CN104153197B - A kind of mordanting technique of half shading window decorations - Google Patents
A kind of mordanting technique of half shading window decorations Download PDFInfo
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- CN104153197B CN104153197B CN201410397415.7A CN201410397415A CN104153197B CN 104153197 B CN104153197 B CN 104153197B CN 201410397415 A CN201410397415 A CN 201410397415A CN 104153197 B CN104153197 B CN 104153197B
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- mordanting
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- window decorations
- grey cloth
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- 238000000034 method Methods 0.000 title claims abstract description 29
- 238000005034 decoration Methods 0.000 title claims abstract description 19
- 239000004744 fabric Substances 0.000 claims abstract description 67
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 45
- 238000000576 coating method Methods 0.000 claims abstract description 27
- 239000003292 glue Substances 0.000 claims abstract description 27
- 239000002002 slurry Substances 0.000 claims abstract description 27
- 239000011248 coating agent Substances 0.000 claims abstract description 26
- 239000000975 dye Substances 0.000 claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 21
- 239000003381 stabilizer Substances 0.000 claims abstract description 17
- 238000005096 rolling process Methods 0.000 claims abstract description 15
- 238000004040 coloring Methods 0.000 claims abstract description 12
- 239000013530 defoamer Substances 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 239000006097 ultraviolet radiation absorber Substances 0.000 claims abstract description 11
- 238000001179 sorption measurement Methods 0.000 claims abstract description 8
- 238000004061 bleaching Methods 0.000 claims description 31
- 239000007788 liquid Substances 0.000 claims description 31
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 30
- 229910052760 oxygen Inorganic materials 0.000 claims description 30
- 239000001301 oxygen Substances 0.000 claims description 30
- 239000003795 chemical substances by application Substances 0.000 claims description 24
- 239000002270 dispersing agent Substances 0.000 claims description 22
- -1 polysiloxane Polymers 0.000 claims description 22
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 16
- 239000003063 flame retardant Substances 0.000 claims description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 229910052736 halogen Inorganic materials 0.000 claims description 15
- 150000002367 halogens Chemical class 0.000 claims description 15
- 238000009992 mercerising Methods 0.000 claims description 15
- 150000003017 phosphorus Chemical class 0.000 claims description 15
- 239000004814 polyurethane Substances 0.000 claims description 14
- 229920002635 polyurethane Polymers 0.000 claims description 14
- 239000000985 reactive dye Substances 0.000 claims description 14
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 12
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 12
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 claims description 12
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 12
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 11
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- 230000006837 decompression Effects 0.000 claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 8
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 8
- 230000000740 bleeding effect Effects 0.000 claims description 8
- 239000004408 titanium dioxide Substances 0.000 claims description 8
- 238000000518 rheometry Methods 0.000 claims description 7
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 claims description 6
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 claims description 6
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 claims description 6
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 claims description 6
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims description 6
- 239000000395 magnesium oxide Substances 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000011787 zinc oxide Substances 0.000 claims description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 5
- 240000007817 Olea europaea Species 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 5
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 5
- GKVKQZRNDGUFSY-NSGFTINJSA-L [Na+].C(C)(CCCCCC)/C(=C(/C(=O)[O-])\C(C)CCCCCC)/C(=O)[O-].[Na+] Chemical group [Na+].C(C)(CCCCCC)/C(=C(/C(=O)[O-])\C(C)CCCCCC)/C(=O)[O-].[Na+] GKVKQZRNDGUFSY-NSGFTINJSA-L 0.000 claims description 5
- 230000002411 adverse Effects 0.000 claims description 5
- 125000000129 anionic group Chemical group 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 5
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 5
- 229910000397 disodium phosphate Inorganic materials 0.000 claims description 5
- 235000019800 disodium phosphate Nutrition 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 5
- 239000004571 lime Substances 0.000 claims description 5
