CN104116454A - Wet tissue and preparation method thereof - Google Patents
Wet tissue and preparation method thereof Download PDFInfo
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- CN104116454A CN104116454A CN201410403669.5A CN201410403669A CN104116454A CN 104116454 A CN104116454 A CN 104116454A CN 201410403669 A CN201410403669 A CN 201410403669A CN 104116454 A CN104116454 A CN 104116454A
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Abstract
The invention relates to the field of daily life, in particular to a wet tissue and a preparation method of the wet tissue. The wet tissue comprises a wet tissue body and wet tissue liquid sprayed on the wet tissue body, and the weight of the wet tissue liquid is 2 times-3 times that of the wet tissue body. The wet tissue liquid comprises, by weight, 0.1-1.0% of limonene, 0.6-6.0% of alkyl glycoside, 0.1-0.3% of polyaminopropyl biguanide, 0.05-0.1% of benzalkonium chloride, 0.05-0.3% of vitamin E, 0.1-1.0% of an aloe extracting solution, 0.005-0.15% of citric acid and 91.45-98.995% of deionized water. According to the wet tissue, the formula of the wet tissue liquid is improved, so that potential safety hazards (such as irritation, corrosivity and carcinogenicity) existing in the prior art are eliminated, and the really safe and nontoxic wet tissue is supplied to people for daily cleanness.
Description
Technical field
The present invention relates to daily sphere of life, in particular to a kind of wet tissue and preparation method thereof.
Background technology
In the daily life that wet tissue has been widely used as a kind of cleaning products.Generally speaking, it comprises wet tissue body and the sprayed coating thimerosal composition on wet tissue body.And for thimerosal, it is generally made up of organic solvent, surfactant and the chemical reagent with sterilization and anticorrosion effect.
In correlation technique, household cleaning series products (comprising the thimerosal that forms wet tissue) mostly is pH value and is highly acid or strong basicity product, and therefore, it is stronger to the excitant of skin in the process using, and also has larger corrosivity.For organic solvent, be mostly organic synthesis gained, its strong detergency simultaneously to article stimulate, corrosivity is large.And large multi-solvent contains toxicity.Its fat-soluble can absorption rapidly through complete skin, Long Term Contact, has a negative impact to health unavoidably.For surfactant, conventional petroleum base surfactant in correlation technique, this surfactant is unavoidable toxic byproduct-dioxanes, oxirane or the nitrosamine etc. of producing in synthetic process; When long-term use, unavoidably the health of human body is produced to adverse influence; In addition, it has certain corrosivity to plastics household this petroleum base surfactant, therefore, while using its long-term wiping plastics household, can produce certain damage to plastics household.For the chemical reagent with sterilization and anticorrosion effect, conventional DMDMH, the different plug azoles of methyl quinoline ketone/methyl chloride different plug azoles quinoline ketone (Kathon CG), Bronopol, IPBC or parabens etc. at present; But, DMDMH is that formaldehyde releaser, the different plug azoles of methyl quinoline ketone/methyl chloride different plug azoles quinoline ketone (Kathon CG) are chloride, may chafe, Bronopol may cause formation, the IPBC of carcinogen nitrosamine in the process using, may cause that iodine is taken in, parabens contains phenyl ring, it easily increases the danger that women suffers from breast cancer after adding up in vivo.
To sum up, common wet tissue in correlation technique, there is certain potential safety hazard (thering are excitant, corrosivity or carcinogenicity etc.) in its thimerosal composition; Therefore be, those skilled in the art's technical problems urgently to be resolved hurrily for people's daily cleaning (kitchen cleaning, bathroom cleaner, furniture clean) provides a kind of wet tissue of safety non-toxic.
Summary of the invention
The object of the present invention is to provide a kind of wet tissue, to solve above-mentioned technical problem.Another object of the present invention is to provide a kind of preparation method of above-mentioned wet tissue.
Wet tissue is provided in an embodiment of the present invention, has comprised that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly; Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 0.10%-1.0%, APG 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride 0.05%-0.10%, vitamin E 0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-0.15%, deionized water 91.45%-98.995%.
