CN104095793B - A kind of Herba Dendrobii cosmetic water and preparation method thereof - Google Patents
A kind of Herba Dendrobii cosmetic water and preparation method thereof Download PDFInfo
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- CN104095793B CN104095793B CN201410354520.2A CN201410354520A CN104095793B CN 104095793 B CN104095793 B CN 104095793B CN 201410354520 A CN201410354520 A CN 201410354520A CN 104095793 B CN104095793 B CN 104095793B
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- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The present invention relates to a kind of Herba Dendrobii cosmetic water and preparation method thereof.Currently there are no a kind of Herba Dendrobii cosmetic water that can retain effective ingredient in Herba Dendrobii and preparation method thereof.The Herba Dendrobii cosmetic water of the present invention includes the Herba Dendrobii extract after the filtration that parts by weight are 8.0～13.0 parts, containing polysaccharide, chlorophyll, vitamin and protein in the Herba Dendrobii extract after this filtration.The preparation method of Herba Dendrobii cosmetic water includes following operation successively: A pretreatment procedure；B low temperature superfine grinding operation: being placed in homogenizer by the Herba Dendrobii after water temperature 2～the water of 10 DEG C and cut-out, Herba Dendrobii is 1:6～1:8 with the weight ratio of water, startup homogenizer and control discharge fineness, below 200～300 μm, obtain Herba Dendrobii extract；C filter progress；D emulsification process.The present invention carries out low-temperature extraction with iron-sheet dendrobe fresh product for raw material, retains Herba Dendrobii effective ingredient as far as possible.
Description
Technical field
The present invention relates to a kind of cosmetic water and preparation method thereof, especially relate to a kind of Herba Dendrobii cosmetic water and preparation method thereof,
Belong to medicinal plants manufacture field.
Background technology
Herba Dendrobii is the fresh stem of orchid Herba Dendrobii (Dendrobium officinale Kimura et Migo),
Belong to national conservative plant, there is health preserving and the medical value of preciousness.Herba Dendrobii is gained the name because its epidermis is ferrum green, goes through
The most on the books for Chinese medicine ancient books and records, the classics such as comprehensive Shennong's Herbal, Compendium of Material Medica, " detailed outline is picked up any lost article from the road " and " not Lu "
The works discussion to Herba Dendrobii, its primary efficacy is reinforcing YIN-essence benefit essence, clearing away heat and promoting production of body fluid, can tonifying five ZANG-organs asthenia, thick the intestines and stomach, by force
Muscle reinforcing and bone strengthening, arresting convulsion of calming the nerves, make light of one's life by commiting suicide and prolong life.Taoism regimen classical works " Taoist Scriptures " by Herba Dendrobii, Herba Saussureae Involueratae, three liang
The Radix Ginseng of weight, the hundred vicennial Radixs Polygoni Multiflori, Fu desert (Poria and Herba Cistanches), remote mountains Ganoderma, seabed Margarita and the Cordyceps of cycle of sixty years
And it being referred to as China's nine big Herba mesonae chinensis, Herba Dendrobii ranks first.Herba Dendrobii nature and flavor: sweet, are slightly cold, and enter stomach, kidney channel；Property belong to
Clear and rich, clear in have benefit, invigorating middle warmer to have clearly.
The efficacy effect of Herba Dendrobii, successive dynasties well-known doctor is respectively arranged with discussion, specific as follows:
" explaining abstruseness of the canon of materia medica " cloud: " Herba Dendrobii, sweet energy pleases spleen, salty energy kidney tonifying, therefore many merits are dirty in water and soil two: but gas width delays, nothing
The merit that victory is played, ancients are with this generation tea, on very clear diaphragm.”
Supplementary Amplifications of the Compendium of Materia Medica cloud: " Herba Dendrobii clearing stomach except deficiency-heat, promote the production of body fluid and strain, with for tea, merit is with joining stilbene.”