- 238000005517 mercerization Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 229920005646 polycarboxylate Polymers 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000007670 refining Methods 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 5
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 239000004793 Polystyrene Substances 0.000 claims description 4
- SHLNMHIRQGRGOL-UHFFFAOYSA-N barium zinc Chemical compound [Zn].[Ba] SHLNMHIRQGRGOL-UHFFFAOYSA-N 0.000 claims description 4
- 235000019628 coolness Nutrition 0.000 claims description 4
- 239000000017 hydrogel Substances 0.000 claims description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 4
- 229920002223 polystyrene Polymers 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 3
- MGFRKBRDZIMZGO-UHFFFAOYSA-N barium cadmium Chemical compound [Cd].[Ba] MGFRKBRDZIMZGO-UHFFFAOYSA-N 0.000 claims description 3
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims description 3
- 229920002401 polyacrylamide Polymers 0.000 claims description 3
- 229940065285 cadmium compound Drugs 0.000 claims description 2
- YAXWOADCWUUUNX-UHFFFAOYSA-N 1,2,2,3-tetramethylpiperidine Chemical compound CC1CCCN(C)C1(C)C YAXWOADCWUUUNX-UHFFFAOYSA-N 0.000 claims 1
- RKMGAJGJIURJSJ-UHFFFAOYSA-N 2,2,6,6-Tetramethylpiperidine Substances CC1(C)CCCC(C)(C)N1 RKMGAJGJIURJSJ-UHFFFAOYSA-N 0.000 claims 1
- CEKJAYFBQARQNG-UHFFFAOYSA-N cadmium zinc Chemical compound [Zn].[Cd] CEKJAYFBQARQNG-UHFFFAOYSA-N 0.000 claims 1
- 230000007613 environmental effect Effects 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000004043 dyeing Methods 0.000 description 11
- 239000002351 wastewater Substances 0.000 description 10
- 238000007639 printing Methods 0.000 description 8
- 230000000694 effects Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 239000004753 textile Substances 0.000 description 4
- SLETZFVTVXVPLS-UHFFFAOYSA-N [Zn].[Cd].[Ba] Chemical compound [Zn].[Cd].[Ba] SLETZFVTVXVPLS-UHFFFAOYSA-N 0.000 description 3
- 239000010865 sewage Substances 0.000 description 3
- 230000007306 turnover Effects 0.000 description 3
- YEYCMBWKTZNPDH-UHFFFAOYSA-N (2,2,6,6-tetramethylpiperidin-4-yl) benzoate Chemical compound C1C(C)(C)NC(C)(C)CC1OC(=O)C1=CC=CC=C1 YEYCMBWKTZNPDH-UHFFFAOYSA-N 0.000 description 2
- 229920002334 Spandex Polymers 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000004759 spandex Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 206010020843 Hyperthermia Diseases 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 210000005252 bulbus oculi Anatomy 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- 230000036031 hyperthermia Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Landscapes
- Coloring (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to the preparation technology of window decorations, particularly relate to a kind of mordanting technique of half shading window decorations.It comprises successively: prepared by grey cloth; Water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 25-45 part, stiffening glue 13-18 part, water 35-47 part, high-efficient penetrant 1-5 part, defoamer 0.01-0.2 part, colouring stabilizer 0.2-1.5 part, ultra-violet absorber 0.5-1.5 part, dyestuff 8-10 part by weight; Mordanting and coating: described grey cloth is put into described water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4Mpa, speed 10-15m/min; Smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating; Final finishing: 165-170 DEG C of first time oven dry, dry 170-175 DEG C of second time, then lower the temperature with cold wind; With cold wind cooling specifically in order to 110-90 DEG C, 90-80 DEG C, 78-69 DEG C, 68-62 DEG C, 61-58 DEG C, 57-50 DEG C, 48-38 DEG C, 35-28 DEG C gradual cooling, temperature fall time is 20-27min; Rolling is again cooled in last room temperature again.Water-based mordanting slurry safety and environmental protection of the present invention, can realize environmental protection and produce.
Description
Technical field
The present invention relates to the preparation technology of window decorations, particularly relate to a kind of mordanting technique of half shading window decorations.
Background technology
Beautifully to attract eyeball very much although modern textiles coating dyeing and finishing product color is out gorgeous, the cost that the gorgeous beautiful behind of this color is paid is water pollution; Dyeing waste water is processing cotton, fiber crops, chemical fibre and blending product thereof is the waste water that main printing and dyeing mill discharges; The textiles waste water of about 70-80% is from printing and dyeing.The dyeing waste water water yield is comparatively large, and every dyeing and printing process 1 ton of textiles water consumption 100 ~ 200 tons, wherein 80 ~ 90% become waste water.Textile printing and dyeing wastewater has the features such as the water yield is large, organic pollution content is high, alkalescence is large, change of water quality is large, belong to one of unmanageable industrial wastewater, containing dyestuff, slurry, auxiliary agent, finish, soda acid, fiber impurity, sand class material, inorganic salts etc. in waste water.It is reduce sewage to produce that printing and dyeing arrange industry a great problem.
