CN104153197A - Mordanting process for half shading window decoration - Google Patents
Mordanting process for half shading window decoration Download PDFInfo
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- CN104153197A CN104153197A CN201410397415.7A CN201410397415A CN104153197A CN 104153197 A CN104153197 A CN 104153197A CN 201410397415 A CN201410397415 A CN 201410397415A CN 104153197 A CN104153197 A CN 104153197A
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- mordanting
- fabric
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- sodium
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- 238000000034 method Methods 0.000 title claims abstract description 25
- 238000005034 decoration Methods 0.000 title claims abstract description 19
- 239000004744 fabric Substances 0.000 claims abstract description 67
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 238000000576 coating method Methods 0.000 claims abstract description 28
- 239000011248 coating agent Substances 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 25
- 239000002002 slurry Substances 0.000 claims abstract description 24
- 238000001816 cooling Methods 0.000 claims abstract description 23
- 239000003381 stabilizer Substances 0.000 claims abstract description 15
- 238000002360 preparation method Methods 0.000 claims abstract description 14
- 238000005096 rolling process Methods 0.000 claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 30
- 229910052760 oxygen Inorganic materials 0.000 claims description 30
- 239000001301 oxygen Substances 0.000 claims description 30
- 238000004061 bleaching Methods 0.000 claims description 26
- 239000003292 glue Substances 0.000 claims description 24
- -1 polysiloxane Polymers 0.000 claims description 22
- 239000002270 dispersing agent Substances 0.000 claims description 19
- 239000000975 dye Substances 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 16
- 238000009992 mercerising Methods 0.000 claims description 15
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000003063 flame retardant Substances 0.000 claims description 14
- 239000000985 reactive dye Substances 0.000 claims description 14
- 150000002367 halogens Chemical group 0.000 claims description 13
- 150000003017 phosphorus Chemical class 0.000 claims description 13
- 239000004814 polyurethane Substances 0.000 claims description 12
- 229920002635 polyurethane Polymers 0.000 claims description 12
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 11
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 11
- 238000004040 coloring Methods 0.000 claims description 11
- 229910052736 halogen Inorganic materials 0.000 claims description 11
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 claims description 10
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 10
- 230000006837 decompression Effects 0.000 claims description 10
- 239000013530 defoamer Substances 0.000 claims description 10
- 239000006097 ultraviolet radiation absorber Substances 0.000 claims description 8
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 7
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 7
- 230000000740 bleeding effect Effects 0.000 claims description 7
- 238000001179 sorption measurement Methods 0.000 claims description 7
- 239000004408 titanium dioxide Substances 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 6
- 238000000518 rheometry Methods 0.000 claims description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 5
- 240000007817 Olea europaea Species 0.000 claims description 5
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 5
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 5
- GKVKQZRNDGUFSY-NSGFTINJSA-L [Na+].C(C)(CCCCCC)/C(=C(/C(=O)[O-])\C(C)CCCCCC)/C(=O)[O-].[Na+] Chemical group [Na+].C(C)(CCCCCC)/C(=C(/C(=O)[O-])\C(C)CCCCCC)/C(=O)[O-].[Na+] GKVKQZRNDGUFSY-NSGFTINJSA-L 0.000 claims description 5
- 230000002411 adverse Effects 0.000 claims description 5
- 125000000129 anionic group Chemical group 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 5
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 5
- 229910000397 disodium phosphate Inorganic materials 0.000 claims description 5
- 235000019800 disodium phosphate Nutrition 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 150000002431 hydrogen Chemical class 0.000 claims description 5
- 239000004571 lime Substances 0.000 claims description 5
- 239000000395 magnesium oxide Substances 0.000 claims description 5
- 238000005517 mercerization Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 5
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 5
- 229920005646 polycarboxylate Polymers 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 238000007670 refining Methods 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 5
