obtains to be arranged in antiseptic; The composition of described antiseptic is: nano modification titanium dioxide: 1.5%o.w.f, bleeding agent XP5:2%o.w.f, dispersing agent C F:1%o.w.f; Stir 30 minutes at normal temperatures by after nano modification titanium dioxide, bleeding agent and dispersant, mixing speed is 150 revs/min, and fabric is processed 5min in antiseptic, and bath raio is 5:1, and treatment temperature is 140 DEG C;
(3) stentering forming arranges: the red bean velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 DEG C, and the speed of a motor vehicle of fabric is 15m/min, and upper overfeed ratio is 25%;
(4) organosilicon, Organic fluoride arrange: described silicone finish adopts block amino-silicone oil softening agent S200, consumption is 3.5% of fabric weight, and bath raio is 5:1, is rolled after fabric is flooded 5min at normal temperatures, pick-up is 50%, then dries 15 minutes at 120 DEG C; Described Organic fluoride arranges and adopts HS1100 type self-cross linking type Organic fluoride finishing agent, and consumption is 1.5% of fabric weight, is rolled after fabric is flooded 3min at normal temperatures, and pick-up is 50%, then after 10 minutes, bakes 5min in 120 DEG C at 80 DEG C of preliminary dryings.
Embodiment 2: a kind of red bean suede shell fabric with health care function, adopts following processing step:
(1) making of red bean velvet fabric:
A, raw material adopt 100% cotton combed yarn, and fineness of yarn is that 36 English prop up, and yarn twist factor is 330;
B, knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, yarn is woven into fabric by the double knit weft machine of pin number 24 pins/inch;
C, refining, bleaching: refining and bleaching are carried out to the fabric that step (b) obtains;
The condition of described refining is: refining liquid component is: the knitting refining agent 729 of 7g/L, 5g/L soda ash, and surplus is water; Refining bath raio is 20:1, and refining temperature is 100 DEG C, and refining time is 45min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 40%, and bleaching bath is than being 20:1, and the temperature of bleaching is 45 DEG C, and bleaching time is 5min;
D, dyeing: the fabric after step (c) process is dyeed; The process of dyeing is: fabric normal temperature enters dye, and programming rate is 1.5 DEG C/min, is warming up to 70 DEG C, insulation 50min, and bath raio is 20:1;
E, dyeing post processing: adopt weak cation softening agent S200 process, the addition of weak cation softening agent S200 is 4.5% of fabric weight, and bath raio is 30:1, is rolled after normal temperature dipping 1min, and pick-up is 80%, then 180 DEG C of oven dry;
F, open width dry finishing: the fabric after step (e) being processed is 35% through dewatering to moisture content, and arrange in open width drying and setting machine, temperature is 165 DEG C, and the speed of a motor vehicle is 16m/min;
Pretreatment before g, napping: fabric is successively through overboard, decatize, drying and processing, the potassium hydroxide aqueous solution of overboard solution to be concentration be 1mol/L, bath raio is 100:1, and fabric soaks 1min in overboard solution, the temperature of drying and processing is 90 DEG C, and drying time is 3min; Then carry out decatize, steam temperature is 105 DEG C, and steam pressure during decatize is 10MPa, and steaming time is 5min;
H, napping process: the fabric after step (f) being processed carries out double-edged napping processing on roughing-up machine, and the speed of a motor vehicle of fabric is 18m/min, the rotating speed of carbon brush hair roller is 2000 turns/min;
(2) antibiotic finish:
The preparation of a, nano modification titanium dioxide: 15g titanium dioxide powder is added in 1L distilled water, then add 4g sodium hexametaphosphate dispersant, vigorous stirring 5 minutes, mixing speed is 150 revs/min to be made to be uniformly dispersed, and obtains mixed solution; Adopt concentration to be that the hydrochloric acid of 0.5mol/L regulates the pH value of mixed solution to be after 11, add 10g odium stearate, stirring reaction 3 hours, mixing speed is 100 revs/min; Filter, adopt alcohol and water washing respectively, in 150 DEG C of dryings 5 minutes, ball mill grinds, grinding rotating speed is 1000 revs/min, and milling time is 30 minutes, obtains nano-titanium dioxide powder; Be added to the water by nano-titanium dioxide powder, and add the PEG of 10g, vigorous stirring reacts 1 hour, and mixing speed is 1000 revs/min; After filtration, respectively with water and ethanol washing, then in 120 DEG C of dryings 3 hours; Grind on dispersion mill, grinding rotating speed is 1000 revs/min, and milling time is 30 minutes, obtains nano modification titanium dioxide again;