CN102433645B (2013-6-19) discloses the production technology of flame-retarded sun-shading curtain cloth, but the waste water that this invention produces is more, and can only prepare full window shade cloth.
Summary of the invention
The object of this invention is to provide a kind of mordanting technique that printing and dyeing and coating are simultaneously completed, that reduce the half shading window decorations that sewage produces.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A mordanting technique for half shading window decorations, it comprises the following steps successively:
(1) grey cloth preparation;
(2) water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 25-45 part, stiffening glue 13-18 part, water 35-47 part, high-efficient penetrant 1-5 part, defoamer 0.01-0.2 part, colouring stabilizer 0.2-1.5 part, ultra-violet absorber 0.5-1.5 part, dyestuff 8-10 part by weight;
(3) mordanting and coating: described grey cloth is put into described water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4Mpa, speed 10-15m/min;
(4) smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
(5) Final finishing: 165-170 DEG C of first time oven dry, dry 170-175 DEG C of second time, then lower the temperature with cold wind; The cooling of described cold wind specifically in order to 110-90 DEG C, 90-80 DEG C, 78-69 DEG C, 68-62 DEG C, 61-58 DEG C, 57-50 DEG C, 48-38 DEG C, 35-28 DEG C gradual cooling, temperature fall time is 20-27min; Rolling is again cooled in last room temperature again.
Mordanting of the present invention and coating paste adopt same water-based mordanting slurry, thus printing and dyeing mordanting and coating are completed simultaneously, decrease waste water and produce; Water-based mordanting slurry safety and environmental protection of the present invention, can realize environmental protection and produce simultaneously; Some nuisances can be separated by hyperthermia drying, improve COLOR FASTNESS; Dry step by step and can improve COLOR FASTNESS further.Adopt gradual cold wind to lower the temperature and can further improve again coloring effect and COLOR FASTNESS.
The water-based mordanting slurry made by special component and proportioning can realize printing and dyeing and half shading coating simultaneously, and half shading coating is effective; Simultaneously by the grey cloth pin hole slurry after mordanting and coating through slurry adsorption plane panel assembly Adsorption, while the overall appearance improving grey cloth and flatness, again because baking and banking up with earth of Final finishing can strengthen degree of staining twice with cold wind cooling, thus final acquisition COLOR FASTNESS is good, half shading window decorations especially half window shade of half good shading effect.
As preferably, described stiffening glue is one or more in the anionic emulsion of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; Described high-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is liquid barium zinc compound stabilizer, liquid barium cadmium compound appraises and decides agent, liquid barium cadmium zinc compound appraises and decides agent or one or more in 4-benzoyloxy-2,2,6,6-tetramethyl piperidine; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567.
As preferably, described grey cloth preparation comprises turns over cloth, and sanction opened by weft yarn, margin to seam, singes and the preparation of flower pattern hollow out institutional framework; Sanction opened by described weft yarn is cut apart with a knife or scissors by weft yarn by fabric; Described margin to seam is that margin to seam between board, between fabric is carried out the parallel margin to seam of weft yarn.
As preferably, described dyestuff comprises REACTIVE DYES and reducing dye, described REACTIVE DYES is at least one in LevafixEA, ProcionH-EXL, CibacronLight type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
As preferably, described environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70-95 part, phthalic anhydride 25-35 part, triethylene glycol 10-12 part, glutaric acid 15-18 part, butantriol 8-10 part, Zinc Oxide 5-7 part, magnesia 3-5 part, neoprene 15-25 part, softening oil 2-3 part, dimethyl carbonate 15-20 part, ethylbenzene 20-30 part, phosphorus series non-halogen fire-retardant dispersant 1-3 part;
The formula of the fire-retardant dispersant of described phosphorus series non-halogen is acrylic acid 25-30 part, aluminium hydroxide 50-55 part, APP 45-55 part, titanium dioxide 28-44 part, polyurethane 6-12 part, water 50-60 part, dispersant 0.2-0.8 part, bleeding agent 0.15-0.35 part, rheology control agent 3-8 part.