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 5
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 5
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 5
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- RTLULCVBFCRQKI-UHFFFAOYSA-N 1-amino-4-[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-4-sulfoanilino]-9,10-dioxoanthracene-2-sulfonic acid Chemical compound C1=2C(=O)C3=CC=CC=C3C(=O)C=2C(N)=C(S(O)(=O)=O)C=C1NC(C=1)=CC=C(S(O)(=O)=O)C=1NC1=NC(Cl)=NC(Cl)=N1 RTLULCVBFCRQKI-UHFFFAOYSA-N 0.000 claims description 4
- 239000004793 Polystyrene Substances 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
- SLETZFVTVXVPLS-UHFFFAOYSA-N [Zn].[Cd].[Ba] Chemical compound [Zn].[Cd].[Ba] SLETZFVTVXVPLS-UHFFFAOYSA-N 0.000 claims description 4
- SHLNMHIRQGRGOL-UHFFFAOYSA-N barium zinc Chemical compound [Zn].[Ba] SHLNMHIRQGRGOL-UHFFFAOYSA-N 0.000 claims description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 4
- 229920002223 polystyrene Polymers 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- RKMGAJGJIURJSJ-UHFFFAOYSA-N 2,2,6,6-tetramethylpiperidine Chemical compound CC1(C)CCCC(C)(C)N1 RKMGAJGJIURJSJ-UHFFFAOYSA-N 0.000 claims description 3
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 3
- MGFRKBRDZIMZGO-UHFFFAOYSA-N barium cadmium Chemical compound [Cd].[Ba] MGFRKBRDZIMZGO-UHFFFAOYSA-N 0.000 claims description 3
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims description 3
- 229920002401 polyacrylamide Polymers 0.000 claims description 3
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 claims description 2
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 claims description 2
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 claims description 2
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- 239000006096 absorbing agent Substances 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract description 3
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 238000009499 grossing Methods 0.000 abstract 1
- 230000000149 penetrating effect Effects 0.000 abstract 1
- 238000004043 dyeing Methods 0.000 description 10
- 239000002351 wastewater Substances 0.000 description 10
- 238000007639 printing Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 239000004753 textile Substances 0.000 description 4
- 235000014692 zinc oxide Nutrition 0.000 description 4
- 150000005686 dimethyl carbonates Chemical class 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 150000002311 glutaric acids Chemical class 0.000 description 3
- 239000010865 sewage Substances 0.000 description 3
- 230000007306 turnover Effects 0.000 description 3
- RNWHGQJWIACOKP-UHFFFAOYSA-N zinc;oxygen(2-) Chemical class [O-2].[Zn+2] RNWHGQJWIACOKP-UHFFFAOYSA-N 0.000 description 3
- 229920002334 Spandex Polymers 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 235000019628 coolness Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000004759 spandex Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 206010020843 Hyperthermia Diseases 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 210000005252 bulbus oculi Anatomy 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- 230000036031 hyperthermia Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Landscapes
- Coloring (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to a preparation process for window decoration, in particular to a mordanting process for a half shading window decoration. The process includes the steps of: fabric preparation; water mordanting paste modulation: preparing 25-45 parts by weight of an environment-friendly soft rubber, 13-18 parts of a stiff rubber, 35-47 parts of water, 1-5 parts of an efficient penetrating agent, 0.01-0.2 part of a defoaming agent, 0.2-1.5 parts of a color stabilizer, 0.5-1.5 parts of a UV absorber and 8-10 parts of a dye; mordanting and coating: placing the fabric into the aqueous mordanting paste for padding, and rolling and coating at the pressure of 0.3-0.4 Mpa and speed of 10-15 m / min by a pressure roller; smoothing treatment: desorbing pinhole slurry in the fabric subjected to mordanting and coating; and finishing: conducting first drying at 165-170 DEG C, conducting second drying at 170-175 DEG C, and then cooling by using cold wind, wherein cold wind cooling conducts 110-90 DEG C, 90-80 DEG C 78-69 DEG C 68-62 DEG C, 61-58 DEG C 57-50 DEG C 48-38 DEG C and 35-28 DEG C gradual cooling, and the cooling time is 20-27min; and finally, cooling at room temperature and coiling. The aqueous mordanting paste provided by the invention is safe and environment-friendly, and can realize green and environment-friendly production.
Description
Technical field
The present invention relates to the preparation technology of window decorations, relate in particular to a kind of mordanting technique of half shading window decorations.
