CN105997690A - Dendrobium officinale facial cleanser and preparation method thereof - Google Patents

Dendrobium officinale facial cleanser and preparation method thereof Download PDF

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Publication number
CN105997690A
CN105997690A CN201610501710.1A CN201610501710A CN105997690A CN 105997690 A CN105997690 A CN 105997690A CN 201610501710 A CN201610501710 A CN 201610501710A CN 105997690 A CN105997690 A CN 105997690A
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herba dendrobii
dendrobium officinale
extract
herba
preparation
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何忠海
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Guangxi Strong Gem Dry Measure Used In Former Times Co Ltd
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Guangxi Strong Gem Dry Measure Used In Former Times Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a dendrobium officinale facial cleanser and a preparation method thereof. The preparation method can keep effective ingredients in dendrobium officinale. The dendrobium officinale facial cleanser comprises 5-9 parts by weight of dendrobium officinale extract. The preparation method of the dendrobium officinale extract comprises the following steps: (1) cleaning and sterilizing pretreatment; (2) soaking: putting the dendrobium officinale and a wax coat-removed microbial strain in deionized water, stirring the dendrobium officinale and the wax coat-removed microbial strain, and soaking the mixture for 10-30 days; (3) filtering; (4) decolorizing: adding active carbon for decolorizing the dendrobium officinale filtrate, and carrying out filtering to obtain a dendrobium officinale extracting solution; (5) grinding: grinding the dendrobium officinale extracting solution and the baked dendrobium officinale through a homogenizer to obtain dendrobium officinale extract; and (6) filtering: carrying out filtering to obtain the filtered dendrobium officinale extract. According to the invention, the dendrobium officinale is taken as a raw material for decolorizing, and low-temperature extraction is carried out, so that the problem that the drug effect is influenced due to the dark color of traditional Chinese medicines is avoided, and the effective ingredients of the dendrobium officinale are well kept.

Description

A kind of Herba Dendrobii cleansing milk and preparation method thereof
Technical field
The present invention relates to a kind of cleansing milk and preparation method thereof, belong to medicinal plants manufacture field, particularly relate to a kind of ferrum Skin Herba Dendrobii cleansing milk and preparation method thereof.
Background technology
Herba Dendrobii is the new of orchid Herba Dendrobii (Dendrobium officinale Kimura et Migo) Fresh stem, belongs to national conservative plant, has health preserving and the medical value of preciousness.Herba Dendrobii obtains because its epidermis is ferrum green Name, successive dynasties Chinese medicine ancient books and records are the most on the books, the classics such as comprehensive Shennong's Herbal, Compendium of Material Medica, " detailed outline is picked up any lost article from the road " and " not Lu " The works discussion to Herba Dendrobii, its primary efficacy is reinforcing YIN-essence benefit essence, clearing away heat and promoting production of body fluid, can tonifying five ZANG-organs asthenia, thick the intestines and stomach, strong muscle Bone, arresting convulsion of calming the nerves, make light of one's life by commiting suicide and prolong life.Taoism regimen classical works " Taoist Scriptures " by Herba Dendrobii, Herba Saussureae Involueratae, three double Radix Ginsengs, The hundred vicennial Radixs Polygoni Multiflori, Fu desert (Poria and Herba Cistanches), remote mountains Ganoderma, seabed Margarita and the Cordyceps of cycle of sixty years are also referred to as China nine Big Herba mesonae chinensis, Herba Dendrobii ranks first.Herba Dendrobii nature and flavor: sweet, are slightly cold, and enter stomach, kidney channel;Property belong to clear and rich, clear in have benefit, invigorating middle warmer Have clear.
Herba Dendrobii also has external efficacy, and modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free Aminoacid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various mould, not only by oral absorption, Herba Dendrobii can also stop blooding, promote wound healing, can be used for outward repairing damaged skin.