Herba Dendrobii described in " property of medicine " " for tea, promote the production of body fluid and wet one's whistle, reinforcing YIN-essence strong foot power by summer." visible, Herba Dendrobii is as being of illnesses and fitness
High tonic long-standing.The traditional Chinese medical science is thought, Herba Dendrobii atrophic gastritis, tumor, diabetes, pharyngolaryngitis and in vain in
The disease treatments such as barrier can extensively be applied.Herba Dendrobii has multiple pharmacological effect, such as the immunocompetence of enhancing body, resists
Oxidation, defying age, reduce blood glucose, YIN nourishing and the production of body fluid promoting etc..The traditional Chinese medical science is thought, " YIN and YANG in a relative equilibrium, life activities being normally maintained." such as cloudy body fluid deficiency
Empty, it is impossible to contain sun, sun is floating without system, and equilibrium between yin and yang is destroyed, and the most all diseases are grown thickly.”
" Ling Shu Miraculous Pivot or Divine Axis Benshen's piece " is said: " the five internal organs main store essential substances person also, can not hinder, and wound is then fallen into enemy hands and the deficiency of YIN, the deficiency of YIN then depletion of QI, nothing
Gas is the most dead." Herba Dendrobii Yin-nourishing and body fluid promoting key medicine just, between old friend referred to as " help Herba mesonae chinensis ".
Shennong's Herbal: main damaging the spleen and stomach, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards, tonifying five ZANG-organs asthenia weakness and emaciation, the thick the intestines and stomach of reinforcing YIN-essence, for a long time clothes.
Compendium of Material Medica: reinforcing YIN-essence benefit essence.Clothes for a long time, thick the intestines and stomach, never sufficient in benefit, flat gastric qi, long muscle, by skin pathogenic heat
Miliaria gas, it is weak that foot knee joint aches cold numbness, determines intelligence and removes frightened, makes light of one's life by commiting suicide and prolong life.
" detailed outline is picked up any lost article from the road ": clearing stomach remove deficiency-heat, promote the production of body fluid the sixth of the twelve Earthly Branches strain, with for tea, appetite promoting and the spleen strengthening.Arresting convulsion treatment wind, energy town saliva expectorant,
Sweet virtue sending down the abnormal ascending QI.
" medicineization justice ": control lung qi prolonged deficiency, cough is more than.
" not Lu ": benefit essence is never sufficient in mending, flat gastric qi, long muscle, by skin pathogenic heat gas, foot knee joint pain weakness, strong sun, mends
The long-pending essence of kidney.
" Japan hanako materia medica ": controlling deficient bad weak strengthening bone and muscle, warming the kidney, Fructus Alpiniae Oxyphyllae, flat gastric qi, by exogenous pathogen.
" book on Chinese herbal medicine is the newest ": reason gastric qi, clearing stomach fire.Except excessive thirst, treatment kidney channel deficiency-heat, arresting convulsion of calming the nerves in the heart, solve night sweat, can dissipate
Summer-heat.
Herba Dendrobii also has external efficacy, and modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free ammonia
Base acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzyme, not only by oral suction
Receiving, Herba Dendrobii can also stop blooding, promote wound healing, can be used for outward repairing damaged skin.
Polysaccharide in A, Herba Dendrobii effect to skin.
Dendrobium officinale polysaccharide has antibacterial, anti-inflammatory effect, the function of enhancing Cell-mediated Immunity, and external can resist dust mite, thin
The infringement to skin such as bacterium；Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thus promotees
Enter wound healing, repair damaged skin tissue.Theory of Chinese medical science is thought, Herba Dendrobii cold nature, is YIN nourishing sage's product, and skin
Grow skin sore, acne, small pox etc. and mostly be caused by hyperactivity of fire caused by deficiency of YIN, therefore Herba Dendrobii can be used for above-mentioned skin problem.
Free amino acid in B, Herba Dendrobii effect to skin.
Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, Sage Extract, has and improve sensitive skin
Antiallergic ability, prevents the generation of wrinkle；Activate the activity of Skin Cell superoxide dismutase peroxide, dispel skin thin
The free radical that born of the same parents are superfluous, effective delay skin aging；The phagocytic function of activating macrophage, the strongest lymphoid toxin expelling,
Function of detoxification, effectively blocks the extraneous harmful substance infringement to skin；Improve resisting skin allergy ability, and to internal nuisance
Matter and aged cells decompose excretion.Can with bivalent metal ion generation chelatropic reaction in wheat bran, stop too much divalent metal from
Son crosslinks effect with the collagen protein in skin, maintains enough collagen fiber and elastic fiber, makes skin slip, thin
Greasy high resilience.
The major function of the vitamin A in C, Herba Dendrobii.