Background technology
Beautifully attract eyeball very much although modern textile product coating dyeing and finishing product color is out gorgeous, the cost that pay the gorgeous beautiful behind of this color is water pollution; Dyeing waste water is that processing cotton, fiber crops, chemical fibre and blending product thereof are the waste water that main printing and dyeing mill discharges; The textiles waste water of 70-80% left and right is from printing and dyeing.The dyeing waste water water yield is larger, 100～200 tons of 1 ton of textiles water consumptions of every dyeing and printing process, and wherein 80～90% become waste water.Textile printing and dyeing wastewater has the features such as the water yield is large, organic pollution content is high, alkalescence large, change of water quality is large, belong to one of unmanageable industrial wastewater, in waste water, contain dyestuff, slurry, auxiliary agent, finish, soda acid, fiber impurity, sand class material, inorganic salts etc.It is to reduce sewage to produce that printing and dyeing arrange industry a great problem.
CN102433645B (2013-6-19) discloses the production technology of flame-retarded sun-shading curtain cloth, but the waste water that this invention produces is more, and can only prepare full window shade cloth.
Summary of the invention
The object of this invention is to provide a kind of by printing and dyeing and coating mordanting technique that complete, that reduce half shading window decorations of sewage generation simultaneously.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A mordanting technique for half shading window decorations, it comprises the following steps successively:
(1) grey cloth preparation;
(2) water-based mordanting slurry modulation: prepare by weight environment-friendly type flexible glue 25-45 part, stiffening glue 13-18 part, water 35-47 part, high-efficient penetrant 1-5 part, defoamer 0.01-0.2 part, colouring stabilizer 0.2-1.5 part, ultra-violet absorber 0.5-1.5 part, dyestuff 8-10 part;
(3) mordanting and coating: described grey cloth is put into described water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4Mpa, speed 10-15m/min;
(4) smooth processing: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
(5) after, arrange: dry for the first time at 165-170 DEG C, dry for the second time at 170-175 DEG C, then lower the temperature with cold wind; Described with cold wind cooling specifically in order to 110-90 DEG C, 90-80 DEG C, 78-69 DEG C, 68-62 DEG C, 61-58 DEG C, 57-50 DEG C, 48-38 DEG C, 35-28 DEG C gradual cooling, temperature fall time is 20-27min; Finally cooling rolling again in room temperature again.
Mordanting of the present invention and coating paste adopt same water-based mordanting slurry, thereby make to print and dye mordanting and coating complete simultaneously, have reduced waste water generation; Water-based mordanting slurry safety and environmental protection simultaneously of the present invention, can realize environmental protection and produce; Hyperthermia drying can separate some nuisances, improves COLOR FASTNESS; Dry and can further improve COLOR FASTNESS step by step.Adopt gradual cold wind cooling to can further improve again coloring effect and COLOR FASTNESS.
The water-based mordanting slurry of making by special component and proportioning can be realized printing and dyeing and half shading coating simultaneously, and half shading coating is effective; Simultaneously by the grey cloth pin hole slurry after mordanting and coating through slurry adsorption plane panel assembly Adsorption, in improving the overall appearance and flatness of grey cloth, because baking and banking up with earth with cold wind of rear arrangement lowered the temperature and can be strengthened degree of staining twice, thereby finally obtain, COLOR FASTNESS is good, especially half window shade of half shading window decorations of half good shading effect again.
As preferably, described stiffening glue is one or more in the anionic emulsion that forms of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; Described high-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is compound agent, compound agent or 4-benzoyloxy-2, one or more in 2,6,6-tetramethyl piperidine appraised and decided of liquid barium cadmium zinc appraised and decided of liquid barium zinc compound stabilizer, liquid barium cadmium; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567.
As preferably, described grey cloth preparation comprises turns over cloth, and weft yarn is opened sanction, and margin to seam is singed and spend type hollow out institutional framework to prepare; Described weft yarn is opened and cut out is that fabric is cut apart with a knife or scissors by weft yarn; Described margin to seam is that margin to seam between board, between fabric is carried out to the parallel margin to seam of weft yarn.
