CN106087219A - The preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function - Google Patents

The preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function Download PDF

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Publication number
CN106087219A
CN106087219A CN201610731261.XA CN201610731261A CN106087219A CN 106087219 A CN106087219 A CN 106087219A CN 201610731261 A CN201610731261 A CN 201610731261A CN 106087219 A CN106087219 A CN 106087219A
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fabric
semen phaseoli
far
infrared magnetic
preparation
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周文江
张洪波
蒋春熬
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WUXI HODOHOME GARMENT CO Ltd
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WUXI HODOHOME GARMENT CO Ltd
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Priority to CN201610731261.XA priority Critical patent/CN106087219A/en
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    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04BKNITTING
    • D04B1/00Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
    • D04B1/14Other fabrics or articles characterised primarily by the use of particular thread materials
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • D06B3/18Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06CFINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C11/00Teasing, napping or otherwise roughening or raising pile of textile fabrics
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/80Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/18Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/20Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01Natural vegetable fibres
    • D10B2201/02Cotton
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20Cellulose-derived artificial fibres
    • D10B2201/22Cellulose-derived artificial fibres made from cellulose solutions
    • D10B2201/24Viscose
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2321/00Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D10B2321/02Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polyolefins
    • D10B2321/022Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polyolefins polypropylene

Abstract

The present invention relates to the preparation method of a kind of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function, carry out the preparation of Semen Phaseoli velvet fabric for raw material initially with one or more in cotton fiber, polypropylene fiber, viscose fiber, the fabric prepared sequentially passes through refine, bleaching, dyeing, dyeing post processing, open width drying and processing, napping pre-treatment and napping process, then Semen Phaseoli velvet fabric employing nano modification tourmaline powder body far-infrared magnetic functional finishing agent is arranged, after arrange through stentering forming and to prepare Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function.Preparation method of the present invention is simple, and step is easily operated, covers one layer of uniform tourmaline finish coating on the surface of Semen Phaseoli velvet fabric, washing good stability, and cloth pale face becomes, technique environmental protection and energy saving and flow process are short, as the application prospect that the performance of underwear fabric is good.

Description

The preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function
Technical field
The present invention relates to the preparation method of a kind of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function, belong to knitting fabric system Standby technical field.
Background technology
Along with the progress and development of science, people are in addition to the primary demand to clothing, to having the clothing demand of New function also Day by day increasing.As underwear fabric, the fabric with far infrared and magnetic property dual-use function can pass through the magnetic line of force, far infrared The deep layer of skin is penetrated by line, accelerates blood circulation, improves microcirculating state, promotes human metabolism, has health care with auxiliary Help the effect of insulation.
Summary of the invention
The invention aims to solve prior art and at cotton textiles and carry out the reddest with the fabric of chemical fibre blending Outward, the problem that magnetic/functionalized arrangement is easy to change, washing fastness is low, fabric hardens, it is provided that Semen Phaseoli floss far-infrared magnetic performance keeps healthy The preparation method of functional fabric.