Vitamin A from the oxidative damage of different link antagonism radical pair cells, strengthens the oxidation resistance of health in vivo,
Alleviate the harm of free radical；Help to maintain skin emolliency and plentiful, improve the lock water function of skin；There is obvious anti-angle
The effect of matter, and energy delay skin aging, division and development at Skin Cell have regulation effect；Help acne
Carry out local to treat, and prevent pachylosis from chapping, chilblain and dandruff etc.；Contribute to strengthening metabolism, make skin protect
Hold younger state.
Vitamin C in D, Herba Dendrobii and vitamin E effect to skin.
Injection Vitamin B_6 effect in terms of beauty and skin care is the most very important.Because the Oxidation of human sebaceous is skin
Old and feeble one of the main reasons, and vitamin E has antioxidation, thus protect sebum and cell membrane protein and skin
Moisture in skin；It can also promote regeneration and the vigor of human body cell, postpones the ageing process of cell.Moreover it is possible to promote
The human body utilization to vitamin A；Synergism, the health of protection skin can be played with vitamin C, reduce occurrence of skin infections；
There is " moistening " to act on the collagen fiber in skin and elastic fibers, thus improve and safeguard the elasticity of skin；Skin can be promoted
Blood circulation in skin, makes skin obtain sufficient nutrition and moisture, to maintain the tender of skin and gloss；May also suppress color
Element speckle, the formation of senile plaque, reduce facial wrinkles and pure white skin, prevent and treat acne.
Also have now and be applied to the effective ingredient in Herba Dendrobii on skin record, if publication date is on 08 14th, 2013,
In the Chinese patent of Publication No. CN103239471A, disclosing a kind of skin moistening external preparation, this skin moistening external preparation is by effectively
Composition and medically acceptable adjuvant composition, described effective ingredient be molecular weight be the Dendrobium officinale polysaccharide of 85-90KDa,
With only the polysaccharide in Herba Dendrobii, the utilization rate of Herba Dendrobii is low, during additionally, extract polysaccharide from Herba Dendrobii,
Have employed decoction extract, supersound extraction and enzymolysis and extraction these three method at 50 DEG C, these extracting method are for Herba Dendrobii
The destruction of the effective ingredient such as vitamin, aminoacid, organized enzyme is the most serious.
The most generally using the method decocted to extract the effective ingredient in Herba Dendrobii, traditional decoction extracting method can cause ferrum
The destruction of the effective ingredient such as polysaccharide, vitamin, aminoacid, organized enzyme in skin Herba Dendrobii, polysaccharide in products obtained therefrom, vitamin,
Chlorophyll, free amino acid equal size are relatively low, greatly reduce the utilization rate of Herba Dendrobii.Currently there are no one can protect
Herba Dendrobii cosmetic water staying effective ingredient in Herba Dendrobii and preparation method thereof.
Summary of the invention
It is an object of the invention to overcome above-mentioned deficiency present in prior art, and provide one to retain iron sheet stone as far as possible
Dry measure used in former times effective ingredient, expands Herba Dendrobii application, gives full play to Herba Dendrobii cosmetic water and preparation thereof that Herba Dendrobii is worth
Method, this Herba Dendrobii cosmetic water and preparation method thereof carries out low-temperature extraction with iron-sheet dendrobe fresh product for raw material, saves conventional iron
The baking operation of skin Herba Dendrobii extract, effective ingredient is difficult to be destroyed, the polysaccharide in products obtained therefrom, vitamin, chlorophyll, free ammonia
Base acid equal size is high.