As preferably, described dyestuff comprises REACTIVE DYES and reducing dye, described REACTIVE DYES is at least one in Levafix EA, Procion H-EXL, the Cibacron Light type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
As preferably, described environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70-95 part, phthalic anhydride 25-35 part, triethylene glycol 10-12 part, glutaric acid 15-18 part, butantriol 8-10 part, Zinc Oxide 5-7 part, magnesia 3-5 part, neoprene 15-25 part, softening oil 2-3 part, dimethyl carbonate 15-20 part, ethylbenzene 20-30 part, the fire-retardant dispersant 1-3 of phosphorus series non-halogen part;
The formula of the fire-retardant dispersant of described phosphorus series non-halogen is acrylic acid 25-30 part by weight, aluminium hydroxide 50-55 part, APP 45-55 part, titanium dioxide 28-44 part, polyurethane 6-12 part, water 50-60 part, dispersant 0.2-0.8 part, bleeding agent 0.15-0.35 part, rheology control agent 3-8 part.
Adopt glue of the present invention, have advantages of that tack is good, fastness is high; Not only good flame retardation effect of fire retardant of the present invention, and can with glue in all the other component Synergistics, increase the tack of glue.When the burning of the fire-retardant dispersant of phosphorus series non-halogen the amount of being fuming little, do not produce poisonous and corrosive gas, the feature of environmental protection is good.
More preferably, described dispersant is polycarboxylate sodium's water treatment dispersion, and described rheology control agent is silicon gel or polyacrylamide.
More preferably, the formula of the fire-retardant dispersant of described phosphorus series non-halogen is 28 parts, acrylic acid by weight, 52 parts, aluminium hydroxide, 50 parts of APP, 40 parts of titanium dioxide, 8 parts of polyurethane, 54 parts, water, 0.5 part of dispersant, 0.25 part of bleeding agent, 5 parts of rheology control agents.
As preferably, before mordanting and coating, also comprise grey cloth to move back to boil and float and mercerization finish, described move back to boil to float comprise moving back to boil with oxygen and float, employing is boiled and is floated combined production line, adopt after six lattice adverse current open washings, fabric is carried out to roll compacting to control moisture content as 45-55%, then directly pad liquid lime chloride and make the bleaching of fabric decatize; Speed of a motor vehicle when described oxygen floats is 58-65m/min, described oxygen bleaching method be fabric is placed in to oxygen bleaching liquor and in pressurized vessel, repeatedly pressurize, decompression operation, the bath raio of oxygen bleaching liquor is 3-5:1, the hydrogen peroxide of refining agent OPE, the 8-10g/L of the sodium metasilicate of the sodium carbonate that described oxygen bleaching liquor is 6-10g/L, the sodium hydrogen phosphate of 2-3g/L, 1-3g/L, the lauryl sodium sulfate of 4-6g/L, 2-5g/L and water composition; Described pressurization should make temperature in pressurized tank reach 95-105 DEG C, and described decompression is to discharge the pressure in this pressurized tank to atmosphere fast after pressurized, heated; Described mercerising is to adopt containing damp rate auto-controller to make fabric contain damp rate to be controlled at 25-35%, carries out half wet mercerising in the mercerising solution that comprises 265-300g/L concentration hydrogen sodium oxide molybdena, 5-8g/L alkylol sulfuric ester sodium salt.
Adopt the method to process the impurity on it to described grey cloth, can prevent polyster fibre and the impaired and powerful decline of spandex core-covered high temperature simultaneously; By traditional moving back, boil, bleaching process is reduced to a step and boils and float associating, reduces the damage to terylene and spandex, further reduced waste water generation; Adopt of the present invention boil to float can shorten the time, rapid pressure change boils and floats, and further improves the comfortable feel of grey cloth.
As preferably, lower the temperature specifically in order to 100 DEG C with cold wind, 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature are lowered the temperature, and temperature fall time is 20-27min; Finally it is gradual cooling in rolling at room temperature.