Dendrobium officinale polysaccharide has antibacterial, anti-inflammatory effect, the function of enhancing Cell-mediated Immunity, external can resist dirt hide from, The infringement to skin such as antibacterial;Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thus promotees Enter wound healing, repair damaged skin tissue.Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, equilibrium oil Fat, has the antiallergic ability improving sensitive skin, prevents the generation of wrinkle;Activate Skin Cell superoxide dismutase peroxidating The activity of thing, dispels the free radical that Skin Cell is superfluous, effective delay skin aging;The phagocytic function of activating macrophage, increases Strong lymphoid toxin expelling, function of detoxification, effectively block the extraneous harmful substance infringement to skin;Improve resisting skin allergy energy Power, and internal harmful substance and aged cells are decomposed excretion etc..
Also have now and be applied to the effective ingredient in Herba Dendrobii on skin record, if open mouth is 2013 08 month 14 Mouthful, in the Chinese patent of Publication No. CN103239471A, disclosing a kind of skin moistening external preparation, this skin moistening external preparation is by having Effect composition and medically acceptable adjuvant composition, described effective ingredient be molecular weight be that the Herba Dendrobii of 85-90KDa is many Sugar, with only the polysaccharide in Herba Dendrobii, and the utilization rate of Herba Dendrobii is low, during additionally, extract polysaccharide from Herba Dendrobii, Have employed decoction extract, supersound extraction and enzymolysis and extraction these three method at 50 DEG C, these extracting method are for Herba Dendrobii The destruction of the effective ingredient such as vitamin, aminoacid, organized enzyme is the most serious.
The most generally using the method decocted to extract the effective ingredient in Herba Dendrobii, traditional decoction extracting method can be led Causing the destruction of the effective ingredient such as polysaccharide, vitamin, aminoacid, organized enzyme in Herba Dendrobii, polysaccharide, dimension in products obtained therefrom are raw Element, chlorophyll, free amino acid equal size are relatively low, greatly reduce the utilization rate of Herba Dendrobii.Currently there are no one can Retain Herba Dendrobii cleansing milk of effective ingredient and preparation method thereof in Herba Dendrobii.
First Herba Dendrobii is clayed into power it addition, also have, the preparation method being then added in the substrate of skin care item, this Although method can retain the effective ingredient of Herba Dendrobii, but owing to Herba Dendrobii Chinese medicine color is deep, for not affecting skin care item Outward appearance, manufacturer the most only adds the most a small amount of Herba Dendrobii, causes the skin-care effect of Herba Dendrobii to be had a greatly reduced quality.
Summary of the invention
For solving above-mentioned technical problem, the technical solution used in the present invention is:
A kind of Herba Dendrobii cleansing milk, including the following raw material counted by weight: Herba Dendrobii extract 5-9 part, Herba Cymbopogonis Citrari Extract 12-25 part, Fructus Cucumidis sativi extract 5-10 part, preservative 0. 5-1.0 part, surfactant 12-20 part, palm fibre put acid 6-10 Part, propylene glycol 4-10 part, wetting agent 1-12, glycerol 5-8 part, Margarita powder 5-8 part, deionized water 30-50 part, emulsifying agent 5-10 Part.
Preferably technical scheme is: Herba Dendrobii extract preparation method comprises the following steps:
(1) pretreatment: root and the stipes of fresh Herba Dendrobii are cleaned sterilization processing;
(2) soak: the Herba Dendrobii of sterilization is put in deionized water, and add the microorganism fungus kind sloughing wax coat, stirring Uniformly, soak 10~30 days, in the pigmentolysis of Herba Dendrobii to water;
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and filtrate;
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii filtrate;
(5) grinding step: the Herba Dendrobii after temperature 2~the Herba Dendrobii extracting solution of 10 DEG C and filtration is placed in homogenizer, Herba Dendrobii is 1:4~1:9 with the weight ratio of Herba Dendrobii extracting solution, starts homogenizer and controls discharge fineness 200~300 Below m, obtains Herba Dendrobii extract;
(6) filter progress: thick Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration.