A kind of preparation method of Herba Dendrobii cosmetic water, its feature is: include following operation successively:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
Gathered before blooming Herba Dendrobii；
B sterilizes,
Fresh Herba Dendrobii after Xi Jinging is placed in boiling water sterilization 3～5min, takes out and is placed in water cooling；
C cutting,
By Herba Dendrobii cutting；
B low temperature superfine grinding operation,
Being placed in homogenizer by Herba Dendrobii after water temperature 2～the water of 10 DEG C and cut-out, Herba Dendrobii with the weight ratio of water is
1:6～1:8, startup homogenizer and control discharge fineness, below 200～300 μm, obtain Herba Dendrobii extract；
C filter progress,
Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration, the Herba Dendrobii extraction after this filtration
Containing polysaccharide, chlorophyll, vitamin and protein in liquid；
D emulsification process,
By the water of formula ratio, butanediol, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, nicotiamide, sweet
Dish alkali, hyaluronate sodium, glycyrrhizic acid dipotassium and allantoin add in ingredients pot, are heated to 80～85 DEG C, and stirring and dissolving is gone out
Some minutes of bacterium, obtains base material；It is cooled to 40～45 DEG C the most while stirring, the Herba Dendrobii after the filtration of formula ratio is extracted
Liquid, IPBC and dimethyloldimethylhydantoin add in base material, if continuing stirring and emulsifying
Dry minute, carry out emulsifying 5min with homogenizer, stop stirring, cooling, obtain Herba Dendrobii cosmetic water；
E fill operation,
Herba Dendrobii cosmetic water is carried out fill.
So that in the course of processing of the present invention whole Herba Dendrobii extract, in addition to instantaneously sterilising, all below 30 DEG C
Completing, even if in the course of processing of Herba Dendrobii cosmetic water, its temperature also controls, below 45 DEG C, to be sufficiently reserved iron sheet
Various effective ingredient in Herba Dendrobii.
As preferably, in a Herba Dendrobii ingredient requirement of A pretreatment procedure of the present invention, Herba Dendrobii raw material is 3 years
The Herba Dendrobii of trophophase.
As preferably, in the b sterilization of A pretreatment procedure of the present invention, 200L caldron adds 150L purified water,
Heated and boiled, Herba Dendrobii first rinses 3 times with tap water, then rinses 2 times by purified water, by stainless steel clamp by Herba Dendrobii
Put and boiling water " quenches " 3～5min, take out in rearmounted purified water and cool down.
As preferably, C filter progress of the present invention in turn includes the following steps:
A coarse filtration step,
Being soaked by 100 mesh nylon filtering cloths, be folded in 2 layers of funnel being laid in vacuum filtration, edge is placed in outside funnel,
Opening vacuum filtration machine, vacuum is more than 0.07MPa, then pours in funnel by Herba Dendrobii extract, the coarse filtration being filtrated to get
Liquid, clears up once when filtering residue thickness reaches 0.5～1cm；
B fine straining step,
Starting high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump
It is 150～250r/min, by feed pipe to coarse filtration liquid, the Herba Dendrobii extract after being filtered after centrifugal filtration, incited somebody to action
Herba Dendrobii extract after filter is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue is once.
As preferably, in D emulsification process of the present invention, sterilization time is 30 minutes, and the continuation stirring and emulsifying time is 20min.
As preferably, in E fill operation of the present invention, take the packaging material disinfected, with automatic filling machine, inspection is closed
The Herba Dendrobii cosmetic water of lattice carries out fill, and pouring process controls the loading amount of product, and overgauge is within 7.5%.
A kind of Herba Dendrobii cosmetic water, its feature is: the preparation method described in the employing of this Herba Dendrobii cosmetic water is prepared from.
The present invention compared with prior art, has the following advantages and effect: carry out low-temperature extraction with iron-sheet dendrobe fresh product for raw material,
The course of processing of whole Herba Dendrobii extract, in addition to instantaneously sterilising, all accomplished below at 30 DEG C, even if at iron sheet stone
The course of processing of dry measure used in former times cosmetic water, its temperature also controls below 45 DEG C, the various effective ingredient being sufficiently reserved in Herba Dendrobii,
Eliminating the baking operation of tradition Herba Dendrobii, effective ingredient is difficult to be destroyed.It is demonstrated experimentally that iron sheet stone in the employing present invention
In Herba Dendrobii extract obtained by the preparation method of dry measure used in former times cosmetic water, calculate after giving money as a gift according to Herba Dendrobii extract, polysaccharide
Content reaches 60% (being 1.5～2 times of traditional decoction extraction process), and it (is tradition that Vitamin C content reaches 50mg/100g
Decoct 20 times of extraction process), chlorophyll content reaches 60mg/100g, and (and traditional decoction extraction process almost makes chlorophyll become
Point all destroy), and protein content also reaches 8.9% (about 1.2～1.5 times of traditional decoction extraction process), and extraction
Acquirement rate also exceeds more than 1.5 times than traditional handicraft, and extraction process advantage the most of the present invention is clearly, useful
Effect highly significant.The compositions such as polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii can be inhaled by human body by skin
Receiving, can be that skin provides very abundant nutrition, have document to report, Herba Dendrobii has hemostasis and promotes effect of wound healing,
External can repair damaged skin, and the present invention has expanded the application of Herba Dendrobii, has boundless market prospect.
