CN104173248B - Natural plant essential oil-containing disinfecting liquid soap, as well as preparation method and application thereof - Google Patents
Natural plant essential oil-containing disinfecting liquid soap, as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention relates to disinfecting liquid soap and a preparation method thereof, and particularly relates to natural plant essential oil-containing disinfecting liquid soap and a preparation method thereof. The disinfecting liquid soap is prepared from N-(4-chlorphenyl)-N'-(3,4-dichlorophenyl)urea (triclocarban), ethanol, litsea cubeba essential oil, sweet orange essential oil, PEG40 hydrogenated castor oil (CO-40), N-trimethylglycine (betaine), carbomer U20 (Carbopol Ultrez 20 polymer), triethanolamine and deionized water. Antimicrobial tests indicate that the disinfecting liquid soap has a relatively strong bacteriostatic effect, is applicable to medical mechanisms, hotels, food processing manufacture enterprises, dining and entertainment facilities and the like.
Description
Technical field
The present invention relates to a kind of type disinfecting liquid, especially a kind of type disinfecting liquid containing natural plant essential oils, especially
Suitable for medical institutions, hotel, food processing manufacturing enterprise, food and drink public place of entertainment etc..
Background technology
In human body, both hands are the most positions of harmful microorganism such as contact bacterium, virus.There are some researches show, people
Can adhere to much more than 150 plant bacterium, virus etc. on hand, including Escherichia coli, Candida albicans, staphylococcus aureus,
Pseudomonas aeruginosa, salmonella, tubercle bacillus, influenza virus, hepatitis viruse etc..Separately there are some researches show, up to more than 80% stomach
Intestines problem, disease of skin etc. are all have germ infection on hand.Duty is washed one's hands, then be effective pre- preventing germs infection and biography
A kind of mode broadcast；And select correct hand-washing article, then it is the whether effective key point of this mode.Particularly with medical matters work
For author, in the contact with patient, in links such as diagnosis and treatment, detection, nursing, the germ of the directly or indirectly property for causing is handled
Infection probability is much higher than general population, therefore selects suitable effectively handwashing disinfection articles for use most important.
Medium-sized hand cleanser only has the basic function of cleaning hand, and its bactericidal action is very limited, can only wash
Take away by the effect of flowing water 20%～30% bacterium during hand, and it is picture staphylococcus aureus, Candida albicans, green
The high pathogenic bacteria such as purulence bacillus then can not be killed.This is clearly inadequate for medical personnel, it is therefore necessary to which selection has
The professional disinfection hand cleanser of bactericidal effect.This kind of professional hand disinfection in the face of medical personnel that currently there are is sterilized
Cleaning products, the overwhelming majority is the leave antiseptic hand washing gel based on " alcohol+isopropanol+acetic acid chlorhexidine " composition.
Such product alcohol content is high, and skin degreasing can be made after skin alcohol exposure, reduces skin elasticity and gloss；And gas
Taste is big, and use feeling is not good；If even more being not suitable for using to the crowd of alcohol intolerance.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of type disinfecting liquid containing natural plant essential oils.Effect product sterilization is killed
Bacterium effect substantially, and has the effect for nursing hand skin concurrently, and safety and stability, smell is pleasant, is particularly suitable for medical personnel and uses.
Technical proposal that the invention solves the above-mentioned problems is：
A kind of disinfection hand cleanser containing natural plant essential oils, comprising N- (4- chlorphenyls)-N'- (3,4- dichlorophenyl) urea,
Ethanol, Betaine, the polymer of Carbopol Ultrez 20, triethanolamine and deionized water, it is characterized by also containing
Have：Litsea cubeba oil, sweet orange oil and Cremophor RH40.
