CN104313900A - Dyeing technology of bright blue-containing reactive dye - Google Patents
Dyeing technology of bright blue-containing reactive dye Download PDFInfo
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- CN104313900A CN104313900A CN201410495702.1A CN201410495702A CN104313900A CN 104313900 A CN104313900 A CN 104313900A CN 201410495702 A CN201410495702 A CN 201410495702A CN 104313900 A CN104313900 A CN 104313900A
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Abstract
The invention discloses a dyeing technology of bright blue-containing reactive dye. The technology includes the following steps: 1, scouring and bleaching: sequentially adding 1g/L of a stabilizer, 3.5g/L of soda ash, 0.35g/L of a non-foam detergent agent, 2.0g/L of a wrinkle resistant agent CD and 6g/L of hydrogen peroxide at 40DEG C, and heating to 90DEG C, wherein the time is 60min, and a bath ratio is 1:10; and 2, dyeing: dyeing by using 3g/L of active bright blue B-BGFN, 1.43g/L of active bright yellow B-4GLN, 0.95g/L of active golden yellow B-4RNF, 80g/L of sodium sulfate, 25g/L of soda ash, 2g/L of a leveling agent RG-133 and 1g/L of a dispersant EXL-106, wherein a bath ratio is 1:10. The dyeing technology has the advantages of simplicity, practicality, difficult fading, improvement of the dyeing defect problem of grey cloth, and obvious fastness improvement.
Description
Technical field
The invention particularly relates to a kind of dyeing containing emerald green blue REACTIVE DYES.
Background technology
Dyeing is a very ancient technique.From unearthed relics, China and India, Egyptian as far back as prehistoric just know to dye with some natural dye.After the bright synthetic dyestuffs of amber golden hair in 1856, the dyeing theory of people to dyestuff is studied successively, but much more fruitful basic research is after the World War I, and cuprammonium rayon, viscose acetal fibre and acetate fibre come out.After World War II, various synthetic fiber just constantly occur.
Although all the time performing containing in emerald green blue REACTIVE DYES during deep colour dyeing technique during technological operation, as used chelated dispersants, salt adding, add alkali repeatedly substep, the methods such as heating rate is extremely slow are very careful, and the probability of look flower is still very high.Time dye after for this reason will stripping, still faces this problem after backwater and fastness is bad.Think that mainly the molecular weight of emerald green blue dyestuff causes very greatly colouring fast by analysis, but fastness is poor, wash water is unclean.Hold concurrently in above shortcoming, by first adding dyestuff in actual production, then gradation adds saltcake, adds alkali and extends the method Optimization Technology of process time.Facts have proved, not only look flower problem has clear improvement, and fastness is improved.
Summary of the invention
For the problems referred to above, the invention provides a kind of dyeing containing emerald green blue REACTIVE DYES, dyeing simply, not fugitive color.
In order to solve the problem, technical scheme provided by the invention is: a kind of dyeing containing emerald green blue REACTIVE DYES, comprises the following steps:
(1) drift is boiled: technology preparation (g/L): hydrogen peroxide 6, stabilizing agent 1, soda ash 3.5, still an a conduit made of long bamboo oil S0.35, anti-creasing agent CD2.0, time/min, 50-60 bath raio is l:10; Successively add stabilizing agent, soda ash, a still a conduit made of long bamboo oil S, anti-creasing agent CD, hydrogen peroxide when 40 DEG C successively, be warming up to 90 DEG C;
(2) : dyeing craft prescription, (0, w, f %) : reactive turquoise blue B - BGFN3.0, reactive flavine B - 4 gln1. 43, active golden B - 4 rfn0. 95, 80, glauber's salt soda ash 25, leveling agent RG - 1332, dispersant EXL - 1061, bath ratio of l: 10; Dyeing process of sequence is RG a levelling agent 133 (3 g/l), a dispersant EXL 106 (1 g/l) temperature 40 ℃ to 40 ℃ one plus with clear hydrated good dye (30 min) insulation ~ 20 min - mirabilite 2/5 x 20 min one plus mirabilite 3/5 x 20 min one heats up to 60 ℃, 1.5 ℃ / min), a heat preservation mnin a soda ash 2% x 20 min 8% x 20 min a soda ash and soda ash 15% x 20 min a heat preservation 40 min to wash water l5min adding glacial acetic acid (45 ℃ by 15 min) a hot water wash (15 min) is 80 ℃ ~ soaping twice (90 ℃ X15min) by hot water wash (80 ℃ Xl5min) ~ hot water washing (60 ℃ by 15 min) 1 and PH6-7 (45 ℃ by 15 min) - fixation (45 ℃ by 15 min) ~ (45 ℃ by 15 min) _ - soft cloth.