In the present invention, the preparation method of Herba Dendrobii cosmetic water remains the effective ingredient of Herba Dendrobii as far as possible, with iron sheet stone
Dry measure used in former times fresh goods is that raw material carries out low-temperature extraction, saves the baking operation of tradition Herba Dendrobii, and effective ingredient is difficult to be destroyed, gained
Polysaccharide, vitamin, chlorophyll, free amino acid equal size height in product；Use low-temperature extraction technology, Herba Dendrobii is many
Sugar, dendrobine, aminoacid at utmost extract, simultaneously protection Herba Dendrobii Determination of Chlorophyll, vitamin and organized enzyme
Deng composition from high temperature.
Owing to current Herba Dendrobii product is many to take orally, Herba Dendrobii expanded by the Herba Dendrobii cosmetic water in the present invention
Application, substantially more plays it and is worth.
Accompanying drawing explanation
Fig. 1 is the schematic flow sheet of the preparation method of Herba Dendrobii cosmetic water in the embodiment of the present invention.
Fig. 2 is the schematic flow sheet of Herba Dendrobii extract preparation technology in the embodiment of the present invention.
Detailed description of the invention
The present invention is described in further detail below in conjunction with the accompanying drawings and by embodiment, and following example are to the present invention
Explain and the invention is not limited in following example.
Embodiment.
See Fig. 1 to Fig. 2,
Table one Herba Dendrobii extraction process and major parameter
Finally determine preparation technology and the parameter of Herba Dendrobii cosmetic water.
The preparation method of the Herba Dendrobii cosmetic water in the present embodiment includes following operation successively.
(1) pre-treatment.
1, Herba Dendrobii ingredient requirement.
Select the Herba Dendrobii of 3 years trophophases, and gathered time (April～June) before blooming.The experiment proved that, the florescence
Growth of Dendrobium candidum the most vigorous period before, Dendrobium officinale polysaccharide, vitamin, free amino acid, chlorophyll and other
Active enzyme content is the highest in the whole year, and its epidermis and stem are all green in ferrum, and fiber content is low, is beneficial to improve product extraction
Yield.
2, sterilization.
In 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii tap water is rinsed 3 times, then uses
Purified water is rinsed 2 times, grips appropriate Herba Dendrobii with rustless steel and puts boiling water and " quench " 3～5min, takes out to put in purified water and cools down.
3, cutting.
Taking the Herba Dendrobii that sterilization is complete, carry out cutting with medicine cutter, it is 150～180 times/min that cutting speed controls, every segment length
Controlling 0.5～1.5cm, the Herba Dendrobii section the cut stainless steel cask sterilized is collected, standby.
(2) low temperature superfine grinding technique and parameter.
First homogenizer all parts is carried out, and is the ethanol disinfection of 75% by percent by volume, treat that ethanol volatilizes, peace
Install standby, adjust the gap of stator and rotor, be allowed to 0.3～0.5mm, open cooling water valve.Take appropriate cryogenic purincation
Water (water temperature 2～10 DEG C), weighs, pours in homogenizer hopper, make purified water liquid level between 1/3～2/3 of hopper.Again
Taking the Herba Dendrobii of the most above-mentioned section of cutting, weigh, making Herba Dendrobii is 1:6～1:8 with the ratio of purified water.By outlet valve
Door be adjusted to " circulation ", start homogenizing button, monitoring discharge fineness, make size controlling below 200～300 μm, iron sheet stone
In dry measure used in former times superfine grinding liquid, turning barrel is collected, standby.
(3) filtering technique and parameter.
1, coarse filtration.
Being soaked by 100 mesh nylon filtering cloths, be folded in 2 layers of funnel being laid in vacuum filtration, edge is placed in outside funnel,
Open vacuum filtration machine, it is ensured that vacuum is more than 0.07MPa, then pours in funnel by Herba Dendrobii superfine grinding liquid, filter extremely
In liquid medicine storage tank, filtering residue thickness reaches cleaning when 0.5～1cm and once, collects filtering residue otherwise utilized.
