CN106038396A - Dendrobium officinale mask and preparation method thereof - Google Patents
Dendrobium officinale mask and preparation method thereof Download PDFInfo
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- CN106038396A CN106038396A CN201610500928.5A CN201610500928A CN106038396A CN 106038396 A CN106038396 A CN 106038396A CN 201610500928 A CN201610500928 A CN 201610500928A CN 106038396 A CN106038396 A CN 106038396A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a dendrobium officinale mask and a preparation method thereof. The preparation method can reserve effective ingredients in dendrobium officinale. The dendrobium officinale mask comprises 5-8 parts by weight of filtered dendrobium officinale extract. A preparation method of the dendrobium officinale extract comprises the following steps: (1) cleaning, and carrying out sterilization pre-treatment; (2) soaking, namely putting dendrobium officinale and microbial strains with wax coats removed into deionized water, adding, stirring, and soaking for 10-30 days; (3) filtering; (4) decolourizing, namely adding activated carbon for decolourizing dendrobium officinale filtrate, and filtering, so that a dendrobium officinale extracting solution is obtained; (5) grinding, namely grinding the dendrobium officinale extracting solution and baked dendrobium officinale by virtue of a homogenizer, so that dendrobium officinale extract is obtained; and (6) filtering, so that filtered dendrobium officinale extract is obtained. According to the preparation method, dendrobium officinale is taken as a raw material for carrying out decolourization and low temperature extraction, pharmaceutical effects can not be influenced due to colour of the traditional Chinese medicine, and the effective ingredients of dendrobium officinale are well reserved.
Description
Technical field
The present invention relates to a kind of facial film and preparation method thereof, belong to medicinal plants manufacture field, particularly relate to a kind of iron sheet
Herba Dendrobii facial film and preparation method thereof.
Background technology
Herba Dendrobii is the new of orchid Herba Dendrobii (Dendrobium officinale Kimura et Migo)
Fresh stem, belongs to national conservative plant, has health preserving and the medical value of preciousness.Herba Dendrobii obtains because its epidermis is ferrum green
Name, successive dynasties Chinese medicine ancient books and records are the most on the books, the classics such as comprehensive Shennong's Herbal, Compendium of Material Medica, " detailed outline is picked up any lost article from the road " and " not Lu "
The works discussion to Herba Dendrobii, its primary efficacy is reinforcing YIN-essence benefit essence, clearing away heat and promoting production of body fluid, can tonifying five ZANG-organs asthenia, thick the intestines and stomach, strong muscle
Bone, arresting convulsion of calming the nerves, make light of one's life by commiting suicide and prolong life.Taoism regimen classical works " Taoist Scriptures " by Herba Dendrobii, Herba Saussureae Involueratae, three double Radix Ginsengs,
The hundred vicennial Radixs Polygoni Multiflori, Fu desert (Poria and Herba Cistanches), remote mountains Ganoderma, seabed Margarita and the Cordyceps of cycle of sixty years are also referred to as China nine
Big Herba mesonae chinensis, Herba Dendrobii ranks first.Herba Dendrobii nature and flavor: sweet, are slightly cold, and enter stomach, kidney channel;Property belong to clear and rich, clear in have benefit, invigorating middle warmer
Have clear.
Herba Dendrobii also has external efficacy, and modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free
Aminoacid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various mould, not only by oral absorption,
Herba Dendrobii can also stop blooding, promote wound healing, can be used for outward repairing damaged skin.
Dendrobium officinale polysaccharide has antibacterial, anti-inflammatory effect, the function of enhancing Cell-mediated Immunity, external can resist dirt hide from,
The infringement to skin such as antibacterial;Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thus promotees
Enter wound healing, repair damaged skin tissue.Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, equilibrium oil
Fat, has the antiallergic ability improving sensitive skin, prevents the generation of wrinkle；Activate Skin Cell superoxide dismutase peroxidating
The activity of thing, dispels the free radical that Skin Cell is superfluous, effective delay skin aging；The phagocytic function of activating macrophage, increases
Strong lymphoid toxin expelling, function of detoxification, effectively block the extraneous harmful substance infringement to skin；Improve resisting skin allergy energy
Power, and internal harmful substance and aged cells are decomposed excretion etc..
Also have now and be applied to the effective ingredient in Herba Dendrobii on skin record, if open mouth is 2013 08 month 14
Mouthful, in the Chinese patent of Publication No. CN103239471A, disclosing a kind of skin moistening external preparation, this skin moistening external preparation is by having
Effect composition and medically acceptable adjuvant composition, described effective ingredient be molecular weight be that the Herba Dendrobii of 85-90KDa is many
Sugar, with only the polysaccharide in Herba Dendrobii, and the utilization rate of Herba Dendrobii is low, during additionally, extract polysaccharide from Herba Dendrobii,
Have employed decoction extract, supersound extraction and enzymolysis and extraction these three method at 50 DEG C, these extracting method are for Herba Dendrobii
The destruction of the effective ingredient such as vitamin, aminoacid, organized enzyme is the most serious.
