CN104116454B - A kind of wet tissue and preparation method thereof - Google Patents
A kind of wet tissue and preparation method thereof Download PDFInfo
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- CN104116454B CN104116454B CN201410403669.5A CN201410403669A CN104116454B CN 104116454 B CN104116454 B CN 104116454B CN 201410403669 A CN201410403669 A CN 201410403669A CN 104116454 B CN104116454 B CN 104116454B
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Abstract
The present invention relates to daily sphere of life, in particular to a kind of wet tissue and preparation method thereof.The wet tissue, including wet tissue body and be sprayed on wet tissue body and weight for 23 times of wet tissue body wet tissue liquid；Wherein, according to percent by weight, in wet tissue liquid, its component Bao Kuo limonenes 0.10% 1.0%, APG 0.60% 6.0%, polyaminopropyl biguanide 0.10% 0.30%, benzalkonium chloride 0.05% 0.10%, vitamin E 0.05% 0.3%, extract solution from aloe 0.10% 1.0%, citric acid 0.005% 0.15%, deionized water 91.45% 98.995%.The wet tissue that the present invention is provided is improved by the prescription to wet tissue liquid, potential safety hazard present in prior art (excitant, corrosivity or carcinogenicity etc.) is overcome, so that for the daily cleaning of people provides a kind of wet tissue of real safety non-toxic.
Description
Technical field
The present invention relates to daily sphere of life, in particular to a kind of wet tissue and preparation method thereof.
Background technology
In the daily life that wet tissue has been widely used as a kind of cleaning products.In general, it is wrapped
Include the thimerosal composition of wet tissue body and sprayed coating on wet tissue body.And for thimerosal, it is typically lived by organic solvent, surface
Property agent and the chemical reagent with sterilization and anticorrosion effect composition.
In the related art, household cleaning class product (including constituting the thimerosal of wet tissue) is generally pH value in highly acid or strong
Basic products, therefore, its excitant to skin during use is stronger, also with larger corrosivity.For organic
Solvent, is mostly organic synthesis gained, and its strong detergency stimulates article simultaneously, corrosivity is big.And big multi-solvent contains toxicity.
Its is fat-soluble can rapidly to absorb through complete skin, and Long Term Contact has a negative impact to health unavoidably.Lived for surface
Property agent, oil based surfactants are commonly used in correlation technique, the surfactant is unavoidable during synthesis to produce malicious by-product
Thing-dioxanes, oxirane or nitrosamine etc.；During long-term use, the health to human body has adverse effect on unavoidably；In addition,
It has certain corrosivity to plastics household to this oil based surfactants, therefore, use its long-term wiping plastics household
When, certain damage can be produced to plastics household.For the chemical reagent with sterilization and anticorrosion effect, acyl in DMDM second is commonly used at present
The different plug oxazoline ketone (Kathon CG) of the different plug oxazoline ketone/methyl chloride of urea, methyl, Bronopol, IPBC or parabens etc.；However,
DMDMH is chloride Form aldehyde release body, the different plug oxazoline ketone (Kathon CG) of the different plug oxazoline ketone/methyl chloride of methyl, may be stimulated
Skin, Bronopol may result in the formation of carcinogen nitrosamine, IPBC iodine is may result in during use to be taken the photograph
Enter, parabens contains phenyl ring, after it adds up in vivo, easily increase the danger that women suffers from breast cancer.
To sum up, wet tissue common in correlation technique, its thimerosal composition exist certain potential safety hazard (have excitant,
Corrosivity or carcinogenicity etc.)；Therefore, it is a kind of daily cleaning (kitchen cleaning, bathroom cleaner, furniture cleaning) peace of offer of people
The wet tissue of Atoxic is those skilled in the art's technical problem urgently to be resolved hurrily.
The content of the invention
It is an object of the invention to provide a kind of wet tissue, to solve above-mentioned technical problem.Another object of the present invention
It is that a kind of preparation method of above-mentioned wet tissue is provided.
Wet tissue is provided in an embodiment of the present invention, including wet tissue body and is sprayed on the wet tissue body and weight
It is the wet tissue liquid of 2-3 times of the wet tissue body；Wherein, according to percent by weight, in the wet tissue liquid, its component bag
Kuo limonenes 0.10%-1.0%, APG 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride
0.05%-0.10%, vitamin E 0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-
0.15%th, deionized water 91.45%-98.995%.