2, fine straining.
Start high speed tube centrifuge (rotating speed 15000r/min) and peristaltic pump, set the rotating speed of peristaltic pump as 150～
250r/min, by feed pipe to coarse filtration liquid, starts centrifugal filtration to liquid medicine storage tank.Every centrifugal filtration 200～300L is clear
Reason filtering residue once, collect filtering residue, with on merge, otherwise utilized.The filtrate obtained after fine straining is the iron sheet stone after filtering
Dry measure used in former times extract.
(4) emulsifying process and parameter.
By deionized water, butanediol, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, nicotiamide, Radix Betae
The raw materials such as alkali, hyaluronate sodium, glycyrrhizic acid dipotassium and allantoin add in ingredients pot, are heated to 80～85 DEG C, stirring and dissolving,
Sterilizing 30 minutes；When being the most slowly cooled to 40～45 DEG C, the Herba Dendrobii extract after filtering, iodo third
Alkynyl butyl carbamate and dimethyloldimethylhydantoin add in base material, continue stirring and emulsifying 20min, use homogenizing
Machine carries out emulsifying 5min, and discharging is treated in stopping stirring, cooling, then censorship.
The course of processing of whole Herba Dendrobii extract, in addition to instantaneously sterilising, all accomplished below at 30 DEG C, even if at ferrum
The course of processing of skin Herba Dendrobii cosmetic water, its temperature also controls below 45 DEG C, be sufficiently reserved in Herba Dendrobii various effectively
Composition.
(5) fill.
Take the packaging material disinfected, with automatic filling machine to checking qualified Herba Dendrobii cosmetic water to carry out fill, fill
The loading amount of process control product, overgauge is within 7.5%.
Owing to current Herba Dendrobii product is many to take orally, Herba Dendrobii expanded by the Herba Dendrobii cosmetic water in the present invention
Application, substantially more plays it and is worth.
Embodiment 2.
Herba Dendrobii extract after filtration is adopted and is prepared with the following method: the fresh Herba Dendrobii after cleaning is placed in boiling water
Sterilization 3～5min, takes out and is placed in water cooling, then cut off, by the iron sheet after water temperature 2～the water of 10 DEG C and cut-out
Herba Dendrobii is placed in homogenizer, and Herba Dendrobii is 1:6～1:8 with the weight ratio of water, starts homogenizer and control discharge fineness exists
Below 200～300 μm, obtain Herba Dendrobii extract, Herba Dendrobii extract is filtrated to get the iron sheet stone after filtration
Dry measure used in former times extract.
In the present embodiment, the preparation method of Herba Dendrobii cosmetic water includes following operation successively:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
Gathering before blooming Herba Dendrobii, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
B sterilizes,
Adding 150L purified water, heated and boiled in 200L caldron, Herba Dendrobii first rinses 3 times with tap water, then uses
Purified water is rinsed 2 times, is put by Herba Dendrobii by stainless steel clamp and " quenches " 3～5min in boiling water, takes out in rearmounted purified water and cool down.
C cutting,
By Herba Dendrobii cutting.
B low temperature superfine grinding operation,
Being placed in homogenizer by Herba Dendrobii after water temperature 2～the water of 10 DEG C and cut-out, Herba Dendrobii with the weight ratio of water is
1:6～1:8, such as Herba Dendrobii can be 1:6,1:6.5,1:7,1:7.5,1:8,1:6.3,1:6.8 with the weight ratio of water,
1:7.2,1:7.7 etc., startup homogenizer and control discharge fineness, below 200～300 μm, obtain Herba Dendrobii extract.
C filter progress,
A coarse filtration step,
Being soaked by 100 mesh nylon filtering cloths, be folded in 2 layers of funnel being laid in vacuum filtration, edge is placed in outside funnel,
Opening vacuum filtration machine, vacuum is more than 0.07MPa, then pours in funnel by Herba Dendrobii extract, the coarse filtration being filtrated to get
Liquid, clears up once when filtering residue thickness reaches 0.5～1cm.
B fine straining step,
Starting high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump
It is 150～250r/min, by feed pipe to coarse filtration liquid, the Herba Dendrobii extract after being filtered after centrifugal filtration, this mistake
Containing polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract after filter.Herba Dendrobii after being filtered
Extract is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue is once.