The present invention adopts the following technical scheme that the preparation method of a kind of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function, Comprise the steps:
(1) preparation of Semen Phaseoli velvet fabric:
A. with one or more fiber blends in cotton fiber, polypropylene fiber, viscose fiber as raw material, fineness of yarn be 21~ 50 English prop up, and yarn twist factor is 325~330;
B. knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, the one side of pin number 24 pins/inch Yarn is woven into fabric by knitting weft machine;
C. refine, bleaching: the fabric obtaining step (b) carries out refine and bleaching, refine bath raio is 10~20:1, refine temperature Degree is 90~100 DEG C, and refining time is 45~50min, and bleaching bath ratio is 5~20:1, and the temperature of bleaching is 10~45 DEG C, bleaching Time is 5~15min;
D. dyeing: the fabric after bleaching is carried out dyeing process;
E. dye post processing: using weak cation softening agent to process, the addition of weak cation softening agent is fabric weight 3.5~4.5%, bath raio is 5~30:1, rolls after normal temperature dipping 1~5min, and pick-up is 50%~80%, in 140 DEG C ~180 DEG C of conditions decline fabric and dry;
F. open width dry finishing: the fabric after process is 25~35% through being dehydrated to moisture content, enters in open width drying and setting machine Row arranges;
G. pretreatment before napping: fabric napping process before successively through overboard, decatize, drying and processing,;
H. napping processes: the fabric after processing carries out double-edged napping processing on roughing-up machine, and the speed of fabric is 16 ~the rotating speed of 18m/min, carbon brush hair roller is 1800~2000 turns/min, obtain Semen Phaseoli velvet fabric;
(2) finishing functions of Semen Phaseoli velvet fabric: the Semen Phaseoli velvet fabric that step (1) obtains is placed in nano modification tourmaline far infrared Magnetic functional finishing agent arranges;In described nano modification tourmaline far-infrared magnetic functional finishing agent, each component is: nanometer changes Property tourmaline powder body: 1.5 ~ 5g/L, penetrating agent: 2 ~ 5% g/L, dispersant: 1 ~ 3 g/L, coupling agent 1-5 g/L;By nano modification The method of tourmaline far-infrared magnetic functional finishing agent uniform application or dipping contacts with Semen Phaseoli velvet fabric, then at pressure 0.5MPa Rolling Semen Phaseoli velvet fabric along coat side under ~ 10MPa, treatment temperature is 140~190 DEG C, processes time 0.5 ~ 5min, obtains Semen Phaseoli floss Far-infrared magnetic performance shell fabric with health care function;
(3) stentering forming arranges: the Semen Phaseoli velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 ~ 190 DEG C, the speed of fabric is 15 ~ 25m/min, and upper overfeed ratio is 25 ~ 35%.
Further, described penetrating agent be nonionic surfactant XP-50, nonionic surfactant XP-70, alkyl One or more in alcohol sulfuric acid, alkylsulfonate or phosphate compound.
Further, described dispersant is poly carboxylic acid derivative dispersing agent C F, fatty alcohol-polyoxyethylene ether, alkyl phenol polyoxy One or more in vinyl Ether, aliphatic acid polyethenoxy ether, tristerin, liquid paraffin.
Further, described coupling agent is zirconium aluminate low molecule inorganic polymer, monoalkoxytitanates, gamma-amino third One or more mixing in ethyl triethoxy silicane alkane, monoalkoxy vinyl Ether, many alkoxy vinyl ether, titanate esters.
Further, the preparation method of the nano modification tourmaline far-infrared magnetic functional finishing agent in described step (2) is: By one or more in iron tourmaline powder body, dravite powder body, elbaite powder body according to concentration be 1.5 ~ 5 g/L add Distilled water carries out mix and blend, adds 1~4g sodium hexameta phosphate, is stirred vigorously 5~20 min, and mixing speed is 50~150 Rad/ min makes to be uniformly dispersed, and obtains nano modification tourmaline mixed solution;Add is that 1.5 ~ 5g/L coupling agent, 2 ~ 5g/L ooze Agent and 1 ~ 3g/L dispersant thoroughly, stirring reaction 3~10 h, mixing speed is 30~100 rad/ min;Obtain nano modification torr Agate beautiful jade far-infrared magnetic functional finishing agent.
Further, described iron tourmaline powder body, dravite powder body, the size of elbaite powder body are 0.5- 100nm。
Further, the refining liquid component in described step (1) is: 3~7g/L knitting refining agents 729,1~5g/L are pure Alkali, surplus is water.
Further, the bleaching liquid in described step (1) is concentration 1~the hydrogen peroxide of 40%.
Further, the arrangement temperature of described open width collator is 150~165 DEG C, and speed is 15~16m/min.