B, the red bean velvet fabric that step (1) obtains to be arranged in antiseptic; The composition of described antiseptic is: nano modification titanium dioxide: 5%o.w.f, bleeding agent XP70:5%o.w.f, dispersing agent C F:3 %o.w.f; Stir 5 minutes at normal temperatures by after nano modification titanium dioxide, bleeding agent and dispersant, mixing speed is 300 revs/min, and fabric is processed 1min in antiseptic, and bath raio is 40:1, and treatment temperature is 190 DEG C;
(3) stentering forming arranges: the red bean velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 190 DEG C, and the speed of a motor vehicle of fabric is 25m/min, and upper overfeed ratio is 35%;
(4) organosilicon, Organic fluoride arrange: described silicone finish adopts block amino-silicone oil softening agent S200, consumption is 4.5% of fabric weight, and bath raio is 20:1, is rolled after fabric is flooded 1min at normal temperatures, pick-up is 80%, then dries 5 minutes at 140 DEG C; Described Organic fluoride arranges and adopts HS1100 type self-cross linking type Organic fluoride finishing agent, and consumption is 3.5% of fabric weight, is rolled after fabric is flooded 1min at normal temperatures, and pick-up is 80%, then after 3 minutes, bakes 1min in 160 DEG C at 100 DEG C of preliminary dryings.
Embodiment 3: a kind of red bean suede shell fabric with health care function, adopts following processing step:
(1) making of red bean velvet fabric:
A, raw material adopt 100% cotton combed yarn, and fineness of yarn is that 40 English prop up, and yarn twist factor is 330;
B, knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, yarn is woven into fabric by the double knit weft machine of pin number 24 pins/inch;
C, refining, bleaching: refining and bleaching are carried out to the fabric that step (b) obtains;
The condition of described refining is: refining liquid component is: the knitting refining agent 729 of 5g/L, 2g/L soda ash, and surplus is water; Refining bath raio is 15:1, and refining temperature is 95 DEG C, and refining time is 46min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 20%, and bleaching bath is than being 10:1, and the temperature of bleaching is 30 DEG C, and bleaching time is 10min;
D, dyeing: the fabric after step (c) process is dyeed; The process of dyeing is: fabric normal temperature enters dye, and programming rate is 1 DEG C/min, is warming up to 66 DEG C, insulation 55min, and bath raio is 15:1;
E, dyeing post processing: adopt weak cation softening agent S200 process, the addition of weak cation softening agent S200 is 4% of fabric weight, and bath raio is 20:1, is rolled after normal temperature dipping 4min, and pick-up is 60%, then 160 DEG C of oven dry;
F, open width dry finishing: the fabric after step (e) being processed is 30% through dewatering to moisture content, and arrange in open width drying and setting machine, temperature is 155 DEG C, and the speed of a motor vehicle is 15m/min;
Pretreatment before g, napping: fabric is successively through overboard, decatize, drying and processing, the aqueous sodium carbonate of overboard solution to be concentration be 0.05mol/L, bath raio is 60:1, and fabric soaks 20min in overboard solution, the temperature of drying and processing is 80 DEG C, and drying time is 5min; Then carry out decatize, steam temperature is 100 DEG C, and steam pressure during decatize is 5MPa, and steaming time is 20min;
H, napping process: the fabric after step (f) being processed carries out double-edged napping processing on roughing-up machine, and the speed of a motor vehicle of fabric is 17m/min, the rotating speed of carbon brush hair roller is 1900 turns/min;
(2) antibiotic finish:
The preparation of a, nano modification titanium dioxide: 10g titanium dioxide powder is added in 1L distilled water, then add 2g sodium hexametaphosphate dispersant, vigorous stirring 10 minutes, mixing speed is 100 revs/min to be made to be uniformly dispersed, and obtains mixed solution; Adopt concentration to be that the hydrochloric acid of 0.2mol/L regulates the pH value of mixed solution to be after 10, add 6g odium stearate, stirring reaction 5 hours, mixing speed is 50 revs/min; Filter, adopt alcohol and water washing respectively, in 120 DEG C of dryings 15 minutes, ball mill grinds, grinding rotating speed is 500 revs/min, and milling time is 60 minutes, obtains nano-titanium dioxide powder; Be added to the water by nano-titanium dioxide powder, and add the PEG of 6g, vigorous stirring reacts 2 hours, and mixing speed is 500 revs/min; After filtration, respectively with water and ethanol washing, then in 100 DEG C of dryings 6 hours; Grind on dispersion mill, grinding rotating speed is 500 revs/min, and milling time is 60 minutes, obtains nano modification titanium dioxide again;