Adopt glue of the present invention, there is the advantage that tack is good, fastness is high; Fire retardant of the present invention not only good flame retardation effect, and with all the other the component Synergistics in glue, the tack of glue can be increased.Phosphorus series non-halogen fire-retardant dispersant burning time the amount of being fuming little, do not produce poisonous and corrosive gas, the feature of environmental protection is good.
More preferably, described dispersant is polycarboxylate sodium's water treatment dispersion, and described rheology control agent is Silica hydrogel or polyacrylamide.
More preferably, the formula of the fire-retardant dispersant of described phosphorus series non-halogen is 28 parts, acrylic acid, 52 parts, aluminium hydroxide, APP 50 parts, titanium dioxide 40 parts, polyurethane 8 parts, 54 parts, water, dispersant 0.5 part, bleeding agent 0.25 part, rheology control agent 5 parts.
As preferably, also comprise before mordanting and coating to grey cloth move back boil drift and mercerization finish, described moving back is boiled drift and is comprised moving back and boil and oxygen bleaching, drift combined production line is boiled in employing, after adopting six lattice adverse current open washings, roll compacting is carried out to control moisture content for 45-55% to fabric, then directly pads liquid lime chloride and fabric decatize is bleached; Speed of a motor vehicle during described oxygen bleaching is 58-65m/min, described oxygen bleaching method be fabric is placed in oxygen bleaching liquid and repeatedly pressurize in pressurized vessel, decompression operation, the bath raio of oxygen bleaching liquid is 3-5:1, and described oxygen bleaching liquid is the sodium carbonate of 6-10g/L, the sodium hydrogen phosphate of 2-3g/L, the sodium metasilicate of 1-3g/L, the lauryl sodium sulfate of 4-6g/L, the hydrogen peroxide of refining agent OPE, 8-10g/L of 2-5g/L and water composition; Described pressurization should make temperature in pressurized tank reach 95-105 DEG C, and described decompression is the pressure discharged to air fast after pressurized, heated in this pressurized tank; Described mercerising adopts to make fabric contain damp rate to control at 25-35% containing damp rate auto-controller, carries out half wet mercerising in the mercerising solution comprising 265-300g/L sodium hydroxide, 5-8g/L alkylol sulfuric ester sodium salt.
Employing the method can process the impurity on it to described grey cloth, can prevent polyster fibre and the impaired and powerful decline of spandex core-covered high temperature simultaneously; By traditional moving back, boil, bleaching process is reduced to a step and boils drift associating, reduces the damage to terylene and spandex, further reduces waste water and produce; Adopt and of the present inventionly boil drift and can shorten the time, rapid pressure change boils drift, improves the comfortable feel of grey cloth further.
As preferably, with cold wind cooling specifically in order to 100 DEG C, 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature coolings, temperature fall time is 20-27min; Last its at room temperature gradual cooling in rolling.
Detailed description of the invention
Embodiment one
Prepared by grey cloth: comprise and turn over cloth, sanction opened by weft yarn, margin to seam, singes and the preparation of flower pattern hollow out institutional framework; Sanction opened by weft yarn is cut apart with a knife or scissors by weft yarn by fabric; Margin to seam is that margin to seam between board, between fabric is carried out the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 25 parts, stiffening 13 parts, glue, 35 parts, water, high-efficient penetrant 1 part, defoamer 0.01 part, colouring stabilizer 0.2 part, ultra-violet absorber 0.5 part, dyestuff 8 parts by weight;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70 parts, phthalic anhydride 25 parts, triethylene glycol 10 parts, glutaric acid 15 parts, butantriol 8 parts, Zinc Oxide 5 parts, 3 parts, magnesia, neoprene 15 parts, softening oil 2 parts, dimethyl carbonate 15 parts, 20 parts, ethylbenzene, the fire-retardant dispersant of phosphorus series non-halogen 1 part;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 25 parts, acrylic acid, 50 parts, aluminium hydroxide, APP 45 parts, titanium dioxide 28 parts, polyurethane 6 parts, 50 parts, water, polycarboxylate sodium's water treatment dispersion 0.2 part, bleeding agent 0.15 part, Silica hydrogel 3 parts;
Stiffening glue is the anionic emulsion of polystyrene and acrylic ester copolymer; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is liquid barium zinc compound stabilizer, liquid barium cadmium and liquid barium cadmium zinc compound are appraised and decided in agent or 4-benzoyloxy-2,2,6,6-tetramethyl piperidine one or more; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567;
Dyestuff comprises REACTIVE DYES and reducing dye, REACTIVE DYES is at least one in LevafixEA, ProcionH-EXL, CibacronLight type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4Mpa, speed 10-15m/min;
Smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Final finishing: 165-170 DEG C of first time oven dry, dry 170-175 DEG C of second time, then lower the temperature with cold wind; Cold wind cooling specifically comprises with cold wind cooling specifically in order to 100 DEG C, and 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature cooling rates are 20-27min; Make its at room temperature gradual cooling in rolling.