This wet tissue provided by the invention, it is that its 2-3 wet tissue liquid doubly forms by wet tissue body and weight, wherein, in wet tissue liquid, it comprises the active princlples such as limonene, APG, polyaminopropyl biguanide, benzalkonium chloride, vitamin E, extract solution from aloe.
Ju body ， limonene is a kind of green and environment-friendly solvent, has the fragrant fragrance of sweet orange, has stronger clean effect simultaneously, and has natural bactericidal action, natural, nontoxic, nuisanceless.Substitute with it various organic solvents that use at present, change the heavy chemicals poisonous and harmful in correlation technique or there is excitant or this defect of corrosivity.
APG wetting power is strong, strong detergency, foam are abundant fine and smooth, nontoxic, harmless, non-stimulated to skin, and biodegradation is thorough rapidly, is internationally recognized first-selection " green " functional surface activating agent.Substitute existing petroleum base surfactant with it, do not contain toxic byproduct dioxanes, oxirane and nitrosamine etc., and there is good compatibility with plastic products, and then overcome in prior art because petroleum base surfactant is poisonous or the technological deficiency of corrosivity and damage plastics household.
Polyaminopropyl biguanide and benzalkonium chloride compound sterilizing system, two compositions all belong to non oxidizing bactericide, by affecting the osmotic pressure of microbial cell, make membranolysis, shrink and dehydration, thereby reach the effect of sterilization.Wherein, polyaminopropyl biguanide is a Novel sterilizing sterilization antiseptic, and to bacterium, saccharomycete and mould have the bacteriostatic activity of wide spectrum.It has gentle natural character, can be used for mucous membrane class and comprises eye mucous membrane product.And benzalkonium chloride is a traditional disinfectant, bacterium mould is had to the inhibitory action of wide spectrum.After two components are composite, reach the effect of Synergistic, carry out BA detection through laboratory, it is to bacterial classifications such as Escherichia coli, staphylococcus aureus, Pseudomonas aeruginosa, Klebsiella Pneumoniaes, contact condition is 5min, and its sterilizing rate reaches 99.99%, aspergillus niger is had to bacteriostasis simultaneously; Therefore can be effectively as the antisepsis and sterilization disinfectant in the application's wet tissue liquid.
In addition, set percetage by weight vitamin E has the effect of skin care, does not hinder hand, safety non-toxic; Extract solution from aloe has at skin surface formation air-permeable protective film; easily isolating exterior pollutes the infringement to hand; simultaneously clean; there is the effects such as the skin contraction of making, antiallergy, moisturizing, anti-inflammatory; and the citric acid of set percetage by weight its can make the pH of whole wet tissue liquid maintain between 5.0-7.0 (to be faintly acid); this scope is pressed close to the pH of human body skin, and then makes it not injure skin sparing film, jointly reaches the effect of care both hands.
Therefore, compared with prior art, the application's wet tissue is by improving the prescription of wet tissue liquid, and set specific compatibility relationship, make the wet tissue of making overcome the potential safety hazard (excitant, corrosivity or carcinogenicity etc.) existing in prior art, thereby provide a kind of wet tissue of real safety non-toxic for people's daily cleaning (kitchen cleaning, bathroom cleaner, furniture are clean).
Optionally, Suo Shu limonene extracts and obtains from citrus fruit.
Optionally, described APG extracts and obtains from corn or coconut oil.
Optionally, described APG is octyl group/Plantacare 818.
Optionally, described wet tissue body is spunlace non-woven cloth.
It is a kind of according to the preparation method of above-mentioned wet tissue that the embodiment of the present invention also provides, and comprises the following steps:
(1), configuration wet tissue liquid;
(2), described wet tissue liquid is spilt uniformly after dropping in wet tissue body and packed according to set weight ratio, obtain wet tissue.
Optionally, in step (1), specifically comprise that: stirs after limonene, APG mix according to set weight ratio, obtains the first mixed liquor;
The polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are joined in deionized water, stir, obtain the second mixed liquor;
Described the second mixed liquor is joined in described the first mixed liquor, stir and evenly mix, and drip citric acid, the pH of the first mixed liquor that is mixed with the second mixed liquor is adjusted to 5.0-7.0, obtain wet tissue liquid.
Optionally, stir after limonene, APG mix according to set weight ratio described, obtain in the step of the first mixed liquor: temperature when described mixing is 20-30 DEG C.