Preferably technical scheme is: above-mentioned Herba Dendrobii cleansing milk, described in slough the microorganism fungus kind of wax coat be hydrocarbon oxygen Change bacterium be pseudomonas (Pseudomonas), acinetobacter calcoaceticus (Acinetobacter), sporeformer (Bacillus), bud pole Bacterium (Geobacillus), vibrio (Vibrionaceae), micrococcus luteus (Micrococcus) or arthrobacterium (Arthrobacter) Deng.
In patent of the present invention, further, the microorganism fungus kind quality sloughing wax coat described in accounts for Herba Dendrobii quality 0.05~0.5%.
In patent of the present invention, further, quality of activated carbon accounts for the 1~3% of Herba Dendrobii filtrate quality.
In patent of the present invention, further, in described step (6), filtration includes coarse filtration step and fine straining step;Described slightly Filter uses 100 mesh nylon filtering cloths to soak filtration;Described fine straining step uses high speed tube centrifuge, and rotating speed is 15000r/min.
A kind of Herba Dendrobii cleansing milk preparation method, including following preparation process:
Step one, by Herba Cymbopogonis Citrari extract, Fructus Cucumidis sativi extract and Herba Dendrobii extract, weighs required number mix and blend equal Even, obtain nutritional solution after sterilization, and preservation is standby at 15-25 DEG C;
Step 2, takes nutritional solution, and adds Margarita powder, after homogenizing processes 10-15 minute, adds emulsifying agent, wetting agent, anticorrosion Agent and water, be stirred and heated to 50-65 DEG C, and after being incubated 10-15 minute, 20-25 DEG C to be naturally cooled to obtains semi-finished product;
Step 3, takes glycerol, surfactant, palm fibre put acid, propylene glycol adds in semi-finished product, subpackage after stir 10-15 minute, must Herba Dendrobii cleansing milk.
In sum, owing to have employed technique scheme, the invention has the beneficial effects as follows:
1, the present invention carries out immersion treatment to Herba Dendrobii, it is thus achieved that Herba Dendrobii filtrate and Herba Dendrobii, and merge grinding Processing, this preparation method remains the effective ingredient of Herba Dendrobii as far as possible, extracts for raw material with iron-sheet dendrobe fresh product, Effective ingredient is difficult to be destroyed, polysaccharide, vitamin, chlorophyll, free amino acid equal size height in products obtained therefrom;
2, the present invention uses hydrocarbon oxidation bacteria microorganism, decomposes the wax coat on Herba Dendrobii surface, makes Herba Dendrobii and water fully connect Touch, make effective ingredient rapid dispersion in Herba Dendrobii in water;
3, the present invention uses immersion technology, Herba Dendrobii pigment, polysaccharide, dendrobine, aminoacid is at utmost extracted, exempts from It is damaged;Use activated carbon that Herba Dendrobii filtrate is decoloured, it is to avoid Chinese medicine color is the deepest simultaneously, affect sending out of drug effect Wave, it is to avoid affect the using effect of cleansing milk;
4, the scientific formulation, rationally of Herba Dendrobii cleansing milk of the present invention, can produce cooperative effect, it is possible to more efficient between composition Given play to effect of polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract, and advantageously in skin absorption Polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract.
Detailed description of the invention
Being described in further detail the detailed description of the invention of the present invention below, following example are only used for clearly Technical scheme is described, and can not limit the scope of the invention.
A kind of Herba Dendrobii cleansing milk is including the following raw material counted by weight: Herba Dendrobii extract 5-9 part, fragrant Rhizoma Imperatae extract 12-25 part, Fructus Cucumidis sativi extract 5-10 part, preservative 0. 5-1. 0 part, surfactant 12-20 part, palm fibre put acid 6-10 part, propylene glycol 4-10 part, wetting agent 1-12, glycerol 5-8 part, Margarita powder 5-8 part, deionized water 30-50 part, emulsifying agent 5- 10 parts.