Preferably, boiling drift initial temperature described in is 50 DEG C.
Preferably, boiling drift initial temperature described in is 55 DEG C.
Preferably, boiling drift initial temperature described in is 60 DEG C.
Compared with prior art, beneficial effect of the present invention is: this dyeing is simple, practical, not fugitive color, and grey cloth look flower problem improves, and fastness is significantly improved.
Detailed description of the invention
The present invention will be further described below:
Embodiment one:
Containing a dyeing for emerald green blue REACTIVE DYES, comprise the following steps:
(1) drift is boiled: technology preparation (g/L): hydrogen peroxide 6, stabilizing agent 1, soda ash 3.5, still an a conduit made of long bamboo oil S0.35, anti-creasing agent CD2.0, time/min, 50 bath raioes are l:10; Successively add stabilizing agent, soda ash, a still a conduit made of long bamboo oil S, anti-creasing agent CD, hydrogen peroxide when 40 DEG C successively, be warming up to 90 DEG C;
(2) : dyeing craft prescription, (0, w, f %) : reactive turquoise blue B - BGFN3.0, reactive flavine B - 4 gln1. 43, active golden B - 4 rfn0. 95, 80, glauber's salt soda ash 25, leveling agent RG - 1332, dispersant EXL - 1061, bath ratio of l: 10; Dyeing process of sequence is RG a levelling agent 133 (3 g/l), a dispersant EXL 106 (1 g/l) temperature 40 ℃ to 40 ℃ one plus with clear hydrated good dye (30 min) insulation ~ 20 min - mirabilite 2/5 x 20 min one plus mirabilite 3/5 x 20 min one heats up to 60 ℃, 1.5 ℃ / min), a heat preservation mnin a soda ash 2% x 20 min 8% x 20 min a soda ash and soda ash 15% x 20 min a heat preservation 40 min to wash water l5min adding glacial acetic acid (45 ℃ by 15 min) a hot water wash (15 min) is 80 ℃ ~ soaping twice (90 ℃ X15min) by hot water wash (80 ℃ Xl5min) ~ hot water washing (60 ℃ by 15 min) 1 and PH6-7 (45 ℃ by 15 min) - fixation (45 ℃ by 15 min) ~ (45 ℃ by 15 min) _ - soft cloth.
Compared with prior art, beneficial effect of the present invention is: this dyeing is simple, practical, not fugitive color, and grey cloth look flower problem improves, and fastness is significantly improved.
Embodiment two:
Containing a dyeing for emerald green blue REACTIVE DYES, comprise the following steps:
(1) drift is boiled: technology preparation (g/L): hydrogen peroxide 6, stabilizing agent 1, soda ash 3.5, still an a conduit made of long bamboo oil S0.35, anti-creasing agent CD2.0, time/min, 55 bath raioes are l:10; Successively add stabilizing agent, soda ash, a still a conduit made of long bamboo oil S, anti-creasing agent CD, hydrogen peroxide when 40 DEG C successively, be warming up to 90 DEG C;
(2) : dyeing craft prescription, (0, w, f %) : reactive turquoise blue B - BGFN3.0, reactive flavine B - 4 gln1. 43, active golden B - 4 rfn0. 95, 80, glauber's salt soda ash 25, leveling agent RG - 1332, dispersant EXL - 1061, bath ratio of l: 10; Dyeing process of sequence is RG a levelling agent 133 (3 g/l), a dispersant EXL 106 (1 g/l) temperature 40 ℃ to 40 ℃ one plus with clear hydrated good dye (30 min) insulation ~ 20 min - mirabilite 2/5 x 20 min one plus mirabilite 3/5 x 20 min one heats up to 60 ℃, 1.5 ℃ / min), a heat preservation mnin a soda ash 2% x 20 min 8% x 20 min a soda ash and soda ash 15% x 20 min a heat preservation 40 min to wash water l5min adding glacial acetic acid (45 ℃ by 15 min) a hot water wash (15 min) is 80 ℃ ~ soaping twice (90 ℃ X15min) by hot water wash (80 ℃ Xl5min) ~ hot water washing (60 ℃ by 15 min) 1 and PH6-7 (45 ℃ by 15 min) - fixation (45 ℃ by 15 min) ~ (45 ℃ by 15 min) _ - soft cloth.