Detailed description of the invention
Embodiment mono-
Grey cloth preparation: comprise and turn over cloth, weft yarn is opened sanction, margin to seam, singes and spends the preparation of type hollow out institutional framework; Weft yarn is opened and cut out is that fabric is cut apart with a knife or scissors by weft yarn; Margin to seam is that margin to seam between board, between fabric is carried out to the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare by weight 25 parts of environment-friendly type flexible glues, 13 parts, stiffening glue, 35 parts, water, 1 part of high-efficient penetrant, 0.01 part of defoamer, 0.2 part of colouring stabilizer, 0.5 part of ultra-violet absorber, 8 parts of dyestuffs;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
70 parts of polyurethane, 25 parts of phthalic anhydrides, 10 parts of triethylene glycols, 15 parts of glutaric acids, 8 parts of butantriols, 5 parts of Zinc Oxides, 3 parts, magnesia, 15 parts of neoprenes, 2 parts of softening oils, 15 parts of dimethyl carbonates, 20 parts, ethylbenzene, 1 part of the fire-retardant dispersant of phosphorus series non-halogen;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 25 parts, acrylic acid by weight, 50 parts, aluminium hydroxide, 45 parts of APP, 28 parts of titanium dioxide, 6 parts of polyurethane, 50 parts, water, 0.2 part of polycarboxylate sodium's water treatment dispersion, 0.15 part of bleeding agent, 3 parts of silicon gels;
Stiffening glue is the anionic emulsion that polystyrene and acrylic ester copolymer form; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is compound agent or 4-benzoyloxy-2, one or more in 2,6,6-tetramethyl piperidine appraised and decided of liquid barium zinc compound stabilizer, liquid barium cadmium and liquid barium cadmium zinc; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567;
Dyestuff comprises REACTIVE DYES and reducing dye, REACTIVE DYES is at least one in Levafix EA, Procion H-EXL, the Cibacron Light type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, under air pressure 0.3-0.4Mpa, speed 10-15m/min, apply through pressure roller pressure rolling;
Smooth processing: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Rear arrangement: dry for the first time at 165-170 DEG C, dry for the second time at 170-175 DEG C, then lower the temperature with cold wind; Cold wind cooling specifically comprises with cold wind lowers the temperature specifically in order to 100 DEG C, and 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature cooling rates are 20-27min; Make it gradual cooling in rolling at room temperature.
Embodiment bis-
Grey cloth preparation: comprise and turn over cloth, weft yarn is opened sanction, margin to seam, singes and spends the preparation of type hollow out institutional framework; Weft yarn is opened and cut out is that fabric is cut apart with a knife or scissors by weft yarn; Margin to seam is that margin to seam between board, between fabric is carried out to the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare by weight 35 parts of environment-friendly type flexible glues, 15 parts, stiffening glue, 37 parts, water, 4 parts of high-efficient penetrants, 0.015 part of defoamer, 0.9 part of colouring stabilizer, 1.2 parts of ultra-violet absorbers, 9 parts of dyestuffs;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
85 parts of polyurethane, 30 parts of phthalic anhydrides, 11 parts of triethylene glycols, 16 parts of glutaric acids, 9 parts of butantriols, 6 parts of Zinc Oxides, 4 parts, magnesia, 18 parts of neoprenes, 2.5 parts of softening oils, 18 parts of dimethyl carbonates, 25 parts, ethylbenzene, 2 parts of the fire-retardant dispersants of phosphorus series non-halogen;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 30 parts, acrylic acid by weight, 55 parts, aluminium hydroxide, 55 parts of APP, 44 parts of titanium dioxide, 12 parts of polyurethane, 60 parts, water, 0.8 part of polycarboxylate sodium's water treatment dispersion, 0.35 part of bleeding agent, 5 parts of silicon gels;
Stiffening glue is one or more in the anionic emulsion that forms of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is liquid barium zinc compound stabilizer; Ultra-violet absorber is septichen phenyl ester;
Dyestuff comprises REACTIVE DYES and reducing dye, and REACTIVE DYES is the Levafix EA of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, under air pressure 0.3Mpa, speed 10m/min, apply through pressure roller pressure rolling;
Smooth processing: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Rear arrangement: dry for the first time at 165 DEG C, dry for the second time at 170 DEG C, then lower the temperature with cold wind; Described with cold wind cooling specifically in order to 110-90 DEG C, 90-80 DEG C, 78 DEG C, 68 DEG C, 61 DEG C, 57 DEG C, 48 DEG C, 35 DEG C gradual coolings, temperature fall time is 20min; Finally cooling rolling again in room temperature again.