Herba Dendrobii cleansing milk is prepared into by following processing step:
(1) pretreatment: root and the stipes of fresh Herba Dendrobii are cleaned sterilization processing;
(2) soak: the Herba Dendrobii of sterilization is put in deionized water, and adds pseudomonas, stir, soak 10 days, Then ultrasonic wave concussion, in the pigmentolysis of Herba Dendrobii to water;
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate;
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii filtrate;
(5) grinding step: the Herba Dendrobii after the Herba Dendrobii extracting solution of temperature 2 DEG C and filtration is placed in homogenizer, iron sheet Herba Dendrobii is 1:4 with the weight ratio of Herba Dendrobii extracting solution, and startup homogenizer and control discharge fineness, at 200~300 below m, obtain To Herba Dendrobii extract;
(6) filter progress: soaked by l00 mesh nylon filtering cloth, is folded in 2 layers of funnel being laid in vacuum filtration, and edge is placed in Outside funnel, open vacuum filtration machine, then Herba Dendrobii superfine grinding liquid poured in funnel, filter to liquid medicine storage tank, Filtering residue thickness reaches cleaning when 0.5~lcm and once, collects filtering residue otherwise utilized;
Fine straining: start high speed tube centrifuge (rotating speed is 15000r/min) and peristaltic pump, set the rotating speed of peristaltic pump as 150~ 250r/min, by feed pipe to coarse filtration liquid, starts centrifugal filtration to new liquid medicine storage tank.Every centrifugal filtration 200~300L Cleaning filtering residue once, is collected by filtration filtering residue, merges with the filtering residue obtained in coarse filtration, otherwise utilized.The filter obtained after fine straining Liquid is the Herba Dendrobii extract after filtering;
(7) by Herba Cymbopogonis Citrari extract, Fructus Cucumidis sativi extract and Herba Dendrobii extract, required number mixing and stirring is weighed, Obtain nutritional solution after sterilization, and preservation is standby at 15-25 DEG C;
(8) taking nutritional solution, and add Margarita powder, homogenizing processed after 10-15 minute, add emulsifying agent, wetting agent, preservative and Water, is stirred and heated to 50-65 DEG C, and after being incubated 10-15 minute, 20-25 DEG C to be naturally cooled to obtains semi-finished product;
(9) take glycerol, surfactant, palm fibre puts acid, propylene glycol adds in semi-finished product, subpackage after stirring 10-15 minute, obtains iron sheet Herba Dendrobii cleansing milk.

Claims (7)

1. a Herba Dendrobii cleansing milk, it is characterised in that: include the following raw material counted by weight: Herba Dendrobii extract 5-9 part, Herba Cymbopogonis Citrari extract 12-25 part, Fructus Cucumidis sativi extract 5-10 part, preservative 0. 5-1. 0 part, surfactant 12-20 Part, palm fibre put acid 6-10 part, propylene glycol 4-10 part, wetting agent 1-12, glycerol 5-8 part, Margarita powder 5-8 part, deionized water 30-50 Part, emulsifying agent 5-10 part.
Herba Dendrobii cleansing milk the most according to claim 1, it is characterised in that: described Herba Dendrobii extract preparation method bag Include following steps:
(1) pretreatment: root and the stipes of fresh Herba Dendrobii are cleaned sterilization processing;
(2) soak: the Herba Dendrobii of sterilization is put in deionized water, and add the microorganism fungus kind sloughing wax coat, stirring Uniformly, soak 10~30 days, in the pigmentolysis of Herba Dendrobii to water;
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate;
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii filtrate;
(5) grinding step: the Herba Dendrobii after temperature 2~the Herba Dendrobii extracting solution of 10 DEG C and filtration is placed in homogenizer, Herba Dendrobii is 1:4~1:9 with the weight ratio of Herba Dendrobii extracting solution, starts homogenizer and controls discharge fineness 200~300 Below m, obtains Herba Dendrobii extract;
(6) filter progress: thick Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration.