Compared with prior art, beneficial effect of the present invention is: this dyeing is simple, practical, not fugitive color, and grey cloth look flower problem improves, and fastness is significantly improved.
Embodiment three:
Containing a dyeing for emerald green blue REACTIVE DYES, comprise the following steps:
(1) drift is boiled: technology preparation (g/L): hydrogen peroxide 6, stabilizing agent 1, soda ash 3.5, still an a conduit made of long bamboo oil S0.35, anti-creasing agent CD2.0, time/min, 60 bath raioes are l:10; Successively add stabilizing agent, soda ash, a still a conduit made of long bamboo oil S, anti-creasing agent CD, hydrogen peroxide when 40 DEG C successively, be warming up to 90 DEG C;
(2) : dyeing craft prescription, (0, w, f %) : reactive turquoise blue B - BGFN3.0, reactive flavine B - 4 gln1. 43, active golden B - 4 rfn0. 95, 80, glauber's salt soda ash 25, leveling agent RG - 1332, dispersant EXL - 1061, bath ratio of l: 10; Dyeing process of sequence is RG a levelling agent 133 (3 g/l), a dispersant EXL 106 (1 g/l) temperature 40 ℃ to 40 ℃ one plus with clear hydrated good dye (30 min) insulation ~ 20 min - mirabilite 2/5 x 20 min one plus mirabilite 3/5 x 20 min one heats up to 60 ℃, 1.5 ℃ / min), a heat preservation mnin a soda ash 2% x 20 min 8% x 20 min a soda ash and soda ash 15% x 20 min a heat preservation 40 min to wash water l5min adding glacial acetic acid (45 ℃ by 15 min) a hot water wash (15 min) is 80 ℃ ~ soaping twice (90 ℃ X15min) by hot water wash (80 ℃ Xl5min) ~ hot water washing (60 ℃ by 15 min) 1 and PH6-7 (45 ℃ by 15 min) - fixation (45 ℃ by 15 min) ~ (45 ℃ by 15 min) _ - soft cloth.
Compared with prior art, beneficial effect of the present invention is: this dyeing is simple, practical, not fugitive color, and grey cloth look flower problem improves, and fastness is significantly improved.
More than show and describe general principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (4)
1., containing a dyeing for emerald green blue REACTIVE DYES, comprise the following steps:
(1) drift is boiled: technology preparation (g/L): hydrogen peroxide 6, stabilizing agent 1, soda ash 3.5, still an a conduit made of long bamboo oil S0.35, anti-creasing agent CD2.0, time/min, 50-60 bath raio is l:10; Successively add stabilizing agent, soda ash, a still a conduit made of long bamboo oil S, anti-creasing agent CD, hydrogen peroxide when 40 DEG C successively, be warming up to 90 DEG C;
(2) : dyeing craft prescription, (0, w, f %) : reactive turquoise blue B - BGFN3.0, reactive flavine B - 4 gln1. 43, active golden B - 4 rfn0. 95, 80, glauber's salt soda ash 25, leveling agent RG - 1332, dispersant EXL - 1061, bath ratio of l: 10; Dyeing process of sequence is RG a levelling agent 133 (3 g/l), a dispersant EXL 106 (1 g/l) temperature 40 ℃ to 40 ℃ one plus with clear hydrated good dye (30 min) insulation ~ 20 min - mirabilite 2/5 x 20 min one plus mirabilite 3/5 x 20 min one heats up to 60 ℃, 1.5 ℃ / min), a heat preservation mnin a soda ash 2% x 20 min 8% x 20 min a soda ash and soda ash 15% x 20 min a heat preservation 40 min to wash water l5min adding glacial acetic acid (45 ℃ by 15 min) a hot water wash (15 min) is 80 ℃ ~ soaping twice (90 ℃ X15min) by hot water wash (80 ℃ Xl5min) ~ hot water washing (60 ℃ by 15 min) 1 and PH6-7 (45 ℃ by 15 min) - fixation (45 ℃ by 15 min) ~ (45 ℃ by 15 min) _ - soft cloth.