Optionally, stir after limonene, APG mix according to set weight ratio described, obtain in the step of the first mixed liquor:
The rotating speed of described stirring is that 1500-2000 rev/min, time are 10-20 minute.
Optionally, described, described the second mixed liquor is joined in described the first mixed liquor, stirs and evenly mixs, and drip citric acid, the pH of the first mixed liquor that is mixed with the second mixed liquor is adjusted to 5.0-7.0, obtain in the step of wet tissue liquid:
The rotating speed of described stirring is that 1000-1500 rev/min, time are 10-20 minute.
Brief description of the drawings
In order to be illustrated more clearly in the specific embodiment of the invention or technical scheme of the prior art, to the accompanying drawing of required use in detailed description of the invention or description of the Prior Art be briefly described below, apparently, accompanying drawing in the following describes is some embodiments of the present invention, for those of ordinary skill in the art, do not paying under the prerequisite of creative work, can also obtain according to these accompanying drawings other accompanying drawing.
The preparation flow schematic diagram of the wet tissue that Fig. 1 provides for the embodiment of the present invention four.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer; to technical scheme of the present invention be carried out to clear, complete description below; based on the detailed description of the invention in the present invention; all other embodiments that those of ordinary skill in the art obtain under the prerequisite of not making creative work, all belong to the scope that the present invention protects.
This wet tissue provided by the invention, comprises that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly;
Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 0.10%-1.0%, APG 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride 0.05%-0.10%, vitamin E 0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-0.15%, deionized water 91.45%-98.995%; In addition, as preferred scheme, Suo Shu limonene extracts and obtains from citrus fruit; With or described APG from corn or coconut oil, extract and obtain; In addition, APG is preferably octyl group/Plantacare 818.And described wet tissue body is spunlace non-woven cloth, as being viscose fiber or terylene or material that both mix in any proportion, unit grammes per square metre is 30-150 Ke/㎡.
In addition, the present invention, also in conjunction with above-mentioned content, provides following specific embodiment to the composition of wet tissue:
Embodiment mono-
The wet tissue of the present embodiment, comprises that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly; Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 0.1%, octyl group/Plantacare 818 0.6%, polyaminopropyl biguanide 0.1%, benzalkonium chloride 0.1%, vitamin E 0.05%, extract solution from aloe 1.0%, citric acid 0.01%, deionized water 98.04%.
Embodiment bis-
The wet tissue of the present embodiment, comprises that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly; Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 0.5%, octyl group/Plantacare 818 3.3%, polyaminopropyl biguanide 0.2%, benzalkonium chloride 0.07%, vitamin E 0.2%, extract solution from aloe 0.55%, citric acid 0.07%, deionized water 95.11%.
Embodiment tri-
The wet tissue of the present embodiment, comprises that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly; Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 1.0%, octyl group/Plantacare 818 6.0%, polyaminopropyl biguanide 0.3%, benzalkonium chloride 0.05%, vitamin E 0.3%, extract solution from aloe 0.10%, citric acid 0.1%, deionized water 92.15%.
In addition, in above-mentioned all embodiment, as further alternative scheme, octyl group/Plantacare 818 can by etc. his APG of weight substitute, as APG0814, APG0816, APG1214, the APG class surfactant that the carbochain components such as APG1216 differ.In addition,, in above-mentioned all embodiment, preferred limonene is selected to extract and obtain from citrus fruit, from citrus fruit, extract its fragrant fragrance with sweet orange of Huo get limonene and there is stronger clean effect simultaneously, and there is natural bactericidal action, natural, nontoxic, nuisanceless.Be identified as in the world food flavor additive, for the freed-from-inspection product of U.S. food and FAD (FDA), safe; APG extracts and obtains from corn and coconut oil; Corn source is easier, can be its preparation sufficient guarantee is provided.