D emulsification process,
By the water of formula ratio, butanediol, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, nicotiamide, sweet
Dish alkali, hyaluronate sodium, glycyrrhizic acid dipotassium and allantoin add in ingredients pot, are heated to 80～85 DEG C, and stirring and dissolving is gone out
Some minutes of bacterium, sterilization time is preferably 30 minutes, obtains base material；It is cooled to 40～45 DEG C the most while stirring, by formula ratio
Filtration after Herba Dendrobii extract, IPBC and dimethyloldimethylhydantoin add
In base material, continuing stirring and emulsifying some minutes, the continuation stirring and emulsifying time is preferably 20min, carries out emulsifying with homogenizer
5min, stops stirring, cooling, obtains Herba Dendrobii cosmetic water.
E fill operation,
Take the packaging material disinfected, with automatic filling machine to checking qualified Herba Dendrobii cosmetic water to carry out fill, fill
The loading amount of process control product, overgauge is within 7.5%.
The invention still further relates to a kind of Herba Dendrobii cosmetic water prepared by above-mentioned preparation method, use above-mentioned preparation method to prepare
Herba Dendrobii cosmetic water is used directly on skin, and the polysaccharide in Herba Dendrobii, chlorophyll, vitamin become with protein etc.
Divide and can be absorbed by the body by skin, can be that skin provides very abundant nutrition, expand the application of Herba Dendrobii,
Substantially more play it to be worth.
The course of processing of whole Herba Dendrobii extract in the present embodiment, in addition to instantaneously sterilising, all accomplished below at 30 DEG C,
Even if in the course of processing of Herba Dendrobii cosmetic water, its temperature also controls, below 45 DEG C, to be sufficiently reserved in Herba Dendrobii
Various effective ingredient.The preparation method of this Herba Dendrobii cosmetic water remains the effective ingredient of Herba Dendrobii as far as possible, with
Iron-sheet dendrobe fresh product is that raw material carries out low-temperature extraction, saves the baking operation of tradition Herba Dendrobii, and effective ingredient is difficult to be destroyed,
Polysaccharide, vitamin, chlorophyll, free amino acid equal size height in products obtained therefrom；Use low-temperature extraction technology, by iron sheet stone
Dry measure used in former times polysaccharide, dendrobine, aminoacid at utmost extract, simultaneously protection Herba Dendrobii Determination of Chlorophyll, vitamin and work
The compositions such as property enzyme are from high temperature.
Although the present invention is open the most as above with embodiment, but it is not limited to protection scope of the present invention, and any be familiar with should
The technical staff of item technology, in the change made without departing from the spirit and scope of the invention and retouching, all should belong to the present invention
Protection domain.
Claims (7)
1. the preparation method of a Herba Dendrobii cosmetic water, it is characterised in that: include following operation successively:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
Gathered before blooming Herba Dendrobii；
B sterilizes,
Fresh Herba Dendrobii after Xi Jinging is placed in boiling water sterilization 3～5min, takes out and is placed in water cooling；
C cutting,
By Herba Dendrobii cutting；
B low temperature superfine grinding operation,
Being placed in homogenizer by Herba Dendrobii after water temperature 2～the water of 10 DEG C and cut-out, Herba Dendrobii with the weight ratio of water is
1:6～1:8, startup homogenizer and control discharge fineness, in 200～300 μm, obtain Herba Dendrobii extract；
C filter progress,
Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration, the Herba Dendrobii extraction after this filtration
Containing polysaccharide, chlorophyll, vitamin and protein in liquid；
D emulsification process,
By the water of formula ratio, butanediol, Hamamelis virginiana extract, nicotiamide, glycine betaine, hyaluronate sodium, glycyrrhizic acid
Dipotassium and allantoin add in ingredients pot, are heated to 80～85 DEG C, stirring and dissolving, and some minutes of sterilizing obtains base material；Then
It is cooled to 40～45 DEG C while stirring, by the Herba Dendrobii extract after the filtration of formula ratio, iodo propinyl butylamino first
Acid esters and dimethyloldimethylhydantoin add in base material, continue stirring and emulsifying some minutes, carry out homogenizing with homogenizer
Emulsifying 5min, stops stirring, cooling, obtains Herba Dendrobii cosmetic water；
E fill operation,
Herba Dendrobii cosmetic water is carried out fill.