This wet tissue that the present invention is provided, it is that its 2-3 times wet tissue liquid is constituted by wet tissue body and weight, wherein,
In wet tissue liquid, its Bao Han limonenes, APG, polyaminopropyl biguanide, benzalkonium chloride, vitamin E, extract solution from aloe etc.
Active princlple.
Specific , limonenes are a kind of green and environment-friendly solvent, the fragrant aroma with sweet orange, while having stronger decontamination to imitate
Really, it is natural, nontoxic, nuisanceless and with natural bactericidal action.The various organic solvents for using at present are substituted with it, is changed
Heavy chemicals poisonous and harmful in correlation technique or with excitant or corrosivity this defect.
APG wetting power is strong, strong detergency, foaming abundancy are fine and smooth, nontoxic, harmless, non-stimulated to skin, biology drop
Solution is rapid thoroughly, is internationally recognized first-selection " green " functional surfactant.Existing petroleum base surface-active is substituted with it
Agent, without harmful by-products dioxanes, oxirane and nitrosamine etc., and has good compatibility, Jin Erke with plastic products
Take in the prior art because oil based surfactants are poisonous or the technological deficiency of corrosivity and damage plastics household.
Polyaminopropyl biguanide and benzalkonium chloride compound sterilizing system, two-component belong to non oxidizing bactericide, by influence
The osmotic pressure of microbial cell, makes membranolysis, shrinks and dehydration, so as to reach the effect of sterilization.Wherein, poly- aminopropyl is double
Guanidine is a Novel sterilizing sterilization antiseptic, and to bacterium, saccharomycete and mould have the bacteriostatic activity of wide spectrum.It has gentle day
Right property, can be used for mucous membrane class includes eye mucous membranes product.And benzalkonium chloride is a traditional disinfection bactericide, have to bacterium mould
The inhibitory action of wide spectrum.After two components compounding, the effect of Synergistic is reached, BA detection is carried out through laboratory, its is right
The strains such as Escherichia coli, staphylococcus aureus, Pseudomonas aeruginosa, Klebsiella Pneumoniae, contact condition is 5min, and its sterilizing rate reaches
99.99%, while having bacteriostasis to aspergillus niger；Therefore can be effectively as the antisepsis and sterilization in the wet tissue liquid of the application
Disinfectant.
Additionally, set percetage by weight vitamin E has the effect of skin care, do not hurt hands, safety non-toxic；Aloe is extracted
Liquid has and forms air-permeable protective film in skin surface, easily isolation infringement of the external contamination to hand, cleaning simultaneously, with making skin
The effects such as skin convergence, antiallergy, moisturizing, anti-inflammatory, and the citric acid of set percetage by weight its can cause whole wet tissue liquid
PH maintain between 5.0-7.0 (in faintly acid), the scope presses close to the pH of human body skin, and then it is not injured skin sparing
Film, reaches the effect of care both hands jointly.
Therefore, compared with prior art, the wet tissue of the application is improved by the prescription to wet tissue liquid, and sets spy
Fixed compatibility relationship so that the wet tissue being made overcomes potential safety hazard present in prior art (excitant, corrosivity or carcinogenic
Property etc.), so that for the daily cleaning (kitchen cleaning, bathroom cleaner, furniture cleaning) of people provides a kind of real safety non-toxic
Wet tissue.
Optionally, Suo Shu limonenes are extracted from citrus fruit and obtained.
Optionally, the APG is extracted from corn or coconut oil and obtained.
Optionally, the APG is octyl group/Plantacare 818.
Optionally, the wet tissue body is spunlace non-woven cloth.
The embodiment of the present invention additionally provides a kind of preparation method according to above-mentioned wet tissue, comprises the following steps：
(1) wet tissue liquid, is configured；
(2), the wet tissue liquid is uniformly spilt according to set weight ratio and packed after dropping in wet tissue body, obtained
Wet tissue.