Further, time overboard in described step (1) solution be concentration be the alkaline aqueous solution of 0.01~1mol/L, bath raio Being 50~100:1, fabric soaks 1~50min in overboard solution, and the temperature of drying and processing is 60~90 DEG C, and drying time is 3 ~10min;Then carrying out decatize, steam temperature is 50~105 DEG C, and steam pressure during decatize is 2MPa~10MPa, during decatize Between be 5~60min.
Preparation method of the present invention is simple, and step is easily operated, covers one layer of uniform torr agate on the surface of Semen Phaseoli velvet fabric Beautiful jade finish coating, washes good stability, and cloth pale face becomes, and technique environmental protection and energy saving and flow process are short, as underwear fabric table The best application prospect.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further illustrated.
Penetrating agent in the present invention is XP-50 or XP-70 nonionic surfactant, and being purchased from outward Germany's BASF chemical industry has Limit company;Dispersant is poly carboxylic acid derivative dispersing agent C F, is purchased from outward Suzhou Liansheng Chemicals Co., Ltd.;Weak cation softening agent It is purchased from Chemical Reagent Co., Ltd., Sinopharm Group outside S200, is purchased from Suzhou Liansheng Chemicals Co., Ltd. outside knitting refining agent 729 public Department.
Embodiment one:
The preparation method of a kind of Semen Phaseoli floss far infrared heating magnetic property healthcare face fabric, comprises the steps:
(1) preparation of Semen Phaseoli velvet fabric:
A. raw material uses cotton fiber, polypropylene fiber blending, and fineness of yarn is that 40 English prop up, and yarn twist factor is 330;
B. knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, the Fructus Zanthoxyli Dissiti of pin number 24 pins/inch Knit weft machine and yarn is woven into fabric;
C. refine, bleaching: the fabric obtaining step (b) carries out refine and bleaching;
The condition of refine is: refining liquid component is: the knitting refining agent of 3g/L 729,5g/L soda, and surplus is water;Refine bath raio is 20:1, refining temperature is 90 DEG C, and refining time is 45min;
The condition of bleaching is: bleaching liquid is the hydrogen peroxide of concentration 10%, and bleaching bath ratio is for 20:1, and the temperature of bleaching is 45 DEG C, bleaching Time is 15min;
D. dyeing: the fabric after step (c) processes is dyeed;
E. dye post processing: using weak cation softening agent S200 process, the addition of weak cation softening agent S200 is The 3.5% of fabric weight, bath raio is 30:1, rolls after normal temperature dipping 5min, and pick-up is 80%, then 180 DEG C of drying;
F. open width dry finishing: the fabric after step (e) being processed is 35% through dehydration to moisture content, at open width drying and setting machine In arrange, temperature is 165 DEG C, and speed is 16m/min;
G. pretreatment before napping: fabric successively through overboard, decatize, drying and processing, overboard solution be concentration be the alkali of 0.01mol/L Property aqueous solution, bath raio is 100:1, and fabric soaks 50min in overboard solution, and the temperature of drying and processing is 90 DEG C, drying time For 10min;Then carrying out decatize, steam temperature is 105 DEG C, and steam pressure during decatize is 10MPa, and steaming time is 60min;
H. napping processes: the fabric after step (f) being processed carries out double-edged napping processing, the car of fabric on roughing-up machine Speed is 2000 turns/min for 18m/min, the rotating speed of carbon brush hair roller;
(2) nano modification tourmaline powder body far-infrared magnetic finishing functions: Semen Phaseoli velvet fabric step (1) obtained is at nano modification Tourmaline far-infrared magnetic functional finishing agent arranges;The composition of nano modification tourmaline far-infrared magnetic functional finishing agent is: Nano modification tourmaline powder body: 1.5 ~ 5g/L, penetrating agent: 2 ~ 5% g/L, dispersant: 1 ~ 3 g/L, coupling agent 1-5 g/L;To receive Stirring 30 minutes at normal temperatures after rice modifying titanium dioxide, penetrating agent and dispersant, mixing speed is 150 revs/min, will Nano modification tourmaline far-infrared magnetic functional finishing agent uniform application forms uniform coating at web surface, then at pressure Rolling fabric along coat side under 10MPa pressure, treatment temperature is 190 DEG C, processes time 5min;
The preparation method of nano modification tourmaline far-infrared magnetic functional finishing agent: be 1.5g/L according to concentration by iron tourmaline powder body Adding distilled water and carry out mix and blend, add 1g sodium hexameta phosphate, be stirred vigorously 20 min, mixing speed is 50 rad/ Min makes to be uniformly dispersed, and obtains nano modification tourmaline mixed solution;Add as 1.5g/L coupling agent, 2g/L penetrating agent and 1g/ L dispersant, stirring reaction 3 h, mixing speed is 100 rad/ min;Obtain nano modification tourmaline far-infrared magnetic finishing functions Agent.