Embodiment tri-
Grey cloth preparation: comprise and turn over cloth, weft yarn is opened sanction, margin to seam, singes and spends the preparation of type hollow out institutional framework; Weft yarn is opened and cut out is that fabric is cut apart with a knife or scissors by weft yarn; Margin to seam is that margin to seam between board, between fabric is carried out to the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare by weight 45 parts of environment-friendly type flexible glues, 18 parts, stiffening glue, 47 parts, water, 5 parts of high-efficient penetrants, 0.2 part of defoamer, 1.5 parts of colouring stabilizers, 1.5 parts of ultra-violet absorbers, 10 parts of dyestuffs;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
95 parts of polyurethane, 35 parts of phthalic anhydrides, 12 parts of triethylene glycols, 18 parts of glutaric acids, 10 parts of butantriols, 7 parts of Zinc Oxides, 5 parts, magnesia, 25 parts of neoprenes, 3 parts of softening oils, 20 parts of dimethyl carbonates, 30 parts, ethylbenzene, 3 parts of the fire-retardant dispersants of phosphorus series non-halogen;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 28 parts, acrylic acid by weight, 52 parts, aluminium hydroxide, 49 parts of APP; 39 parts of titanium dioxide, 11 parts of polyurethane, 58 parts, water; 0.6 part of polycarboxylate sodium's water treatment dispersion, bleeding agent 0.15-0.35 part, 8 parts of polyacrylamides;
Stiffening glue is the anionic emulsion that acrylic acid and acrylic ester copolymer form; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; To be that liquid barium cadmium zinc is compound appraise and decide agent to colouring stabilizer; Ultra-violet absorber is 2-(2-hydroxy-5-methyl base phenyl) BTA;
Dyestuff comprises REACTIVE DYES and reducing dye, and REACTIVE DYES is at least one in the Procion H-EXL type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, under air pressure 0.4Mpa, speed 15m/min, apply through pressure roller pressure rolling;
Smooth processing: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Rear arrangement: dry for the first time at 170 DEG C, dry for the second time at 175 DEG C, then lower the temperature with cold wind; Described with cold wind cooling specifically in order to 90 DEG C, 80 DEG C, 69 DEG C, 68-62 DEG C, 58 DEG C, 50 DEG C, 38 DEG C, 28 DEG C gradual coolings, temperature fall time is 27min; Finally cooling rolling again in room temperature again.
Embodiment tetra-
With embodiment mono-, different is before mordanting and coating, also to comprise grey cloth to move back to boil to float and mercerization finish, move back to boil to float and comprise moving back to boil with oxygen and float, employing is boiled and is floated combined production line, adopt after six lattice adverse current open washings, fabric is carried out to roll compacting to control moisture content as 48%, then directly pad liquid lime chloride and make the bleaching of fabric decatize; Speed of a motor vehicle when oxygen floats is 60m/min, oxygen bleaching method be fabric is placed in to oxygen bleaching liquor and in pressurized vessel, repeatedly pressurize, decompression operation, the bath raio of oxygen bleaching liquor is 4:1, the hydrogen peroxide of refining agent OPE, the 9g/L of the sodium metasilicate of the sodium carbonate that oxygen bleaching liquor is 8g/L, the sodium hydrogen phosphate of 2-3g/L, 2g/L, the lauryl sodium sulfate of 5g/L, 2-5g/L and water composition; Pressurization should make temperature in pressurized tank reach 100 DEG C, and decompression is to discharge the pressure in this pressurized tank to atmosphere fast after pressurized, heated; Mercerising is to adopt containing damp rate auto-controller to make fabric contain damp rate to be controlled at 28%, carries out half wet mercerising in the mercerising solution that comprises 290g/L concentration hydrogen sodium oxide molybdena, 7g/L alkylol sulfuric ester sodium salt.