Optionally, in step (1), specifically include：Stirred after limonene, APG are according to set weight ratio mixing
Uniformly, the first mixed liquor is obtained；
The polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are added to deionization
In water, stir, obtain the second mixed liquor；
Second mixed liquor is added in first mixed liquor, is stirred and evenly mixed, and citric acid is added dropwise, will be mixed with
The pH of the first mixed liquor of two mixed liquors is adjusted to 5.0-7.0, obtains wet tissue liquid.
Optionally, it is described Jiang limonene, APG according to set weight than mixing after stir, obtain first and mix
In the step of closing liquid：The temperature during mixing is 20-30 DEG C.
Optionally, it is described Jiang limonene, APG according to set weight than mixing after stir, obtain first and mix
In the step of closing liquid：
The rotating speed of the stirring is 1500-2000 revs/min, the time is 10-20 minutes.
Optionally, second mixed liquor is added in first mixed liquor described, is stirred and evenly mixed, and lemon is added dropwise
Lemon acid, the pH that will be mixed with the first mixed liquor of the second mixed liquor is adjusted to 5.0-7.0, the step of obtain wet tissue liquid in：
The rotating speed of the stirring is 1000-1500 revs/min, the time is 10-20 minutes.
Brief description of the drawings
In order to illustrate more clearly of the specific embodiment of the invention or technical scheme of the prior art, below will be to specific
The accompanying drawing to be used needed for implementation method or description of the prior art is briefly described, it should be apparent that, in describing below
Accompanying drawing is some embodiments of the present invention, for those of ordinary skill in the art, before creative work is not paid
Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the preparation flow schematic diagram of the wet tissue that the embodiment of the present invention four is provided.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below
Clear, complete description, based on the specific embodiment in the present invention, those of ordinary skill in the art are not making creativeness
Resulting all other implementation method on the premise of work, belongs to the scope that the present invention is protected.
This wet tissue that the present invention is provided, including wet tissue body and be sprayed on the wet tissue body and weight is for described wet
The wet tissue liquid of 2-3 times of towel body；
Wherein, according to percent by weight, in the wet tissue liquid, its component Bao Kuo limonenes 0.10%-1.0%, alkane
Base glucosides 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride 0.05%-0.10%, vitamin E
0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-0.15%, deionized water 91.45%-
98.995%；In addition, used as preferred scheme, Suo Shu limonenes are extracted from citrus fruit and obtained；And/or the APG
Extracted from corn or coconut oil and obtained；In addition, APG is preferably octyl group/Plantacare 818.Also, the wet tissue body
It is spunlace non-woven cloth, the material for such as mixing in any proportion for viscose fiber or terylene or both, unit grammes per square metre is 30-150 grams/
㎡。
Additionally, the present invention constitutes the embodiment for providing in detail below herein in connection with above-mentioned content to wet tissue：
Embodiment one
The wet tissue of the present embodiment, including wet tissue body and be sprayed on the wet tissue body and weight be the wet tissue body
2-3 times of wet tissue liquid；Wherein, it is its component Bao Kuo limonenes 0.1%, pungent in the wet tissue liquid according to percent by weight
Base/Plantacare 818 0.6%, polyaminopropyl biguanide 0.1%, benzalkonium chloride 0.1%, vitamin E 0.05%, extract solution from aloe
1.0%th, citric acid 0.01%, deionized water 98.04%.
Embodiment two
The wet tissue of the present embodiment, including wet tissue body and be sprayed on the wet tissue body and weight be the wet tissue body
2-3 times of wet tissue liquid；Wherein, it is its component Bao Kuo limonenes 0.5%, pungent in the wet tissue liquid according to percent by weight
Base/Plantacare 818 3.3%, polyaminopropyl biguanide 0.2%, benzalkonium chloride 0.07%, vitamin E 0.2%, extract solution from aloe
0.55%th, citric acid 0.07%, deionized water 95.11%.
Embodiment three
The wet tissue of the present embodiment, including wet tissue body and be sprayed on the wet tissue body and weight be the wet tissue body
2-3 times of wet tissue liquid；Wherein, it is its component Bao Kuo limonenes 1.0%, pungent in the wet tissue liquid according to percent by weight
Base/Plantacare 818 6.0%, polyaminopropyl biguanide 0.3%, benzalkonium chloride 0.05%, vitamin E 0.3%, extract solution from aloe
0.10%th, citric acid 0.1%, deionized water 92.15%.