Herba Dendrobii cleansing milk the most according to claim 2, it is characterised in that the microorganism fungus kind sloughing wax coat described in: is Hydrocarbon oxidation bacteria be pseudomonas, acinetobacter calcoaceticus, sporeformer, bud pole bacterium, vibrio, micrococcus luteus or arthrobacterium.
Herba Dendrobii cleansing milk the most according to claim 2, it is characterised in that slough the microorganism fungus kind matter of wax coat described in: Amount accounts for the 0.05~0.5% of Herba Dendrobii quality.
Herba Dendrobii cleansing milk the most according to claim 2, it is characterised in that: quality of activated carbon accounts for Herba Dendrobii filtrate quality 1~3%.
Herba Dendrobii cleansing milk the most according to claim 2, it is characterised in that: described step (6) filters and includes that coarse filtration walks Rapid and fine straining step;Described coarse filtration uses 100 mesh nylon filtering cloths to soak filtration;Described fine straining step uses high speed tubular type to be centrifuged Machine, rotating speed is 15000r/min.
7. a Herba Dendrobii cleansing milk preparation method, it is characterised in that: this preparation method comprises the steps:
Step one, by Herba Cymbopogonis Citrari extract, Fructus Cucumidis sativi extract and Herba Dendrobii extract, weighs required number mix and blend equal Even, obtain nutritional solution after sterilization, and preservation is standby at 15-25 DEG C;
Step 2, takes nutritional solution, and adds Margarita powder, after homogenizing processes 10-15 minute, adds emulsifying agent, wetting agent, anticorrosion Agent and water, be stirred and heated to 50-65 DEG C, and after being incubated 10-15 minute, 20-25 DEG C to be naturally cooled to obtains semi-finished product;
Step 3, takes glycerol, surfactant, palm fibre put acid, propylene glycol adds in semi-finished product, subpackage after stir 10-15 minute, must Herba Dendrobii cleansing milk.
CN201610501710.1A 2016-06-30 2016-06-30 Dendrobium officinale facial cleanser and preparation method thereof Pending CN105997690A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107854365A (en) * 2017-12-15 2018-03-30 广东盛美化妆品有限公司 A kind of mildy wash of the Herba Dendrobii extract containing iron sheet and preparation method thereof
CN108478502A (en) * 2018-03-30 2018-09-04 珠海美高美健康科技有限公司 Facial cleanser and preparation method thereof containing dendrobium candidum extract

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116675A (en) * 2014-07-23 2014-10-29 浙江森宇实业有限公司 Dendrobium candidum skin moisturizer and preparation method thereof
CN104288078A (en) * 2014-09-30 2015-01-21 江苏奇力康皮肤药业有限公司 Traditional Chinese medicine facial cleanser and preparation method thereof
CN104352394A (en) * 2014-11-17 2015-02-18 郭根松 Dendrobium nobile-containing Chinese herbal medicine facial-cleanser
CN105395402A (en) * 2015-11-28 2016-03-16 铜仁市金农绿色农业科技有限公司 Facial cleanser and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116675A (en) * 2014-07-23 2014-10-29 浙江森宇实业有限公司 Dendrobium candidum skin moisturizer and preparation method thereof
CN104288078A (en) * 2014-09-30 2015-01-21 江苏奇力康皮肤药业有限公司 Traditional Chinese medicine facial cleanser and preparation method thereof
CN104352394A (en) * 2014-11-17 2015-02-18 郭根松 Dendrobium nobile-containing Chinese herbal medicine facial-cleanser
CN105395402A (en) * 2015-11-28 2016-03-16 铜仁市金农绿色农业科技有限公司 Facial cleanser and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107854365A (en) * 2017-12-15 2018-03-30 广东盛美化妆品有限公司 A kind of mildy wash of the Herba Dendrobii extract containing iron sheet and preparation method thereof
CN108478502A (en) * 2018-03-30 2018-09-04 珠海美高美健康科技有限公司 Facial cleanser and preparation method thereof containing dendrobium candidum extract

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