Embodiment two
Prepared by grey cloth: comprise and turn over cloth, sanction opened by weft yarn, margin to seam, singes and the preparation of flower pattern hollow out institutional framework; Sanction opened by weft yarn is cut apart with a knife or scissors by weft yarn by fabric; Margin to seam is that margin to seam between board, between fabric is carried out the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 35 parts, stiffening 15 parts, glue, 37 parts, water, high-efficient penetrant 4 parts, defoamer 0.015 part, colouring stabilizer 0.9 part, ultra-violet absorber 1.2 parts, dyestuff 9 parts by weight;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 85 parts, phthalic anhydride 30 parts, triethylene glycol 11 parts, glutaric acid 16 parts, butantriol 9 parts, Zinc Oxide 6 parts, 4 parts, magnesia, neoprene 18 parts, softening oil 2.5 parts, dimethyl carbonate 18 parts, 25 parts, ethylbenzene, the fire-retardant dispersant of phosphorus series non-halogen 2 parts;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 30 parts, acrylic acid, 55 parts, aluminium hydroxide, APP 55 parts, titanium dioxide 44 parts, polyurethane 12 parts, 60 parts, water, polycarboxylate sodium's water treatment dispersion 0.8 part, bleeding agent 0.35 part, Silica hydrogel 5 parts;
Stiffening glue is one or more in the anionic emulsion of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is liquid barium zinc compound stabilizer; Ultra-violet absorber is septichen phenyl ester;
Dyestuff comprises REACTIVE DYES and reducing dye, and REACTIVE DYES is the LevafixEA of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3Mpa, speed 10m/min;
Smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Final finishing: 165 DEG C of first time oven dry, dry 170 DEG C of second time, then lower the temperature with cold wind; The cooling of described cold wind specifically in order to 110-90 DEG C, 90-80 DEG C, 78 DEG C, 68 DEG C, 61 DEG C, 57 DEG C, 48 DEG C, 35 DEG C gradual coolings, temperature fall time is 20min; Rolling is again cooled in last room temperature again.
Embodiment three
Prepared by grey cloth: comprise and turn over cloth, sanction opened by weft yarn, margin to seam, singes and the preparation of flower pattern hollow out institutional framework; Sanction opened by weft yarn is cut apart with a knife or scissors by weft yarn by fabric; Margin to seam is that margin to seam between board, between fabric is carried out the parallel margin to seam of weft yarn;
Water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 45 parts, stiffening 18 parts, glue, 47 parts, water, high-efficient penetrant 5 parts, defoamer 0.2 part, colouring stabilizer 1.5 parts, ultra-violet absorber 1.5 parts, dyestuff 10 parts by weight;
Wherein, environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 95 parts, phthalic anhydride 35 parts, triethylene glycol 12 parts, glutaric acid 18 parts, butantriol 10 parts, Zinc Oxide 7 parts, 5 parts, magnesia, neoprene 25 parts, softening oil 3 parts, dimethyl carbonate 20 parts, 30 parts, ethylbenzene, the fire-retardant dispersant of phosphorus series non-halogen 3 parts;
The formula of the fire-retardant dispersant of phosphorus series non-halogen is 28 parts, acrylic acid, 52 parts, aluminium hydroxide, APP 49 parts; titanium dioxide 39 parts, polyurethane 11 parts, 58 parts, water; polycarboxylate sodium's water treatment dispersion 0.6 part, bleeding agent 0.15-0.35 part, polyacrylamide 8 parts;
Stiffening glue is the anionic emulsion of acrylic acid and acrylic ester copolymer; High-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is that liquid barium cadmium zinc compound appraises and decides agent; Ultra-violet absorber is 2-(2-hydroxy-5-methyl base phenyl) BTA;
Dyestuff comprises REACTIVE DYES and reducing dye, and REACTIVE DYES is at least one in the ProcionH-EXL type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
Mordanting and coating: grey cloth is put into water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.4Mpa, speed 15m/min;
Smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
Final finishing: 170 DEG C of first time oven dry, dry 175 DEG C of second time, then lower the temperature with cold wind; The cooling of described cold wind specifically in order to 90 DEG C, 80 DEG C, 69 DEG C, 68-62 DEG C, 58 DEG C, 50 DEG C, 38 DEG C, 28 DEG C gradual coolings, temperature fall time is 27min; Rolling is again cooled in last room temperature again.