In addition, based in above-mentioned all embodiments, used as further alternatively scheme, octyl group/Plantacare 818 can be with
By etc. his APG of weight substitute, the alkane that the carbochain component such as such as APG0814, APG0816, APG1214, APG1216 differs
Base glycoside surfactant.Additionally, in above-mentioned all embodiments, preferred , limonenes selection is extracted from citrus fruit and obtained
Obtain, it has the fragrant aroma of sweet orange while having stronger clean effect to extract Huo get limonenes from citrus fruit, and tool
There is natural bactericidal action, it is natural, nontoxic, nuisanceless.Food flavor additive has been identified as in the world, has been U.S.'s food
And the freed-from-inspection product of FAD (FDA), it is safe；APG is extracted from corn and coconut oil and obtained；Corn comes
Source is easier to, and can provide sufficiently guarantee for its preparation.
In order that the wet tissue for obtaining the above embodiment of the present invention is preferably applied, the more efficient furniture cleaning that is applied to disappears
In the field of poison, the present invention also provides example IV on the basis of above-described embodiment, and example IV gives above-mentioned reality
The preparation method for applying the wet tissue of example, is now described in detail and explains, refer to Fig. 1：
Example IV
Fig. 1 is refer to, in the present embodiment, the preparation method of wet tissue is comprised the following steps：
Step 101：Stirred after limonene, APG are according to set weight ratio mixing, obtain the first mixed liquor；
You Yu limonenes are liposoluble substance, to be applied it in aqueous solution systems (follow-up second mixed liquor), need to be obtained
O/W type emulsification systems, the present embodiment uses hydrophilic lipophilic balance (HLB) method, and selection HLB value is the natural A PG (alkane of 14-16
Base glucosides) as emulsifying agent , Yu limonenes with 6:1 weight obtains the first mixed liquor than mixing after stirring and evenly mixing.
In a step 101, for the effect for realizing that limonene is emulsified fully and quickly mixed, the temperature during mixing
For 20-30 DEG C (in the temperature range, because APG HLB value is higher, in the range of 20-30 DEG C, you can play its work
Property, its larger polar group is stretched into water phase, nonpolar C-H bond gos deep into oil phase, reduces its interfacial tension, forms one layer of guarantor
Cuticula, is surrounded completely by interior to oil, forms O/W emulsions.Conventional emulsification product then needs the breast in the range of 75 DEG C -85 DEG C
Change, this product emulsifying process is simple, and production cost is reduced while improve production efficiency)；The rotating speed of the stirring is
1500-2000 revs/min, the time be 10-20 minutes.
Step 102：The polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are added
To in deionized water, stir, obtain the second mixed liquor；
Specifically, by a container for being pre-loaded with deionized water, polyaminopropyl biguanide, benzene then are pricked into chlorine respectively
Ammonium, vitamin E, extract solution from aloe are added, and after stirring and evenly mixing, obtain the second mixed liquor.
Step 103：Second mixed liquor is added in first mixed liquor, is stirred and evenly mixed, and citric acid is added dropwise,
The pH that the first mixed liquor of the second mixed liquor will be mixed with is adjusted to 5.0-7.0, obtains wet tissue liquid；
In step 103, the rotating speed of the stirring be 1000-1500 revs/min, the time be 10-20 minutes.
Step 104：The wet tissue liquid is uniformly spilt according to set weight ratio and packed after dropping in wet tissue body,
Obtain wet tissue.
Specifically, during drop is spilt, the weight of wet tissue liquid is 2-3 times of wet tissue body.In addition, the present invention is also carried
Supplied above-described embodiment provide wet tissue dirt-removing power test, bactericidal effect test, black-koji mould preservation challenge test and
Plastics product compatibility test；Specifically, to further illustrate practical effect of the invention, using several type testings
Case is illustrated：
1st, dirt-removing power test：
Experiment one：Tested material is kitchen tile wall and marble countertop, there is moderate greasy dirt, with the offer of embodiment one
Wet tissue wipes kitchen tile wall and marble countertop.Wiping is finished, kitchen tile wall and marble countertop without greasy dirt,
Operator is felt to no skin irritation.