B, the red bean velvet fabric that step (1) obtains to be arranged in antiseptic; The composition of described antiseptic is: nano modification titanium dioxide: 4%o.w.f, bleeding agent XP50:4%o.w.f, dispersing agent C F:2%o.w.f; Stir 20 minutes at normal temperatures by after nano modification titanium dioxide, bleeding agent and dispersant, mixing speed is 200 revs/min, and fabric is processed 2min in antiseptic, and bath raio is 20:1, and treatment temperature is 160 DEG C;
(3) stentering forming arranges: the red bean velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 160 DEG C, and the speed of a motor vehicle of fabric is 20m/min, and upper overfeed ratio is 30%;
(4) organosilicon, Organic fluoride arrange: described silicone finish adopts block amino-silicone oil softening agent S200, consumption is 4% of fabric weight, and bath raio is 10:1, is rolled after fabric is flooded 4min at normal temperatures, pick-up is 60%, then dries 10 minutes at 130 DEG C; Described Organic fluoride arranges and adopts HS1100 type self-cross linking type Organic fluoride finishing agent, and consumption is 3% of fabric weight, is rolled after fabric is flooded 2min at normal temperatures, and pick-up is 60%, then after 6 minutes, bakes 4in in 150 DEG C at 90 DEG C of preliminary dryings.
Fig. 1 is the surperficial fine hair figure of the red bean suede shell fabric with health care function that embodiment 3 obtains, and as seen from Figure 1, the length of the fine hair of web surface reaches 0.45cm.
Fig. 2 is the microscope figure after the red bean suede shell fabric with health care function collodion that obtains of embodiment 3 infiltrates.
The present invention weaves red bean velvet fabric to cotton textiles and carries out antiseptic arrangement, be compared to the defects such as traditional natural fiber antibacterial finishing process need use a large amount of chemical cross-linking agents, washing poor stability, easy to change and feel to harden, antibacterial activity nano-mineral is attached on fiber by physical method by present invention process, form the cavity structure of uniform fine and close tapetum and cotton fiber at web surface in conjunction with the unique sanding of red bean velvet fabric, nano-mineral is made effectively to be attached on fiber or to penetrate into fiber lumen inside, without the need to additionally using chemical cross-linking agent.As shown in Figure 3, for red bean velvet fabric antibacterial activity composition (being nano modification titanium dioxide in the present invention) after antibiotic finish is distributed in the schematic diagram of fiber surface.Fig. 4 is the schematic diagram that antibacterial activity composition enters fiber lumen inside.
As shown in Figure 5, Figure 6, for the anti-microbial property examining report of red bean suede shell fabric with health care function, adopting FZ/T73023-2006(AAA) after standard wash 50 times, staphylococcus aureus bacteriostasis rate reaches 90.6%, Escherichia coli bacteriostasis rate reaches 83.8%, Candida albicans bacteriostasis rate 80.3%.
As shown in Figure 7, be the wearability examining report of red bean suede shell fabric with health care function.Wherein, content of formaldehyde is: do not detect, and method of testing adopts GB/T2912.1-2009.
PH value is 6.2, and method of testing is GB/T7573-2009(0.1mol/L KCl solution), critical field is 4.0 ~ 7.5.
The color fastness of resistance to saliva test result is: former state variable color fastness is 4 grades, and staining (cotton) fastness is 4 grades, and staining (wool) fastness is 4 grades, and method of testing is GB/T18886-2002, standard-required >=4 grade.
Washing size changing rate (%) result is: straight is-1.5% to rate of change, and cross directional variations rate is-1.3%; Method of testing is GT/T8628-2001, GB/T8629-2001(5A/A), GT/T8630-2002, standard-required is-3.0% ~+2.0%.
Bursting strength (N) is 440, test side for GB/T19976-2005(steel in diameter be 38mm), standard-required is >=250.