Embodiment five
With embodiment bis-, different is before mordanting and coating, also to comprise grey cloth to move back to boil to float and mercerization finish, move back to boil to float and comprise moving back to boil with oxygen and float, employing is boiled and is floated combined production line, adopt after six lattice adverse current open washings, fabric is carried out to roll compacting to control moisture content as 45%, then directly pad liquid lime chloride and make the bleaching of fabric decatize; Speed of a motor vehicle when oxygen floats is 58m/min, oxygen bleaching method be fabric is placed in to oxygen bleaching liquor and in pressurized vessel, repeatedly pressurize, decompression operation, the bath raio of oxygen bleaching liquor is 3:1, the hydrogen peroxide of refining agent OPE, the 8g/L of the sodium metasilicate of the sodium carbonate that oxygen bleaching liquor is 6g/L, the sodium hydrogen phosphate of 2g/L, 1g/L, the lauryl sodium sulfate of 4g/L, 2g/L and water composition; Pressurization should make temperature in pressurized tank reach 95 DEG C, and decompression is to discharge the pressure in this pressurized tank to atmosphere fast after pressurized, heated; Mercerising is to adopt containing damp rate auto-controller to make fabric contain damp rate to be controlled at 25%, carries out half wet mercerising in the mercerising solution that comprises 265g/L concentration hydrogen sodium oxide molybdena, 5-8g/L alkylol sulfuric ester sodium salt.
Embodiment six
With embodiment tri-, different is before mordanting and coating, also to comprise grey cloth to move back to boil to float and mercerization finish, move back to boil to float and comprise moving back to boil with oxygen and float, employing is boiled and is floated combined production line, adopt after six lattice adverse current open washings, fabric is carried out to roll compacting to control moisture content as 55%, then directly pad liquid lime chloride and make the bleaching of fabric decatize; Speed of a motor vehicle when oxygen floats is 65m/min, oxygen bleaching method be fabric is placed in to oxygen bleaching liquor and in pressurized vessel, repeatedly pressurize, decompression operation, the bath raio of oxygen bleaching liquor is 5:1, the hydrogen peroxide of refining agent OPE, the 10g/L of the sodium metasilicate of the sodium carbonate that oxygen bleaching liquor is 10g/L, the sodium hydrogen phosphate of 3g/L, 3g/L, the lauryl sodium sulfate of 6g/L, 5g/L and water composition; Pressurization should make temperature in pressurized tank reach 105 DEG C, and decompression is to discharge the pressure in this pressurized tank to atmosphere fast after pressurized, heated; Mercerising is to adopt containing damp rate auto-controller to make fabric contain damp rate to be controlled at 35%, carries out half wet mercerising in the mercerising solution that comprises 300g/L concentration hydrogen sodium oxide molybdena, 5-8g/L alkylol sulfuric ester sodium salt.
Comparative example one
With embodiment mono-, different is wherein not contain stiffening glue.
Comparative example two
With embodiment mono-, different is mordanting and coating are specifically put into grey cloth water-based mordanting slurry and are padded, and under air pressure 0.2Mpa, speed 20m/min, apply through pressure roller pressure rolling.
Experiment showed, that not adopt half shading coating effect of the half shading window decorations that water-based mordanting slurry formula of the present invention and mordanting coating process obtain bad, and the sewage producing is relatively many.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art are reading after this description and can make to the present embodiment the amendment that there is no creative contribution as required, but as long as within the scope of claim of the present invention, are all subject to the protection of Patent Law.
Claims (9)
1. a mordanting technique for half shading window decorations, is characterized in that: comprise the following steps successively:
(1) grey cloth preparation;
(2) water-based mordanting slurry modulation: prepare by weight environment-friendly type flexible glue 25-45 part, stiffening glue 13-18 part, water 35-47 part, high-efficient penetrant 1-5 part, defoamer 0.01-0.2 part, colouring stabilizer 0.2-1.5 part, ultra-violet absorber 0.5-1.5 part, dyestuff 8-10 part;
(3) mordanting and coating: described grey cloth is put into described water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4Mpa, speed 10-15m/min;
(4) smooth processing: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
(5) after, arrange: dry for the first time at 165-170 DEG C, dry for the second time at 170-175 DEG C, then lower the temperature with cold wind; Described with cold wind cooling specifically in order to 110-90 DEG C, 90-80 DEG C, 78-69 DEG C, 68-62 DEG C, 61-58 DEG C, 57-50 DEG C, 48-38 DEG C, 35-28 DEG C gradual cooling, temperature fall time is 20-27min; Finally cooling rolling again in room temperature again.
2. the mordanting technique of a kind of half shading window decorations according to claim 1, is characterized in that: described stiffening glue is one or more in the anionic emulsion that forms of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; Described high-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is compound agent, compound agent or 4-benzoyloxy-2, one or more in 2,6,6-tetramethyl piperidine appraised and decided of liquid barium cadmium zinc appraised and decided of liquid barium zinc compound stabilizer, liquid barium cadmium; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567.