Penetrating agent is nonionic surfactant XP-50;
Dispersant is poly carboxylic acid derivative dispersing agent C F, liquid paraffin;
Coupling agent is zirconium aluminate low molecule inorganic polymer, many alkoxy vinyl ether, titanate esters;
(3) stentering forming arranges: the Semen Phaseoli velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 ~ 190 DEG C, the speed of fabric is 15 ~ 25m/min, and upper overfeed ratio is 25 ~ 35%, obtains Semen Phaseoli floss far-infrared magnetic performance health care face Material.
Embodiment two:
The preparation method of a kind of Semen Phaseoli floss far infrared heating magnetic property healthcare face fabric, comprises the steps:
(1) preparation of Semen Phaseoli velvet fabric:
A. raw material uses cotton fiber, polypropylene fiber, three kinds of fiber blends of viscose fiber, and fineness of yarn is that 32 English prop up, and system twisted with the fingers by yarn Number is 325;
B. knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, the Fructus Zanthoxyli Dissiti of pin number 24 pins/inch Knit weft machine and yarn is woven into fabric;
C. refine, bleaching: the fabric obtaining step (b) carries out refine and bleaching;
The condition of described refine is: refining liquid component is: the knitting refining agent of 5g/L 729,4g/L soda, and surplus is water;Refine is bathed Ratio is 20:1, and refining temperature is 90 DEG C, and refining time is 45min;
The condition of described bleaching is: bleaching liquid is the hydrogen peroxide of concentration 15%, and bleaching bath is than for 20:1, and the temperature of bleaching is 45 DEG C, Bleaching time is 10min;
D. dyeing: the fabric after step (c) processes is dyeed;
E. dye post processing: using weak cation softening agent S200 process, the addition of weak cation softening agent S200 is The 3.5% of fabric weight, bath raio is 25:1, rolls after normal temperature dipping 5min, and pick-up is 80%, then 180 DEG C of drying;
F. open width dry finishing: the fabric after step (e) being processed is 35% through dehydration to moisture content, at open width drying and setting machine In arrange, temperature is 165 DEG C, and speed is 16m/min;
G. pretreatment before napping: fabric successively through overboard, decatize, drying and processing, overboard solution be concentration be 0.01~1mol/L Alkaline aqueous solution, bath raio is 50:1, and fabric soaks 1min in overboard solution, and the temperature of drying and processing is 90 DEG C, during drying Between be 3min;Then carrying out decatize, steam temperature is 105 DEG C, and steam pressure during decatize is 10MPa, and steaming time is 15min;
H. napping processes: the fabric after step (f) being processed carries out double-edged napping processing, the car of fabric on roughing-up machine Speed is 2000 turns/min for 18m/min, the rotating speed of carbon brush hair roller;
(2) nano modification tourmaline powder body far-infrared magnetic finishing functions: Semen Phaseoli velvet fabric step (1) obtained is at nano modification Tourmaline far-infrared magnetic functional finishing agent arranges;The composition of described nano modification tourmaline far-infrared magnetic functional finishing agent For: nano modification tourmaline powder body: 4g/L, penetrating agent: 4 g/L, dispersant 2 g/L, coupling agent 2 g/L;By nano modification two Stirring at normal temperatures after titanium oxide, penetrating agent and dispersant 30 minutes, mixing speed is 300 revs/min, by nano modification Tourmaline far-infrared magnetic functional finishing agent uniform application forms uniform coating at web surface, then under pressure 5MPa pressure Rolling fabric along coat side, treatment temperature is 190 DEG C, processes time 5min;