Embodiment four
With embodiment one, unlike also comprise before mordanting and coating to grey cloth move back boil drift and mercerization finish, move back and boil drift and comprise moving back and boil and oxygen bleaching, drift combined production line is boiled in employing, after adopting six lattice adverse current open washings, roll compacting is carried out to control moisture content for 48% to fabric, then directly pads liquid lime chloride and fabric decatize is bleached; Speed of a motor vehicle during oxygen bleaching is 60m/min, oxygen bleaching method be fabric is placed in oxygen bleaching liquid and repeatedly pressurize in pressurized vessel, decompression operation, the bath raio of oxygen bleaching liquid is 4:1, and oxygen bleaching liquid is the sodium carbonate of 8g/L, the sodium hydrogen phosphate of 2-3g/L, the sodium metasilicate of 2g/L, the lauryl sodium sulfate of 5g/L, the hydrogen peroxide of refining agent OPE, 9g/L of 2-5g/L and water composition; Pressurization should make temperature in pressurized tank reach 100 DEG C, and decompression is the pressure discharged to air fast after pressurized, heated in this pressurized tank; Mercerising adopts to make fabric contain damp rate to control 28% containing damp rate auto-controller, carries out half wet mercerising in the mercerising solution comprising 290g/L sodium hydroxide, 7g/L alkylol sulfuric ester sodium salt.
Embodiment five
With embodiment two, unlike also comprise before mordanting and coating to grey cloth move back boil drift and mercerization finish, move back and boil drift and comprise moving back and boil and oxygen bleaching, drift combined production line is boiled in employing, after adopting six lattice adverse current open washings, roll compacting is carried out to control moisture content for 45% to fabric, then directly pads liquid lime chloride and fabric decatize is bleached; Speed of a motor vehicle during oxygen bleaching is 58m/min, oxygen bleaching method be fabric is placed in oxygen bleaching liquid and repeatedly pressurize in pressurized vessel, decompression operation, the bath raio of oxygen bleaching liquid is 3:1, and oxygen bleaching liquid is the sodium carbonate of 6g/L, the sodium hydrogen phosphate of 2g/L, the sodium metasilicate of 1g/L, the lauryl sodium sulfate of 4g/L, the hydrogen peroxide of refining agent OPE, 8g/L of 2g/L and water composition; Pressurization should make temperature in pressurized tank reach 95 DEG C, and decompression is the pressure discharged to air fast after pressurized, heated in this pressurized tank; Mercerising adopts to make fabric contain damp rate to control 25% containing damp rate auto-controller, carries out half wet mercerising in the mercerising solution comprising 265g/L sodium hydroxide, 5-8g/L alkylol sulfuric ester sodium salt.