For the wet tissue that makes the above embodiment of the present invention is better applied, more effectively be applied in the field of furniture cleaning-sterilizing, the present invention also provides embodiment tetra-on the basis of above-described embodiment, embodiment tetra-has provided the preparation method of the wet tissue of above-described embodiment, now be described in detail and explain, please refer to Fig. 1:
Embodiment tetra-
Please refer to Fig. 1, in the present embodiment, the preparation method of wet tissue comprises the following steps:
Step 101: stirs after limonene, APG mix according to set weight ratio, obtains the first mixed liquor;
You Yu limonene is liposoluble substance, apply it in water-soluble system (follow-up the second mixed liquor), need obtain O/W type emulsification system, the present embodiment adopts hydrophilic lipophilic balance (HLB) method, select the natural A PG (APG) that HLB value is 14-16 to mix with the weight ratio of 6:1 Yu limonene as emulsifying agent, after stirring and evenly mixing, obtain the first mixed liquor.
In step 101; in order to realize Jiang limonene emulsification fully and the effect mixing fast, temperature when described mixing be 20-30 DEG C (in this temperature range, because APG HLB value is higher; within the scope of 20-30 DEG C; can bring into play its activity, its larger polar group is stretched to water, nonpolar hydrocarbon key gos deep into oil phase; reduce its interfacial tension; form layer protecting film, be surrounded completely to oil interior, form O/W emulsion.Conventional emulsification product need to be at the scope internal emulsification of 75 DEG C-85 DEG C, and this product emulsifying process is simple and easy, has reduced production cost in enhancing productivity); The rotating speed of described stirring is that 1500-2000 rev/min, time are 10-20 minute.
Step 102: the polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are joined in deionized water, stir, obtain the second mixed liquor;
Concrete, by a container that deionized water is housed in advance, then respectively polyaminopropyl biguanide, benzalkonium chloride, vitamin E, extract solution from aloe are added, after stirring and evenly mixing, obtain the second mixed liquor.
Step 103: described the second mixed liquor is joined in described the first mixed liquor, stir and evenly mix, and drip citric acid, the pH of the first mixed liquor that is mixed with the second mixed liquor is adjusted to 5.0-7.0, obtain wet tissue liquid;
In step 103, the rotating speed of described stirring is that 1000-1500 rev/min, time are 10-20 minute.
Step 104: described wet tissue liquid is spilt uniformly after dropping in wet tissue body and packed according to set weight ratio, obtain wet tissue.
Concrete, spilling in the process of dripping, the weight of wet tissue liquid be wet tissue body 2-3 doubly.In addition, the present invention also provide the dirt-removing power test, bactericidal effect test, the test of black-koji mould preservation challenge of the wet tissue that above-described embodiment provides, with the compatibility test of plastics product; Concrete, for further illustrating practical effect of the present invention, adopt several routine type testing cases to describe:
1, dirt-removing power test:
Test one: tested material is kitchen tile wall and marble countertop, has moderate greasy dirt, the wet tissue wiping kitchen tile wall and the marble countertop that provide with embodiment mono-.Wiping is complete, and kitchen tile wall and marble countertop are without greasy dirt, and operator feels skin nonirritant.
Test two: tested object is glass tea table, and household electrical appliance (refrigerator, television set) shell, has slight tea stain and dirt, the wet tissue wiping tested material surface providing with embodiment bis-.Wiping is complete, and tea stain and dirt are eliminated completely, and operator feels skin nonirritant.
Test three: tested material is bathroom tile wall and sanitary bath equipment, have soap scum, incrustation scale, human body dirt, the wet tissue wiping object providing with embodiment tri-, after wiping, shower wall and sanitary bath equipment dirt are removed substantially, and operator feels skin nonirritant.
2, bactericidal effect test:
The sample providing with embodiment mono-and three, is labeled as respectively: kitchen cleaning pasteurization towelette 1#, kitchen cleaning pasteurization towelette 2#.According to the standard of GB15979/2002 " disposable use amenities sanitary standard ", Escherichia coli, staphylococcus aureus, Pseudomonas aeruginosa, Klebsiella Pneumoniae are carried out to sterilization test through third party authority testing agency.Black-koji mould is carried out to preservation challenge test.Test result is as follows:
The bactericidal effect test of the wet tissue of table 1 various embodiments of the present invention to different strain
3, black-koji mould preservation challenge test:
The wet tissue of table 2 various embodiments of the present invention is to black-koji mould preservative challenge testing
4, with the compatibility test of plastics product:
In the middle of selecting one, nail has plastics (polymethyl methacrylate) test-strips of STAINLESS STEEL NAILS (formation tension force), and short time every day is immersed solution to be measured, the situation of observation test bar after certain hour.Evaluation grade is divided into: unchanged; Form crack; Obviously crack; Fracture.