The preparation method of nano modification tourmaline far-infrared magnetic functional finishing agent: iron tourmaline powder body, dravite powder body are pressed It is that 4g/L addition distilled water carries out mix and blend according to concentration, adds 3g sodium hexameta phosphate, be stirred vigorously 20 min, mixing speed It is that 150 rad/ min make to be uniformly dispersed, obtains nano modification tourmaline mixed solution;Add and ooze for 4g/L coupling agent, 4g/L Agent and 2g/L dispersant thoroughly, stirring reaction 3 h, mixing speed is 100 rad/ min;Obtain nano modification tourmaline far infrared Magnetic functional finishing agent;
Penetrating agent is the mixture that alkylol sulfuric acid, alkylsulfonate or phosphate compound are several;
Dispersant be fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, aliphatic acid polyethenoxy ether, tristerin, The mixture that liquid paraffin is several;
Coupling agent is in γ aminopropyltriethoxy silane, monoalkoxy vinyl Ether, many alkoxy vinyl ether, titanate esters Several mixture;
(3) stentering forming arranges: the Semen Phaseoli velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 DEG C, The speed of fabric is 25m/min, and upper overfeed ratio is 25%, obtains Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function.
Embodiment three:
The preparation method of a kind of Semen Phaseoli floss far infrared heating magnetic property healthcare face fabric, comprises the steps:
(1) preparation of Semen Phaseoli velvet fabric:
A. raw material uses cotton fiber, polypropylene fiber blending, and fineness of yarn is that 21 English prop up, and yarn twist factor is 325;
B. knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, the Fructus Zanthoxyli Dissiti of pin number 24 pins/inch Knit weft machine and yarn is woven into fabric;
C. refine, bleaching: the fabric obtaining step (b) carries out refine and bleaching;
The condition of refine is: refining liquid component is: the knitting refining agent of 7g/L 729,1g/L soda, and surplus is water;Refine bath raio is 10:1, refining temperature is 100 DEG C, and refining time is 50min;
The condition of bleaching is: bleaching liquid is the hydrogen peroxide of concentration 40%, and bleaching bath ratio is for 5:1, and the temperature of bleaching is 10 DEG C, bleaching Time is 5min;
D. dyeing: the fabric after step (c) processes is dyeed;
E. dye post processing: using weak cation softening agent S200 process, the addition of weak cation softening agent S200 is The 4.5% of fabric weight, bath raio is 5:1, rolls after normal temperature dipping 1min, and pick-up is 50%, then 140 DEG C of drying;
F. open width dry finishing: the fabric after step (e) being processed is 25% through dehydration to moisture content, at open width drying and setting machine In arrange, temperature is 150 DEG C, and speed is 15m/min;
G. pretreatment before napping: fabric successively through overboard, decatize, drying and processing, overboard solution be concentration be the alkali of 0.01mol/L Property aqueous solution, bath raio is 100:1, and fabric soaks 50min in overboard solution, and the temperature of drying and processing is 90 DEG C, drying time For 10min;Then carrying out decatize, steam temperature is 105 DEG C, and steam pressure during decatize is 2MPa, and steaming time is 5min;
H. napping processes: the fabric after step (f) being processed carries out double-edged napping processing, the car of fabric on roughing-up machine Speed is 1800 rad/min for 16m/min, the rotating speed of carbon brush hair roller;
(2) nano modification tourmaline powder body far-infrared magnetic finishing functions: Semen Phaseoli velvet fabric step (1) obtained is at nano modification Tourmaline far-infrared magnetic functional finishing agent arranges;The composition of described nano modification tourmaline far-infrared magnetic functional finishing agent For: nano modification tourmaline powder body 5g/L, penetrating agent 5 g/L, dispersant: 3 g/L, coupling agent 5 g/L;By nano modification two Stirring at normal temperatures after titanium oxide, penetrating agent and dispersant 5 minutes, mixing speed is 300 revs/min, by nano modification Tourmaline far-infrared magnetic functional finishing agent uniform application forms uniform coating at web surface, then at pressure 10MPa pressure Lower rolling fabric along coat side, treatment temperature is 190 DEG C, processes time 5min;