The preparation method of Herba Dendrobii cosmetic water the most according to claim 1, it is characterised in that: described A pre-treatment work
In a Herba Dendrobii ingredient requirement of sequence, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
The preparation method of Herba Dendrobii cosmetic water the most according to claim 1, it is characterised in that: described A pre-treatment work
In the b sterilization of sequence, adding 150L purified water, heated and boiled in 200L caldron, Herba Dendrobii first rinses 3 with tap water
Time, then rinse 2 times by purified water, by stainless steel clamp Herba Dendrobii put and boiling water " quenches " 3～5min, take out rearmounted purification
Water cools down.
The preparation method of Herba Dendrobii cosmetic water the most according to claim 1, it is characterised in that: described C filter progress
In turn include the following steps:
A coarse filtration step,
Being soaked by 100 mesh nylon filtering cloths, be folded in 2 layers of funnel being laid in vacuum filtration, edge is placed in outside funnel,
Opening vacuum filtration machine, vacuum is more than 0.07MPa, then pours in funnel by Herba Dendrobii extract, the coarse filtration being filtrated to get
Liquid, clears up once when filtering residue thickness reaches 0.5～1cm；
B fine straining step,
Starting high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump
It is 150～250r/min, feed pipe is placed in coarse filtration liquid, the Herba Dendrobii extract after being filtered after centrifugal filtration, will
Herba Dendrobii extract after filtration is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue is once.
The preparation method of Herba Dendrobii cosmetic water the most according to claim 1, it is characterised in that: described D emulsification process
In, sterilization time is 30 minutes, and the continuation stirring and emulsifying time is 20min.
The preparation method of Herba Dendrobii cosmetic water the most according to claim 1, it is characterised in that: described E fill operation
In, take the packaging material disinfected, with automatic filling machine to checking qualified Herba Dendrobii cosmetic water to carry out fill, fill
The loading amount of process control product, overgauge is within 7.5%.
7. a Herba Dendrobii cosmetic water, it is characterised in that: this Herba Dendrobii cosmetic water uses power as arbitrary in claim 1-6
Preparation method described in profit requirement is prepared from.
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| CN104546594A (en) * | 2014-12-11 | 2015-04-29 | 罗生芳 | Moisturizing toner and preparation method thereof |
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| CN106109288A (en) * | 2016-06-30 | 2016-11-16 | 广西健宝石斛有限责任公司 | A kind of Herba Dendrobii cosmetic water and preparation method thereof |
| CN106137909A (en) * | 2016-07-25 | 2016-11-23 | 谭志华 | A kind of Herba Dendrobii cosmetic water |
| CN107510637A (en) * | 2016-11-17 | 2017-12-26 | 广西九大仙草生物科技有限公司 | A kind of edible dendrobium candidum shin moisturizer and preparation method thereof |
| CN106389305A (en) * | 2016-11-25 | 2017-02-15 | 上海娇云日化有限公司 | Moisturizing cream |
| CN108938528A (en) * | 2018-10-08 | 2018-12-07 | 江苏农林职业技术学院 | A kind of fresh tea leaves essential oil toner and preparation method thereof |
| CN109793691A (en) * | 2019-02-27 | 2019-05-24 | 苏州天成新农生物科技有限公司 | Filter method suitable for dendrobium candidum tender shoots stoste |
| CN109793692A (en) * | 2019-02-27 | 2019-05-24 | 苏州天成新农生物科技有限公司 | Filter method suitable for the dry bud stoste of dendrobium candidum |
| CN116159009A (en) * | 2023-03-17 | 2023-05-26 | 北京迷奇生物科技有限公司 | Peony petal toner and preparation method thereof |
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| KR101081059B1 (en) * | 2009-06-30 | 2011-11-07 | 한국콜마 주식회사 | Flowers Extract Having Anti-oxidation And Whitening Effects And Extraction Method Thereof And Cosmetics Comprising Flowers Extract |
| CN102274138A (en) * | 2010-06-11 | 2011-12-14 | 上海家化联合股份有限公司 | Dendrobe extract and preparation method and application thereof |
| CN103156795A (en) * | 2011-12-13 | 2013-06-19 | 杨明志 | Technology for processing beauty skin care product by using dendrobe |
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