3. the mordanting technique of a kind of half shading window decorations according to claim 2, is characterized in that: described grey cloth preparation comprises turns over cloth, and weft yarn is opened sanction, and margin to seam is singed and spends the preparation of type hollow out institutional framework; Described weft yarn is opened and cut out is that fabric is cut apart with a knife or scissors by weft yarn; Described margin to seam is that margin to seam between board, between fabric is carried out to the parallel margin to seam of weft yarn.
4. the mordanting technique of a kind of half shading window decorations according to claim 3, it is characterized in that: described dyestuff comprises REACTIVE DYES and reducing dye, described REACTIVE DYES is at least one in Levafix EA, Procion H-EXL, the Cibacron Light type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
5. the mordanting technique of a kind of half shading window decorations according to claim 4, is characterized in that: described environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70-95 part, phthalic anhydride 25-35 part, triethylene glycol 10-12 part, glutaric acid 15-18 part, butantriol 8-10 part, Zinc Oxide 5-7 part, magnesia 3-5 part, neoprene 15-25 part, softening oil 2-3 part, dimethyl carbonate 15-20 part, ethylbenzene 20-30 part, the fire-retardant dispersant 1-3 of phosphorus series non-halogen part;
The formula of the fire-retardant dispersant of described phosphorus series non-halogen is acrylic acid 25-30 part by weight, aluminium hydroxide 50-55 part, APP 45-55 part, titanium dioxide 28-44 part, polyurethane 6-12 part, water 50-60 part, dispersant 0.2-0.8 part, bleeding agent 0.15-0.35 part, rheology control agent 3-8 part.
6. according to the mordanting technique of a kind of half shading window decorations described in claim 1-5 any one, it is characterized in that: before mordanting and coating, also comprise grey cloth to move back to boil and float and mercerization finish, described move back to boil to float comprise moving back to boil with oxygen and float, employing is boiled and is floated combined production line, adopt after six lattice adverse current open washings, fabric is carried out to roll compacting to control moisture content as 45-55%, then directly pad liquid lime chloride and make the bleaching of fabric decatize; Speed of a motor vehicle when described oxygen floats is 58-65m/min, described oxygen bleaching method be fabric is placed in to oxygen bleaching liquor and in pressurized vessel, repeatedly pressurize, decompression operation, the bath raio of oxygen bleaching liquor is 3-5:1, the hydrogen peroxide of refining agent OPE, the 8-10g/L of the sodium metasilicate of the sodium carbonate that described oxygen bleaching liquor is 6-10g/L, the sodium hydrogen phosphate of 2-3g/L, 1-3g/L, the lauryl sodium sulfate of 4-6g/L, 2-5g/L and water composition; Described pressurization should make temperature in pressurized tank reach 95-105 DEG C, and described decompression is to discharge the pressure in this pressurized tank to atmosphere fast after pressurized, heated; Described mercerising is to adopt containing damp rate auto-controller to make fabric contain damp rate to be controlled at 25-35%, carries out half wet mercerising in the mercerising solution that comprises 265-300g/L concentration hydrogen sodium oxide molybdena, 5-8g/L alkylol sulfuric ester sodium salt.
7. the mordanting technique of a kind of half shading window decorations according to claim 6, is characterized in that: lower the temperature specifically in order to 100 DEG C with cold wind, 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature are lowered the temperature, and temperature fall time is 20-27min; Finally it is gradual cooling in rolling at room temperature.
8. the mordanting technique of a kind of half shading window decorations according to claim 7, is characterized in that: described dispersant is polycarboxylate sodium's water treatment dispersion, and described rheology control agent is silicon gel or polyacrylamide.
9. the mordanting technique of a kind of half shading window decorations according to claim 8, it is characterized in that: the formula of the fire-retardant dispersant of described phosphorus series non-halogen is 28 parts, acrylic acid by weight, 52 parts, aluminium hydroxide, 50 parts of APP, 40 parts of titanium dioxide, 8 parts of polyurethane, 54 parts, water, 0.5 part of dispersant, 0.25 part of bleeding agent, 5 parts of rheology control agents.
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