The preparation method of nano modification tourmaline far-infrared magnetic functional finishing agent: iron tourmaline powder body, dravite powder body are pressed It is that 5 g/L addition distilled water carry out mix and blend according to concentration, adds 4g sodium hexameta phosphate, be stirred vigorously 10 min, stirring speed Degree is that 100 rad/ min make to be uniformly dispersed, and obtains nano modification tourmaline mixed solution;Add as 5g/L coupling agent, 5g/L Penetrating agent and 3g/L dispersant, stirring reaction 8 h, mixing speed is 80 rad/ min;Obtain nano modification tourmaline far infrared Magnetic functional finishing agent;
Penetrating agent is alkylsulfonate and the mixture of phosphate compound two kinds;
Dispersant is the mixing that alkylphenol polyoxyethylene, aliphatic acid polyethenoxy ether, tristerin, liquid paraffin are several Thing;
Coupling agent be γ aminopropyltriethoxy silane, monoalkoxy vinyl Ether, many alkoxy vinyl ether, titanate esters mixed Compound;
(3) stentering forming arranges: the Semen Phaseoli velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 190 DEG C, The speed of fabric is 25m/min, and upper overfeed ratio is 35%, obtains Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function.
The Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function preparing embodiment two uses standard GB/T/T30127- 2012 standards carry out the detection of textile far infrared performance, and testing result records far infrared transmissivity and reaches more than 0.87, far infrared Radiation temperature rise can reach more than 1.7 DEG C, uses FZ/T01116-2012 standard to carry out textile magnetic property detection, and indices is equal Standard-required can be reached.

Claims (10)

1. the preparation method of a Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function, it is characterised in that: comprise the steps:
(1) preparation of Semen Phaseoli velvet fabric:
A. with one or more fiber blends in cotton fiber, polypropylene fiber, viscose fiber as raw material, fineness of yarn be 21~ 50 English prop up, and yarn twist factor is 325~330;
B. knitting: select cylinder through 34 inches, pin number 28 pins/inch or cylinder through 38 inches, the one side of pin number 24 pins/inch Yarn is woven into fabric by knitting weft machine;
C. refine, bleaching: the fabric obtaining step (b) carries out refine and bleaching, refine bath raio is 10~20:1, refine temperature Degree is 90~100 DEG C, and refining time is 45~50min, and bleaching bath ratio is 5~20:1, and bleaching temperature is 10~45 DEG C, during bleaching Between be 5~15min;
D. dyeing: the fabric after bleaching is carried out dyeing process;
E. dye post processing: using weak cation softening agent to process, the addition of weak cation softening agent is fabric weight 3.5~4.5%, bath raio is 5~30:1, rolls after normal temperature dipping 1~5min, and pick-up is 50~80%, in 140~ 180 DEG C of conditions decline fabric dries;
F. open width dry finishing: the fabric after process is 25~35% through being dehydrated to moisture content, enters in open width drying and setting machine Row arranges;
G. pretreatment before napping: fabric napping process before successively through overboard, decatize, drying and processing,;
H. napping processes: the fabric after processing carries out double-edged napping processing on roughing-up machine, and the speed of fabric is 16 ~the rotating speed of 18m/min, carbon brush hair roller is 1800~2000 turns/min, obtain Semen Phaseoli velvet fabric;