Experiment two：Tested object is glass tea table, and household electrical appliance (refrigerator, television set) shell, have slight tea stain with
And dirt, the wet tissue tested body surface of wiping provided with embodiment two.Wiping is finished, and tea stain and dirt are eliminated completely,
Operator is felt to no skin irritation.
Experiment three：Tested material is bathroom tile wall and sanitary bath equipment, there is soap scum, incrustation scale, human body dirt, uses embodiment
Three wet tissues for providing wipe object, and after wiping is finished, shower wall and sanitary bath equipment dirt are removed substantially, and operator feels right
No skin irritation.
2nd, bactericidal effect test：
The sample provided with embodiment one and three, is respectively labeled as：Kitchen cleaning pasteurization towelette 1#, kitchen cleaning sterilization is wet
Towel 2#.Through third party authority testing agency according to GB15979/2002《Disposable Sanitary Accessory sanitary standard》Standard,
Sterilized test is carried out to Escherichia coli, staphylococcus aureus, Pseudomonas aeruginosa, Klebsiella Pneumoniae.Black-koji mould is prevented
Rotten challenge test.Test result is as follows：
The wet tissue of the various embodiments of the present invention of table 1 is tested the bactericidal effect of different strain
3rd, black-koji mould preservation challenge test：
The wet tissue of the various embodiments of the present invention of table 2 is to black-koji mould preservative challenge testing
4 and plastics product compatibility test：
Nail has plastics (polymethyl methacrylate) test-strips of STAINLESS STEEL NAILS (formation tension force) in the middle of one piece of selection, often
Its short time immerses solution to be measured, and the situation of test-strips is observed after certain hour.Evaluation grade is divided into：It is unchanged；Form crack；
Obvious crack；Fracture.
The wet tissue of the various embodiments of the present invention of table 3 and plastics product compatibility test
| 4 hours | 3 days | 7 days | 14 days | |
| Embodiment one | It is unchanged | It is unchanged | It is unchanged | It is unchanged |
| Embodiment three | It is unchanged | It is unchanged | It is unchanged | It is unchanged |
The preferred embodiments of the present invention are the foregoing is only, is not intended to limit the invention, for the skill of this area
For art personnel, the present invention can have various modifications and variations.It is all within the spirit and principles in the present invention, made any repair
Change, equivalent, improvement etc., should be included within the scope of the present invention.
Claims (7)
1. a kind of wet tissue, it is characterised in that including wet tissue body and be sprayed on the wet tissue body and weight is the wet tissue
The wet tissue liquid of 2-3 times of body；
Wherein, according to percent by weight, in the wet tissue liquid, its component Bao Kuo limonenes 0.10%-1.0%, alkyl sugar
Glycosides 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride 0.05%-0.10%, vitamin E
0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-0.15%, deionized water 91.45%-
98.995%；
The APG is extracted from corn or coconut oil and obtained；The APG is octyl group/Plantacare 818；
Suo Shu limonenes are extracted from citrus fruit and obtained.
2. wet tissue according to claim 1, it is characterised in that the wet tissue body is spunlace non-woven cloth.
3. a kind of preparation method of wet tissue according to claim 1, it is characterised in that comprise the following steps：
(1) wet tissue liquid, is configured；
(2), the wet tissue liquid is uniformly spilt according to set weight ratio and packed after dropping in wet tissue body, obtain wet
Towel.
4. the preparation method of wet tissue according to claim 3, it is characterised in that in step (1), specifically include：
Stirred after limonene, APG are according to set weight ratio mixing, obtain the first mixed liquor；
The polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are added in deionized water,
Stir, obtain the second mixed liquor；
Second mixed liquor is added in first mixed liquor, is stirred and evenly mixed, and citric acid is added dropwise, second will be mixed with and mixed
The pH for closing the first mixed liquor of liquid is adjusted to 5.0-7.0, obtains wet tissue liquid.
5. the preparation method of wet tissue according to claim 4, it is characterised in that it is described Jiang limonene, APG according to
Set weight than being stirred after mixing, the step of obtain the first mixed liquor in：
The temperature during mixing is 20-30 DEG C.