Balling-up (level) result is 3 ~ 4 grades, and method of testing is GB/T4802.1-2008(ballast 780cN, balling-up 600 times).
Fastness to soaping (level) result is, variable color fastness is 4 grades, and staining (cotton) fastness is 4 grades, and staining (wool) fastness is 4 grades; Method of testing is GB/T3921-2008, standard-required >=4 grade.
Colour fastness to rubbing (level) result is: unlubricated friction fastness is 4 ~ 5 grades, and wet fastness of rubbing is 4 grades; Method of testing is GB/T3920-2008, standard-required unlubricated friction >=4 grade, wet to rub >=3 ~ 4 grades.
Acidproof PERSPIRATION COLOR FASTNESS (level) result is: variable color fastness is 4 grades, and staining (cotton) fastness is 4 grades, and staining (wool) fastness is 4 grades; Method of testing is GB/T3922-1995, standard-required >=4 grade.
Alkaline-resisting PERSPIRATION COLOR FASTNESS (level) result is: variable color fastness is 4 grades, and staining (cotton) fastness is 4 grades, and staining (wool) fastness is 4 grades; Method of testing is GB/T3922-1995, standard-required >=4 grade.
Color fastness to water (level) result is: variable color fastness is 4 grades, and staining (cotton) fastness is 4 grades, and staining (wool) fastness is 4 grades; Method of testing is GB/T5713-1997, standard-required >=4 grade.
Heat-insulating property result is: clo value (CLO) is 0.2111, and insulation rate (%) is 24.05; Method of testing is GB/T11048-1989.
Claims (6)
1. a red bean suede shell fabric with health care function, is characterized in that, adopts following manufacture technics:
(1) making of red bean velvet fabric:
A, raw material adopt 100% cotton combed yarn, and fineness of yarn is that 32 ~ 40 English prop up, and yarn twist factor is 325 ~ 330;
B, knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, yarn is woven into fabric by the double knit weft machine of pin number 24 pins/inch;
C, refining, bleaching: refining and bleaching are carried out to the fabric that step (b) obtains;
The condition of described refining is: refining liquid component is: the knitting refining agent 729 of 3 ~ 7g/L, 1 ~ 5g/L soda ash, and surplus is water; Refining bath raio is 10 ~ 20:1, and refining temperature is 90 ~ 100 DEG C, and refining time is 45 ~ 50min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 1% ~ 40%, and bleaching bath ratio is 5 ~ 20:1, and the temperature of bleaching is 10 ~ 45 DEG C, and bleaching time is 5 ~ 15min;
D, dyeing: the fabric after step (c) process is dyeed;
E, dyeing post processing: adopt weak cation softening agent S200 process, the addition of weak cation softening agent S200 is 3.5 ~ 4.5% of fabric weight, and bath raio is 5 ~ 30:1, is rolled after normal temperature dipping 1 ~ 5min, pick-up is 50% ~ 80%, then 140 DEG C ~ 180 DEG C oven dry;
F, open width dry finishing: the fabric after step (e) being processed is 25 ~ 35% through dewatering to moisture content, and arrange in open width drying and setting machine, temperature is 150 ~ 165 DEG C, and the speed of a motor vehicle is 15 ~ 16m/min;
Pretreatment before g, napping: fabric is successively through overboard, decatize, drying and processing, the alkaline aqueous solution of overboard solution to be concentration be 0.01 ~ 1mol/L, bath raio is 50 ~ 100:1, and fabric soaks 1 ~ 50min in overboard solution, the temperature of drying and processing is 60 ~ 90 DEG C, and drying time is 3 ~ 10min; Then carry out decatize, steam temperature is 50 ~ 105 DEG C, and steam pressure during decatize is 2MPa ~ 10MPa, and steaming time is 5 ~ 60min;
H, napping process: the fabric after step (f) being processed carries out double-edged napping processing on roughing-up machine, and the speed of a motor vehicle of fabric is 16 ~ 18m/min, the rotating speed of carbon brush hair roller is 1800 ~ 2000 turns/min;