Further a kind of disinfection hand cleanser containing natural plant essential oils, described thimerosal is aqueous solution, is contained
Following weight ratio ingredient：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.05%～0.1%
Ethanol：25%～35%
Litsea cubeba oil：0.01%～0.025%
Sweet orange oil：0.01%～0.025%
Cremophor RH40 (CO-40)：0.05%～0.1%
Betaine (i.e. glycine betaine)：0.2%～0.5%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.15%～0.3%
Triethanolamine：0.15%～0.3%
Deionized water：63.65%～74.38%
Further, the most preferred weight ratio ingredient of this programme is：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.05%～0.07%
Ethanol：30%～35%
Litsea cubeba oil：0.01%～0.02%
Sweet orange oil：0.01%～0.02%
Cremophor RH40 (CO-40)：0.06%～0.09%
Betaine (i.e. glycine betaine)：0.4%～0.5%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.15%～0.2%
Triethanolamine：0.15%～0.2%
Deionized water：63.9%～69.17%
The technical advantage of the present invention is as follows：
1. product is clear gel, and nontoxic, nonirritant, non-corrosiveness, alcohol content is substantially reduced than conventional products, nothing
Pungent alcohol smell；Without essence pigment, without the material being harmful to human body skin, belongs to green, safe and environment-friendly sterilizing article.
2. the triclocarban that adds in product is a kind of efficiently, wide spectrum, the antibacterial agent of safety, it possess it is lasting, safe,
Stable sterilized feature, has fabulous compatibility with skin, and to gram-positive bacteria, Gram-negative bacteria, fungi, yeast
Bacterium, virus all have efficient inhibitory or killing effect.
3. product has been especially added with two kinds of plant essential oil components, has natural disinfection active ingredient wherein in litsea cubeba oil
Citral, for fungi, gram-positive bacteria, Gram-negative bacteria etc. all have obvious antibacterial action；And natural lemon aldehyde
For liposoluble constituent, skin absorption is advantageous to；And sweet orange oil then have significant antioxidation, can bactericidal antiphlogistic,
And skin whitening can be played a part of.After both natural essential oils and triclocarban compatibility, can effectively strengthen the sterilization of product
Disinfective action, and natural lemon delicate fragrance is carried, using rear skin sense more preferably.
4. the glycine betaine being especially added with product is native amino acid derivative, with significant moistening effect, can be reduced
The chapped skin sense caused due to frequently washing one's hands, keeps moisture of skin.
5. this product does not contain preservative ingredient, because natural essential oil composition therein has had antiseptic and inhibiting bacteria function effect concurrently, can be with
Avoid using chemical preservative, more meet consumer and pursue the natural market demand for washing shield product.
6. this product is Non-water washing type gel, is adapted to the demand of difference occasion and crowd, is particularly suitable for medical personnel and uses,
It also is adapted for school, kindergarten, bakery and confectionery, bank and cashier, hotel etc..
Bacteriostatic experiment result shows：Type disinfecting liquid of the present invention is entirely appropriate to be particularly medical institutions for public place
Medical personnel use, either stability, and bactericidal effect is all fine；And using rear more chloride than other same types and acetic acid class
Skin sense is more preferably.
Specific embodiment
The preparation of disinfection hand cleanser of the embodiment 1 containing natural plant essential oils
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.05g is added to into the ethanol of 30g
In fully dissolve, be subsequently adding by the PEG40 hydrogenated castors of the litsea cubeba oil of 0.02g, the sweet orange oil of 0.01g and 0.09g
Oily (i.e. CO-40) through the mixed liquor that mixes, and fully mix A phases are standby.By the Betaine of 0.3g (i.e. beet
Alkali) it is added in the deionized water of 69.13g with the card ripple U20 (i.e. Carbopol Ultrez20 polymer) of 0.2g and is filled after heating
Divide dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, the triethanolamine of 0.2g is added after fully mixing, filled
Divide after mixing, that is, obtain the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban)：0.05%
Ethanol：30%
Litsea cubeba oil：0.02%
Sweet orange oil：0.01%
Cremophor RH40 (i.e. CO-40)：0.09%
Betaine (i.e. glycine betaine)：0.3%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.2%
Triethanolamine：0.2%
Deionized water：69.13%
The preparation of disinfection hand cleanser of the embodiment 2 containing natural plant essential oils
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.06g is added to into the ethanol of 35g