The wet tissue of table 3 various embodiments of the present invention and the compatibility test of plastics product
| ? | 4 hours | 3 days | 7 days | 14 days |
| Embodiment mono- | Unchanged | Unchanged | Unchanged | Unchanged |
| Embodiment tri- | Unchanged | Unchanged | Unchanged | Unchanged |
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (10)
1. a wet tissue, is characterized in that, comprises that wet tissue body and spray drop on described wet tissue body and weight is described wet tissue body 2-3 wet tissue liquid doubly;
Wherein, according to percetage by weight meter, in described wet tissue liquid, its component Bao Kuo limonene 0.10%-1.0%, APG 0.60%-6.0%, polyaminopropyl biguanide 0.10%-0.30%, benzalkonium chloride 0.05%-0.10%, vitamin E 0.05%-0.3%, extract solution from aloe 0.10%-1.0%, citric acid 0.005%-0.15%, deionized water 91.45%-98.995%.
2. wet tissue according to claim 1, is characterized in that, Suo Shu limonene extracts and obtains from citrus fruit.
3. the preparation of wet tissue according to claim 1 and 2, is characterized in that, described APG extracts and obtains from corn or coconut oil.
4. the preparation of wet tissue according to claim 3, is characterized in that, described APG is octyl group/Plantacare 818.
5. wet tissue according to claim 4, is characterized in that, described wet tissue body is spunlace non-woven cloth.
6. a preparation method for wet tissue according to claim 1, is characterized in that, comprises the following steps:
(1), configuration wet tissue liquid;
(2), described wet tissue liquid is spilt uniformly after dropping in wet tissue body and packed according to set weight ratio, obtain wet tissue.
7. the preparation method of wet tissue according to claim 6, is characterized in that, in step (1), specifically comprises:
After limonene, APG mix according to set weight ratio, stir, obtain the first mixed liquor;
The polyaminopropyl biguanide of set weight proportion, benzalkonium chloride, vitamin E, extract solution from aloe are joined in deionized water, stir, obtain the second mixed liquor;
Described the second mixed liquor is joined in described the first mixed liquor, stir and evenly mix, and drip citric acid, the pH of the first mixed liquor that is mixed with the second mixed liquor is adjusted to 5.0-7.0, obtain wet tissue liquid.
8. the preparation method of wet tissue according to claim 7, is characterized in that, stirs after limonene, APG mix according to set weight ratio described, obtains in the step of the first mixed liquor:
Temperature when described mixing is 20-30 DEG C.
9. the preparation method of wet tissue according to claim 8, is characterized in that, stirs after limonene APG mixes according to set weight ratio described, obtains in the step of the first mixed liquor:
The rotating speed of described stirring is that 1500-2000 rev/min, time are 10-20 minute.
10. according to the preparation method of the wet tissue described in claim 6-9 any one, it is characterized in that, described, described the second mixed liquor is joined in described the first mixed liquor, stir and evenly mix, and drip citric acid, the pH of the first mixed liquor that is mixed with the second mixed liquor is adjusted to 5.0-7.0, obtains in the step of wet tissue liquid:
The rotating speed of described stirring is that 1000-1500 rev/min, time are 10-20 minute.
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Effective date of registration: 20191219 Address after: No. 88, Changda Avenue, high tech Industrial Development Zone, Maoming City, Guangdong Province Patentee after: MAOMING ZHANG TECHNOLOGY DEVELOPMENT CO.,LTD. Address before: Baoan District manhole Street Ho Shenzhen city 518125 Guangdong Province Second Industrial Zone building, third storey high slope Patentee before: SHENZHEN HUANSHENG HOUSEWARE Co.,Ltd. |
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Denomination of invention: Wet towel and its preparation method Effective date of registration: 20221213 Granted publication date: 20170609 Pledgee: China Construction Bank Corporation Maoming Branch Pledgor: MAOMING ZHANG TECHNOLOGY DEVELOPMENT CO.,LTD. Registration number: Y2022980027024 |