(2) finishing functions of Semen Phaseoli velvet fabric: the Semen Phaseoli velvet fabric that step (1) obtains is placed in nano modification tourmaline far infrared Magnetic functional finishing agent arranges;In described nano modification tourmaline far-infrared magnetic functional finishing agent, each component is: nanometer changes Property tourmaline powder body: 1.5 ~ 5g/L, penetrating agent: 2 ~ 5g/L, dispersant: 1 ~ 3 g/L, coupling agent 1 ~ 5 g/L;By nano modification torr The method of agate beautiful jade far-infrared magnetic functional finishing agent uniform application or dipping contacts with Semen Phaseoli velvet fabric, then pressure 0.5 ~ Rolling Semen Phaseoli velvet fabric along coat side under 10MPa, treatment temperature is 140~190 DEG C, processes time 0.5 ~ 5min, obtains Semen Phaseoli floss Far-infrared magnetic performance shell fabric with health care function;
(3) stentering forming arranges: the Semen Phaseoli velvet fabric after step (2) being processed carries out stentering forming arrangement, and temperature is 150 ~ 190 DEG C, the speed of fabric is 15 ~ 25m/min, and upper overfeed ratio is 25 ~ 35%.
2. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute State penetrating agent be nonionic surfactant XP-50, nonionic surfactant XP-70, alkylol sulfuric acid, alkyl sulfonic acid One or more in salt or phosphate compound.
3. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute State dispersant be poly carboxylic acid derivative dispersing agent C F, fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, fatty acid polyoxy second One or more in alkene ether, tristerin, liquid paraffin.
4. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute Stating coupling agent is zirconium aluminate low molecule inorganic polymer, monoalkoxytitanates, γ aminopropyltriethoxy silane, single alkane One or more mixing in ethoxy ethylene ether, many alkoxy vinyl ether, titanate esters.
5. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute The preparation method stating the nano modification tourmaline far-infrared magnetic functional finishing agent in step (2) is: by iron tourmaline powder body, magnesium electricity One or more in gas stone powder body, elbaite powder body are that 1.5 ~ 5 g/L addition distilled water carry out mix and blend according to concentration, Adding 1~4g sodium hexameta phosphate, be stirred vigorously 5~20 min, mixing speed is that 50~150 rad/ min make to be uniformly dispersed, Obtain nano modification tourmaline mixed solution;Adding is 1.5 ~ 5g/L coupling agent, 2 ~ 5g/L penetrating agent and 1 ~ 3g/L dispersant, Stirring reaction 3~10 h, mixing speed is 30~100 rad/ min;Obtain nano modification tourmaline far-infrared magnetic finishing functions Agent.
6. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute State iron tourmaline powder body, dravite powder body, the size of elbaite powder body are 0.5 ~ 100nm.
7. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute The refining liquid component stated in step (1) is: 3~7g/L knitting refining agent 729,1~5g/L soda, surplus is water.
8. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute Stating the bleaching liquid in step (1) is concentration 1~the hydrogen peroxide of 40%.
9. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: institute The arrangement temperature stating open width collator is 150~165 DEG C, and speed is 15~16m/min.
10. the preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function as claimed in claim 1, it is characterised in that: In described step (1) overboard time solution be concentration be the alkaline aqueous solution of 0.01~1mol/L, bath raio is 50~100:1, fabric Soaking 1~50min in overboard solution, the temperature of drying and processing is 60~90 DEG C, and drying time is 3~10min;Then carry out Decatize, steam temperature is 50~105 DEG C, and steam pressure during decatize is 2MPa~10MPa, and steaming time is 5~60min.
CN201610731261.XA 2016-08-26 2016-08-26 The preparation method of Semen Phaseoli floss far-infrared magnetic performance shell fabric with health care function Pending CN106087219A (en)

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