(2) antibiotic finish: the red bean velvet fabric that step (1) obtains is arranged in antiseptic; The composition of described antiseptic is: nano modification titanium dioxide: 1.5 ~ 5%o.w.f, bleeding agent: 2 ~ 5%o.w.f, dispersant: 1 ~ 3 %o.w.f; Stir 5 ~ 30 minutes at normal temperatures by after nano modification titanium dioxide, bleeding agent and dispersant, mixing speed is 150 ~ 300 revs/min, and fabric is processed 1 ~ 5min in antiseptic, and bath raio is 5 ~ 40:1, and treatment temperature is 140 ~ 190 DEG C;
(3) stentering forming arranges: the red bean velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 ~ 190 DEG C, and the speed of a motor vehicle of fabric is 15 ~ 25m/min, and upper overfeed ratio is 25 ~ 35%;
(4) organosilicon, Organic fluoride arrange: described silicone finish adopts block amino-silicone oil softening agent S200, consumption is 3.5 ~ 4.5% of fabric weight; bath raio is 5 ~ 20:1; be rolled after fabric is flooded 1 ~ 5min at normal temperatures; pick-up is 50% ~ 80%, then dries 5 ~ 15 minutes at 120 ~ 140 DEG C; Described Organic fluoride arranges and adopts HS1100 type self-cross linking type Organic fluoride finishing agent, consumption is 1.5 ~ 3.5% of fabric weight, be rolled after fabric is flooded 1 ~ 3min at normal temperatures, pick-up is 50% ~ 80%, after 3 ~ 10 minutes, 1 ~ 5min is baked in 120 ~ 160 DEG C again at 80 ~ 100 DEG C of preliminary dryings.
2. the manufacture craft of red bean suede shell fabric with health care function as claimed in claim 1, it is characterized in that: the process dyeed in described step (1) operation d is: fabric normal temperature enters dye, and programming rate is 1 ~ 1.5 DEG C/min, is warming up to 65 ~ 70 DEG C, insulation 50 ~ 60min, bath raio is 10:1 ~ 20:1.
3. the manufacture craft of red bean suede shell fabric with health care function as claimed in claim 1, is characterized in that: described bleeding agent is bleeding agent XP50 or XP70.
4. the manufacture craft of red bean suede shell fabric with health care function as claimed in claim 1, is characterized in that: described dispersant is dispersing agent C F.
5. the manufacture craft of red bean suede shell fabric with health care function as claimed in claim 1, is characterized in that: described overboard solution is one or more the aqueous solution in NaOH, potassium hydroxide, sodium carbonate, sodium acid carbonate, sodium hydrogen phosphate, dibastic sodium phosphate or sodium phosphate.
6. the manufacture craft of red bean suede shell fabric with health care function as claimed in claim 1, it is characterized in that: in described step (2), the preparation method of nano modification titanium dioxide is: added by 2 ~ 15g titanium dioxide powder in 1L distilled water, add 1 ~ 4g sodium hexametaphosphate dispersant again, vigorous stirring 5 ~ 20 minutes, mixing speed is 50 ~ 150 revs/min to be made to be uniformly dispersed, and obtains mixed solution; Adopt concentration to be that the hydrochloric acid of 0.01 ~ 0.5mol/L regulates the pH value of mixed solution to be after 10 ~ 11, add 3 ~ 10g odium stearate, stirring reaction 3 ~ 10 hours, mixing speed is 30 ~ 100 revs/min; Filter, adopt alcohol and water washing respectively, in 110 ~ 150 DEG C of dryings 5 ~ 45 minutes, ball mill grinds, grinding rotating speed is 200 ~ 1000 revs/min, and milling time is 30 ~ 100 minutes, obtains nano-titanium dioxide powder; Be added to the water by nano-titanium dioxide powder, and add the PEG of 5 ~ 10g, vigorous stirring reaction 1 ~ 6 hour, mixing speed is 200 ~ 1000 revs/min; After filtration, respectively with water and ethanol washing, then in 80 ~ 120 DEG C of dryings 3 ~ 10 hours; Grind on dispersion mill, grinding rotating speed is 200 ~ 1000 revs/min, and milling time is 30 ~ 100 minutes, obtains nano modification titanium dioxide again.
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Effective date of registration: 20191211 Address after: 214199 Xixing Port Road, Donggang Town, Xishan District, Wuxi City, Jiangsu Province Patentee after: Wuxi Hongdou Weaving Co., Ltd Address before: 214199 science and Technology Office of Wuxi red bean Group Co., Ltd., Donggang Town, Xishan District, Jiangsu Patentee before: Wuxi Hodohome Garment Co., Ltd. |