In fully dissolve, be subsequently adding by the PEG40 hydrogenated castors of the litsea cubeba oil of 0.01g, the sweet orange oil of 0.02g and 0.09g
Oily (i.e. CO-40) through the mixed liquor that mixes, and fully mix A phases are standby.By the Betaine of 0.5g (i.e. beet
Alkali) it is added in the deionized water of 63.82g after heating with the card ripple U20 (i.e. the polymer of Carbopol Ultrez 20) of 0.25g
Fully dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, three ethanol of 0.25g are added after fully mixing
Amine, after fully mixing, that is, obtains the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban)：0.06%
Ethanol：35%
Litsea cubeba oil：0.01%
Sweet orange oil：0.02%
Cremophor RH40 (i.e. CO-40)：0.09%
Betaine (i.e. glycine betaine)：0.5%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.25%
Triethanolamine：0.25%
Deionized water：63.82%
The preparation of disinfection hand cleanser of the embodiment 3 containing natural plant essential oils
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.05g is added to into the ethanol of 30g
In fully dissolve, be subsequently adding by the PEG40 hydrogenated castors of the litsea cubeba oil of 0.01g, the sweet orange oil of 0.01g and 0.06g
Oily (i.e. CO-40) through the mixed liquor that mixes, and fully mix A phases are standby.By the Betaine of 0.4g (i.e. beet
Alkali) it is added in the deionized water of 69.17g after heating with the card ripple U20 (i.e. the polymer of Carbopol Ultrez 20) of 0.15g
Fully dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, three ethanol of 0.15g are added after fully mixing
Amine, after fully mixing, that is, obtains the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.05%
Ethanol：30%
Litsea cubeba oil：0.01%
Sweet orange oil：0.01%
Cremophor RH40 (CO-40)：0.06%
Betaine (i.e. glycine betaine)：0.4%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.15%
Triethanolamine：0.15%
Deionized water：69.17%
The preparation of disinfection hand cleanser of the embodiment 4 containing natural plant essential oils
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.07g is added to into the ethanol of 35g
In fully dissolve, be subsequently adding by the PEG40 hydrogenated castors of the litsea cubeba oil of 0.02g, the sweet orange oil of 0.02g and 0.09g
Oily (i.e. CO-40) through the mixed liquor that mixes, and fully mix A phases are standby.By the Betaine of 0.5g (i.e. beet
Alkali) it is added in the deionized water of 63.9g with the card ripple U20 (i.e. Carbopol Ultrez20 polymer) of 0.2g and is filled after heating
Divide dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, the triethanolamine of 0.2g is added after fully mixing, filled
Divide after mixing, that is, obtain the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.07%
Ethanol：35%
Litsea cubeba oil：0.02%
Sweet orange oil：0.02%
Cremophor RH40 (i.e. CO-40)：0.09%
Betaine (i.e. glycine betaine)：0.5%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.2%
Triethanolamine：0.2%
Deionized water：63.9%
The preparation of disinfection hand cleanser of the embodiment 5 containing natural plant essential oils
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.05g is added to into the ethanol of 25g
In fully dissolve, be subsequently adding by the PEG40 hydrogenated castors of the litsea cubeba oil of 0.01g, the sweet orange oil of 0.01g and 0.05g
Oily (i.e. CO-40) through the mixed liquor that mixes, and fully mix A phases are standby.By the Betaine of 0.2g (i.e. beet
Alkali) it is added in the deionized water of 74.38g after heating with the card ripple U20 (i.e. the polymer of Carbopol Ultrez 20) of 0.15g
Fully dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, three ethanol of 0.15g are added after fully mixing
Amine, after fully mixing, that is, obtains the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.05%
Ethanol：25%
Litsea cubeba oil：0.01%
Sweet orange oil：0.01%
Cremophor RH40 (i.e. CO-40)：0.05%
Betaine (i.e. glycine betaine)：0.2%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.15%
Triethanolamine：0.15%
Deionized water：74.38%
The preparation of disinfection hand cleanser of the embodiment 6 containing natural plant essential oils
During N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (i.e. triclocarban) of 0.1g is added to into the ethanol of 35g
Fully dissolving, is subsequently adding by the Cremophor RH40 of the litsea cubeba oil of 0.025g, the sweet orange oil of 0.025g and 0.1g
(i.e. CO-40) through mixing mixed liquor, and fully mix A phases are standby.By the Betaine of 0.5g (i.e. beet
Alkali) it is added in the deionized water of 63.65g with the card ripple U20 (i.e. Carbopol Ultrez20 polymer) of 0.3g and is filled after heating
Divide dissolving cooling and standings, obtain B phases standby.During above-mentioned A is added to into B quite, the triethanolamine of 0.3g is added after fully mixing, filled
Divide after mixing, that is, obtain the finished product of 100g.