6. the preparation method of wet tissue according to claim 5, it is characterised in that it is described Jiang limonene, APG according to
Set weight than being stirred after mixing, the step of obtain the first mixed liquor in：
The rotating speed of the stirring is 1500-2000 revs/min, the time is 10-20 minutes.
7. the preparation method of the wet tissue according to claim any one of 4-6, it is characterised in that mixed described second described
Close liquid to be added in first mixed liquor, stir and evenly mix, and citric acid is added dropwise, the first mixed liquor of the second mixed liquor will be mixed with
PH be adjusted to 5.0-7.0, the step of obtain wet tissue liquid in：
The rotating speed of the stirring is 1000-1500 revs/min, the time is 10-20 minutes.
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| CN104825093B (en) * | 2015-04-30 | 2016-04-20 | 威莱(广州)日用品有限公司 | Cleaning glass wet tissue of a kind of not trace and preparation method thereof |
| CN106038356B (en) * | 2016-07-04 | 2019-02-26 | 苏州宝丽洁日化有限公司 | A kind of physical antibacterial wet tissue and preparation method thereof |
| CN106420591A (en) * | 2016-09-05 | 2017-02-22 | 北京蓝色美城科技有限公司 | Wet tissue containing fermented supernatant fluid of lactic acid bacteria and special wet tissue solution for wet tissue containing fermented supernatant fluid of lactic acid bacteria |
| WO2018080492A1 (en) * | 2016-10-27 | 2018-05-03 | Kimberly-Clark Worldwide, Inc. | Fibrous structures comprising volatile agave compounds |
| US11261568B2 (en) | 2016-10-27 | 2022-03-01 | Kimberly-Clark Worldwide, Inc. | High bulk wet-pressed agave tissue |
| AU2016427801B2 (en) | 2016-10-27 | 2021-11-04 | Kimberly-Clark Worldwide, Inc. | High strength and low stiffness agave tissue |
| CN106421217B (en) * | 2016-11-14 | 2017-12-01 | 广东洛斯特制药有限公司 | A kind of solution of benzalkonium chloride and preparation method thereof |
| WO2018156109A1 (en) | 2017-02-22 | 2018-08-30 | Kimberly-Clark Worldwide, Inc. | Layered tissue comprising non-wood fibers |
| CN107440985A (en) * | 2017-06-16 | 2017-12-08 | 广州白云山拜迪生物医药有限公司 | A kind of efficient sterilizing wet sanitary napkins containing plant component and preparation method thereof |
| CN108192748A (en) * | 2017-12-28 | 2018-06-22 | 泉州市晋江恒安卫生科技有限公司 | A kind of impregnated wipe and preparation method thereof |
| JP7022653B2 (en) * | 2018-06-01 | 2022-02-18 | 大阪化成株式会社 | Processing agent for antiviral fiber and treatment liquid for antiviral fiber, antiviral fiber product processed by it, and manufacturing method thereof |
| CN110477792A (en) * | 2019-09-05 | 2019-11-22 | 林建广 | A kind of nonalcoholic wet tissue and preparation method thereof can be used for breathing mask cleaning-sterilizing |
| CN110585031A (en) * | 2019-10-18 | 2019-12-20 | 海安康瑞纺织品有限公司 | Wet tissue for cleaning, removing sweat and disinfecting skin after exercise and preparation method thereof |
| CN110731936A (en) * | 2019-10-18 | 2020-01-31 | 海安康瑞纺织品有限公司 | Wet towel for cleaning, disinfecting and deodorizing pet body |
| CN111888316A (en) * | 2020-09-11 | 2020-11-06 | 乔康 | Antibacterial high-moisturizing hand cream and preparation method thereof |
| CN112852556B (en) * | 2021-01-07 | 2021-11-30 | 茂名张氏科技发展有限公司 | Household sterilizing, cleaning and mite-removing wet tissue |
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| CN101230310B (en) * | 2007-01-25 | 2012-02-08 | 3M创新有限公司 | Cleaning method and combination |
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| CN102846257A (en) * | 2012-08-29 | 2013-01-02 | 铜陵洁雅生物科技股份有限公司 | Hard surface cleaning disinfecting wet tissue |
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