Embodiment six
With embodiment three, unlike also comprise before mordanting and coating to grey cloth move back boil drift and mercerization finish, move back and boil drift and comprise moving back and boil and oxygen bleaching, drift combined production line is boiled in employing, after adopting six lattice adverse current open washings, roll compacting is carried out to control moisture content for 55% to fabric, then directly pads liquid lime chloride and fabric decatize is bleached; Speed of a motor vehicle during oxygen bleaching is 65m/min, oxygen bleaching method be fabric is placed in oxygen bleaching liquid and repeatedly pressurize in pressurized vessel, decompression operation, the bath raio of oxygen bleaching liquid is 5:1, and oxygen bleaching liquid is the sodium carbonate of 10g/L, the sodium hydrogen phosphate of 3g/L, the sodium metasilicate of 3g/L, the lauryl sodium sulfate of 6g/L, the hydrogen peroxide of refining agent OPE, 10g/L of 5g/L and water composition; Pressurization should make temperature in pressurized tank reach 105 DEG C, and decompression is the pressure discharged to air fast after pressurized, heated in this pressurized tank; Mercerising adopts to make fabric contain damp rate to control 35% containing damp rate auto-controller, carries out half wet mercerising in the mercerising solution comprising 300g/L sodium hydroxide, 5-8g/L alkylol sulfuric ester sodium salt.
Comparative example one
With embodiment one, unlike wherein not containing stiffening glue.
Comparative example two
With embodiment one, specifically grey cloth is put into water-based mordanting slurry unlike mordanting and coating and pad, apply through pressure roller pressure rolling under air pressure 0.2Mpa, speed 20m/min.
Experiment proves, half shading coating effect of the half shading window decorations not adopting water-based mordanting slurry formula of the present invention and mordanting coating process to obtain is bad, and the sewage produced is relatively many.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the amendment not having creative contribution as required after reading this description, as long as but be all subject to the protection of Patent Law in right of the present invention.
Claims (9)
1. a mordanting technique for half shading window decorations, is characterized in that: comprise the following steps successively:
(1) grey cloth preparation;
(2) water-based mordanting slurry modulation: prepare environment-friendly type flexible glue 25-45 part, stiffening glue 13-18 part, water 35-47 part, high-efficient penetrant 1-5 part, defoamer 0.01-0.2 part, colouring stabilizer 0.2-1.5 part, ultra-violet absorber 0.5-1.5 part, dyestuff 8-10 part by weight;
Described environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70-95 part, phthalic anhydride 25-35 part, triethylene glycol 10-12 part, glutaric acid 15-18 part, butantriol 8-10 part, Zinc Oxide 5-7 part, magnesia 3-5 part, neoprene 15-25 part, softening oil 2-3 part, dimethyl carbonate 15-20 part, ethylbenzene 20-30 part, phosphorus series non-halogen fire-retardant dispersant 1-3 part;
The formula of the fire-retardant dispersant of described phosphorus series non-halogen is acrylic acid 25-30 part, aluminium hydroxide 50-55 part, APP 45-55 part, titanium dioxide 28-44 part, polyurethane 6-12 part, water 50-60 part, dispersant 0.2-0.8 part, bleeding agent 0.15-0.35 part, rheology control agent 3-8 part;
(3) mordanting and coating: described grey cloth is put into described water-based mordanting slurry and pad, apply through pressure roller pressure rolling under air pressure 0.3-0.4MPa, speed 10-15m/min;
(4) smooth process: by the grey cloth pin hole slurry Adsorption after mordanting and coating;
(5) Final finishing: 165-170 DEG C of first time oven dry, dry 170-175 DEG C of second time, then lower the temperature with cold wind; The cooling of described cold wind specifically in order to 110-90 DEG C, 90-80 DEG C, 78-69 DEG C, 68-62 DEG C, 61-58 DEG C, 57-50 DEG C, 48-38 DEG C, 35-28 DEG C gradual cooling, temperature fall time is 20-27min; Rolling is again cooled in last room temperature again.
2. the mordanting technique of a kind of half shading window decorations according to claim 1, is characterized in that: described stiffening glue is one or more in the anionic emulsion of polystyrene, acrylic acid or vinyl acetate and acrylic ester copolymer; Described high-efficient penetrant is disecoctylmaleate sodium sulfonate; Defoamer is polysiloxane defoamers; Colouring stabilizer is one or more in tetramethyl piperidine of liquid barium zinc compound stabilizer, liquid barium cadmium compound stabilizer, liquid barum cadmium zinc compound stabilizer or 4-benzoyloxy-2,2,6,6-; Ultra-violet absorber is septichen phenyl ester, 2-(2-hydroxy-5-methyl base phenyl) one or more in BTA or ESCALOL 567.