The disinfection hand cleanser of the present embodiment constitutes as follows knowable to the preparation method of the present embodiment disinfection hand cleanser：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea (also known as triclocarban)：0.1%
Ethanol：35%
Litsea cubeba oil：0.025%
Sweet orange oil：0.025%
Cremophor RH40 (CO-40)：0.1%
Betaine (i.e. glycine betaine)：0.5%
Card ripple U20 (i.e. the polymer of Carbopol Ultrez 20)：0.3%
Triethanolamine：0.3%
Deionized water：63.65%
The antibacterial action of disinfection hand cleanser of the embodiment 7 containing natural plant essential oils
1st, material
Test bacterial classification:Staphylococcus aureus ATCC 6538, ETEC 8099, Candida albicans ATCC
10231, pseudomonas aeruginosa ATCC 15442.
Neutralization agent prescription:Sodium thiosulfate 10g+ tweens (80) 20g+ lecithin 3.0g+PBS 1000mL.
Testing sample：The disinfection hand cleanser containing natural plant essential oils, the containing by the preparation of embodiment 2 prepared by embodiment 1
The disinfection hand cleanser of natural plant essential oils, by embodiment 3 prepare the disinfection hand cleanser containing natural plant essential oils, by embodiment 4
Prepare the disinfection hand cleanser containing natural plant essential oils, by embodiment 5 prepare the disinfection hand cleanser containing natural plant essential oils and
By the disinfection hand cleanser containing natural plant essential oils prepared by embodiment 6.
2nd, method
With reference to QB/T 2738-2012《The evaluation method of daily chemical products antibacterial bacteriostatic effect》Wherein 7.2 antimicrobial form daily use chemicals are produced
The bactericidal effect method of inspection (suspension quantitative method) of product
3rd, result
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 1 see the table below 1：
Table 1
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 2 see the table below 2：
Table 2
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 3 see the table below 3：
Table 3
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 4 see the table below 4：
Table 4
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 5 see the table below 5：
Table 5
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils prepared by embodiment 6 see the table below 6：
Table 6
4th, conclusion
The present invention by embodiment 1 prepare the disinfection hand cleanser containing natural plant essential oils, by embodiment 2 prepare containing natural
The disinfection hand cleanser of plants essential oil, the disinfection hand cleanser containing natural plant essential oils prepared by embodiment 3, prepare by embodiment 4
The disinfection hand cleanser containing natural plant essential oils, by embodiment 5 prepare the disinfection hand cleanser containing natural plant essential oils and by reality
The disinfection hand cleanser containing natural plant essential oils of the preparation of example 6 is applied to staphylococcus aureus, ETEC, Candida albicans
This 4 kinds of microorganisms have significant bactericidal action with pseudomonas aeruginosa, can be used for including that the sterilization needed for daily life is used
On the way.
Claims (9)
1. a kind of disinfection hand cleanser containing natural plant essential oils, by N- (4- chlorphenyls)-N'- (3,4- dichlorophenyl) urea, ethanol,
Betaine, the polymer of Carbopol Ultrez 20, triethanolamine and deionized water and litsea cubeba oil, sweet orange
Essential oil and Cremophor RH40 are constituted；The weight ratio of wherein said components is respectively：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.05%～0.1%；
Ethanol：25%～35%；
Litsea cubeba oil：0.01%～0.025%；
Sweet orange oil：0.01%～0.025%；
Cremophor RH40：0.05%～0.1%；
Betaine：0.2%～0.5%；
The polymer of Carbopol Ultrez 20：0.15%～0.3%；
Triethanolamine：0.15%～0.3%；
Deionized water：63.65%～74.38%.
2. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 1, it is characterized by containing following weight
The component of ratio：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.05%；
Ethanol：30%；
Litsea cubeba oil：0.02%；
Sweet orange oil：0.01%；
Cremophor RH40：0.09%；
Betaine：0.3%；
The polymer of Carbopol Ultrez 20：0.2%；
Triethanolamine：0.2%；
Deionized water：69.13%.
3. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 1, it is characterized by containing following weight
The component of ratio：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.06%；
Ethanol：35%；
Litsea cubeba oil：0.01%；
Sweet orange oil：0.02%；
Cremophor RH40：0.09%；
Betaine：0.5%；
The polymer of Carbopol Ultrez 20：0.25%；
Triethanolamine：0.25%；
Deionized water：63.82%.
4. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 1, it is characterized by containing following weight
The component of ratio：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.05%～0.07%；
Ethanol：30%～35%；
Litsea cubeba oil：0.01%～0.02%；
Sweet orange oil：0.01%～0.02%；
Cremophor RH40：0.06%～0.09%；
Betaine：0.4%～0.5%；
The polymer of Carbopol Ultrez 20：0.15%～0.2%；
Triethanolamine：0.15%～0.2%；
Deionized water：63.9%～69.17%.
5. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 4, it is characterized by containing following weight
The component of ratio：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.05%；
Ethanol：30%；
Litsea cubeba oil：0.01%；
Sweet orange oil：0.01%；
Cremophor RH40：0.06%；
Betaine：0.4%；
The polymer of Carbopol Ultrez 20：0.15%；
Triethanolamine：0.15%；
Deionized water：69.17%.
6. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 4, it is characterized by containing following weight
The component of ratio：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyls) urea：0.07%
Ethanol：35%
Litsea cubeba oil：0.02%
Sweet orange oil：0.02%
Cremophor RH40：0.09%
Betaine：0.5%
The polymer of Carbopol Ultrez 20：0.2%
Triethanolamine：0.2%
Deionized water：63.9%.
7. a kind of method of the disinfection hand cleanser containing natural plant essential oils prepared as described in claim 1-6 any one, its
Step is as follows：
N- (4- chlorphenyls)-N'- (3,4- dichlorophenyl) urea is added in ethanol and is fully dissolved, is subsequently adding by fruit of a cubeb litsea tree essence
Oil, sweet orange oil and Cremophor RH40 through the mixed liquor that mixes, and fully mix A phases are standby；N- trimethyls is sweet
Propylhomoserin is added in deionized water fully dissolving cooling and standings after heating with the polymer of Carbopol Ultrez 20, obtains B phases standby
With；During above-mentioned A is added to into B quite, triethanolamine is added after fully mixing, after fully mixing, that is, obtain finished product.
8. dissipation cause is being prepared or prepared to the disinfection hand cleanser containing natural plant essential oils described in claim 1-6 any one
Application in germ liquid.
9. application according to claim 8, it is characterized by pathogenic bacteria are：It is staphylococcus aureus, ETEC, white
Color candida albicans and pseudomonas aeruginosa.
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| CN104758211A (en) * | 2015-03-20 | 2015-07-08 | 宁海燕 | Essential oil component-containing liquid soap |
| CN104840410B (en) * | 2015-05-28 | 2018-03-09 | 福建农林大学 | A kind of disposable hand disinfection liquid and its preparation and application |
| CN107460054A (en) * | 2016-09-09 | 2017-12-12 | 安徽香杰香精科技有限公司 | A kind of mixing odor type the back of the hand nurses one's health essential oil |
| CN107412090A (en) * | 2017-04-26 | 2017-12-01 | 烟台新时代健康产业日化有限公司 | A kind of long-acting bacteriostatic composition and its preparation method and application |
| CN111265435A (en) * | 2020-03-24 | 2020-06-12 | 上海应用技术大学 | No-clean bacteriostatic hand sanitizer containing navel orange essential oil and preparation method thereof |
| FR3112473A1 (en) * | 2020-07-15 | 2022-01-21 | Societe D'exploitation De Produits Pour Les Industries Chimiques Seppic | Hydro-alcoholic composition for hand disinfection |
| CN117771328A (en) * | 2023-11-15 | 2024-03-29 | 纳奇科化妆品有限公司 | Antibacterial composition, wet tissue containing same and preparation method thereof |
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|---|---|---|---|---|
| JP2002501542A (en) * | 1997-06-04 | 2002-01-15 | ザ、プロクター、エンド、ギャンブル、カンパニー | Liquid antimicrobial cleansing composition providing residual effect against gram negative bacteria |
| US20020172656A1 (en) * | 2000-01-20 | 2002-11-21 | Biedermann Kimberly Ann | Cleansing compositions |
| CN101810555B (en) * | 2010-04-13 | 2011-07-27 | 陈振华 | Concentrated foam liquid soap |
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2014
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