2. the dyeing containing emerald green blue REACTIVE DYES according to claim 1, is characterized in that, described in boil drift initial temperature be 50 DEG C.
3. the dyeing containing emerald green blue REACTIVE DYES according to claim 1, is characterized in that, described in boil drift initial temperature be 55 DEG C.
4. the dyeing containing emerald green blue REACTIVE DYES according to claim 1, is characterized in that, described in boil drift initial temperature be 60 DEG C.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104911927A (en) * | 2015-06-24 | 2015-09-16 | 浙江劲光实业股份有限公司 | Turquoise blue dyeing process of cellulose fiber |
| CN105484065A (en) * | 2015-12-31 | 2016-04-13 | 江苏金辰针纺织有限公司 | Reactive printing technology for machine-printed bleached linen fabric |
| CN105603777A (en) * | 2016-01-21 | 2016-05-25 | 上海婉静纺织科技有限公司 | Environment-friendly dyeing method of easy sleeping blue |
| CN106223075A (en) * | 2016-07-27 | 2016-12-14 | 博森织染（嘉兴）有限公司 | The emerald green colouring method of yarn |
| CN107227634A (en) * | 2017-07-05 | 2017-10-03 | 山东如意科技集团有限公司 | A kind of dyeing applied to colour-spun yarns fabrication processes |
| CN107476093A (en) * | 2017-08-14 | 2017-12-15 | 盐城福汇纺织有限公司 | A kind of combination constant temperature dyeing technique for looped fabric |
| CN108468230A (en) * | 2018-03-12 | 2018-08-31 | 南通楠桥纹织有限公司 | A kind of cotton yarn high temperature heavy colour dyeing and printing process |
| CN114683643A (en) * | 2022-04-18 | 2022-07-01 | 南安市南益电脑针织有限公司 | Breathable and refreshing knitted garment and knitting process |
| CN115807347A (en) * | 2022-12-02 | 2023-03-17 | 福建省新宏港纺织科技有限公司 | Reactive turquoise blue dyeing process |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104911927A (en) * | 2015-06-24 | 2015-09-16 | 浙江劲光实业股份有限公司 | Turquoise blue dyeing process of cellulose fiber |
| CN105484065A (en) * | 2015-12-31 | 2016-04-13 | 江苏金辰针纺织有限公司 | Reactive printing technology for machine-printed bleached linen fabric |
| CN105603777A (en) * | 2016-01-21 | 2016-05-25 | 上海婉静纺织科技有限公司 | Environment-friendly dyeing method of easy sleeping blue |
| CN106223075A (en) * | 2016-07-27 | 2016-12-14 | 博森织染（嘉兴）有限公司 | The emerald green colouring method of yarn |
| CN107227634A (en) * | 2017-07-05 | 2017-10-03 | 山东如意科技集团有限公司 | A kind of dyeing applied to colour-spun yarns fabrication processes |
| CN107476093A (en) * | 2017-08-14 | 2017-12-15 | 盐城福汇纺织有限公司 | A kind of combination constant temperature dyeing technique for looped fabric |
| CN108468230A (en) * | 2018-03-12 | 2018-08-31 | 南通楠桥纹织有限公司 | A kind of cotton yarn high temperature heavy colour dyeing and printing process |
| CN114683643A (en) * | 2022-04-18 | 2022-07-01 | 南安市南益电脑针织有限公司 | Breathable and refreshing knitted garment and knitting process |
| CN115807347A (en) * | 2022-12-02 | 2023-03-17 | 福建省新宏港纺织科技有限公司 | Reactive turquoise blue dyeing process |
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Application publication date: 20150128 |