3. the mordanting technique of a kind of half shading window decorations according to claim 2, is characterized in that: described grey cloth preparation comprises turns over cloth, and sanction opened by weft yarn, margin to seam, singes and the preparation of flower pattern hollow out institutional framework; Sanction opened by described weft yarn is cut apart with a knife or scissors by weft yarn by fabric; Described margin to seam is that margin to seam between board, between fabric is carried out the parallel margin to seam of weft yarn.
4. the mordanting technique of a kind of half shading window decorations according to claim 3, it is characterized in that: described dyestuff comprises REACTIVE DYES and reducing dye, described REACTIVE DYES is at least one in LevafixEA, ProcionH-EXL, CibacronLight type REACTIVE DYES of De Sida company, and reducing dye is at least one in olive T, blue ARN, red R, black ES-SE, blue RSN, blue CLF, purple 2R.
5. the mordanting technique of a kind of half shading window decorations according to claim 4, is characterized in that: described environment-friendly type flexible glue is made up of the raw material of following parts by weight:
Polyurethane 70-95 part, phthalic anhydride 25-35 part, triethylene glycol 10-12 part, glutaric acid 15-18 part, butantriol 8-10 part, Zinc Oxide 5-7 part, magnesia 3-5 part, neoprene 15-25 part, softening oil 2-3 part, dimethyl carbonate 15-20 part, ethylbenzene 20-30 part, phosphorus series non-halogen fire-retardant dispersant 1-3 part;
The formula of the fire-retardant dispersant of described phosphorus series non-halogen is acrylic acid 25-30 part, aluminium hydroxide 50-55 part, APP 45-55 part, titanium dioxide 28-44 part, polyurethane 6-12 part, water 50-60 part, dispersant 0.2-0.8 part, bleeding agent 0.15-0.35 part, rheology control agent 3-8 part.
6. the mordanting technique of a kind of half shading window decorations according to any one of claim 1-5, it is characterized in that: also comprise before mordanting and coating to grey cloth move back boil drift and mercerization finish, described moving back is boiled drift and is comprised moving back and boil and oxygen bleaching, drift combined production line is boiled in employing, after adopting six lattice adverse current open washings, roll compacting is carried out to control moisture content for 45-55% to fabric, then directly pads liquid lime chloride and fabric decatize is bleached; Speed of a motor vehicle during described oxygen bleaching is 58-65m/min, described oxygen bleaching method be fabric is placed in oxygen bleaching liquid and repeatedly pressurize in pressurized vessel, decompression operation, the bath raio of oxygen bleaching liquid is 3-5:1, and described oxygen bleaching liquid is the sodium carbonate of 6-10g/L, the sodium hydrogen phosphate of 2-3g/L, the sodium metasilicate of 1-3g/L, the lauryl sodium sulfate of 4-6g/L, the hydrogen peroxide of refining agent OPE, 8-10g/L of 2-5g/L and water composition; Described pressurization should make temperature in pressurized tank reach 95-105 DEG C, and described decompression is the pressure discharged to air fast after pressurized, heated in this pressurized tank; Described mercerising adopts to make fabric contain damp rate to control at 25-35% containing damp rate auto-controller, carries out half wet mercerising in the mercerising solution comprising 265-300g/L sodium hydroxide, 5-8g/L alkylol sulfuric ester sodium salt.
7. the mordanting technique of a kind of half shading window decorations according to claim 6, is characterized in that: with cold wind cooling specifically in order to 100 DEG C, 85 DEG C, 70 DEG C, 65 DEG C, 60 DEG C, 55 DEG C, 40 DEG C, 30 DEG C of gradual box temperature coolings, and temperature fall time is 20-27min; Last its at room temperature gradual cooling in rolling.
8. the mordanting technique of a kind of half shading window decorations according to claim 7, is characterized in that: described dispersant is polycarboxylate sodium's water treatment dispersion, and described rheology control agent is Silica hydrogel or polyacrylamide.
9. the mordanting technique of a kind of half shading window decorations according to claim 8, it is characterized in that: the formula of the fire-retardant dispersant of described phosphorus series non-halogen is 28 parts, acrylic acid, 52 parts, aluminium hydroxide, APP 50 parts, titanium dioxide 40 parts, polyurethane 8 parts, 54 parts, water, dispersant 0.5 part, bleeding agent 0.25 part, rheology control agent 5 parts.
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