The most generally using the method decocted to extract the effective ingredient in Herba Dendrobii, traditional decoction extracting method can be led
Causing the destruction of the effective ingredient such as polysaccharide, vitamin, aminoacid, organized enzyme in Herba Dendrobii, polysaccharide, dimension in products obtained therefrom are raw
Element, chlorophyll, free amino acid equal size are relatively low, greatly reduce the utilization rate of Herba Dendrobii.Currently there are no one can
Retain Herba Dendrobii facial film of effective ingredient and preparation method thereof in Herba Dendrobii.
First Herba Dendrobii is clayed into power it addition, also have, the preparation method being then added in the substrate of skin care item, this
Although method can retain the effective ingredient of Herba Dendrobii, but owing to Herba Dendrobii Chinese medicine color is deep, for not affecting skin care item
Outward appearance, manufacturer the most only adds the most a small amount of Herba Dendrobii, causes the skin-care effect of Herba Dendrobii to be had a greatly reduced quality.
Summary of the invention
For solving above-mentioned technical problem, the technical solution used in the present invention is:
A kind of Herba Dendrobii facial film, this Herba Dendrobii facial film includes the raw material of following parts by weight: 60～68 parts of water；5～8 parts of mistakes
Herba Dendrobii extract after filter；8～11 parts of dipropylene glycol；5～7 parts of glycerol；2～4 parts of double-PEG-15 methyl ether poly dimethyls
Siloxanes；5～7 parts of Mel；0.3～0.5 part of acrylic aldehyde/acrylic copolymer；0.1～0.2 part of hydroxyethyl cellulose；0.2～
The Flos Rosae Rugosae quintessence oil of 0.3 part；0.15～0.25 part of Cremophor RH40 and propylene glycol；0.2～0.4 part of allantoin；1～3 part
Collagen protein；The mixture of phthalein urea in 0.2～0.4 part of IPBC and dihydroxymethyl dimethyl second.
A kind of Herba Dendrobii facial film, the preparation method of described Herba Dendrobii extract comprises the following steps:
(1) pretreatment: root and the stipes of fresh Herba Dendrobii are cleaned sterilization processing；
(2) soaking: put in deionized water by fresh Herba Dendrobii, and add the microorganism fungus kind sloughing wax coat, stirring is all
Even, soak 10～30 days, in the pigmentolysis of Herba Dendrobii to water；
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate；
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii extracting solution；
(5) grinding step: the Herba Dendrobii of temperature 2～the Herba Dendrobii extracting solution of 10 DEG C and filtration is placed in homogenizer, ferrum
Skin Herba Dendrobii is 1:4～1:9 with the weight ratio of Herba Dendrobii extracting solution, starts homogenizer and controls discharge fineness at 200～300 m
Hereinafter, Herba Dendrobii extract is obtained；
(6) filter progress: Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration.
Preferably technical scheme is: above-mentioned Herba Dendrobii facial film, described in slough the microorganism fungus kind of wax coat be hydrocarbon oxidation
Bacterium be pseudomonas (Pseudomonas), acinetobacter calcoaceticus (Acinetobacter), sporeformer (Bacillus), bud pole bacterium
(Geobacillus), vibrio (Vibrionaceae), micrococcus luteus (Micrococcus) or arthrobacterium (Arthrobacter) etc..
In patent of the present invention, further, the microorganism fungus kind quality sloughing wax coat described in accounts for Herba Dendrobii quality
0.05～0.5%.
In patent of the present invention, further, described quality of activated carbon accounts for the 1～3% of Herba Dendrobii filtrate quality.
In patent of the present invention, further, in described step (6), filtration includes coarse filtration step and fine straining step；Described slightly
Filter uses 100 mesh nylon filtering cloths to soak filtration；Described fine straining step uses high speed tube centrifuge, and rotating speed is 15000r/min.
A kind of Herba Dendrobii facial film preparation method, this preparation method comprises the following steps:
By dipropylene glycol, glycerol, double-PEG-15 methyl ether dimethicone, Mel, Cremophor RH40 and the third two
Alcohol, collagen protein are mixed and heated to 85 DEG C, maintain 30min sterilizing, it is thus achieved that obtain oil phase；By acrylic aldehyde/acrylic copolymer, hydroxyl second
Base cellulose, allantoin are added to the water, and are heated with stirring to 90～100 DEG C, maintain 30min sterilizing, are cooled to 85 DEG C, it is thus achieved that water
Phase；Oil phase is added to stirring and emulsifying in aqueous phase and obtains base material；Iron sheet when dropping to 40～45 DEG C at a temperature of base material, after filtering
In Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl second, phthalein urea is added in base material, continues to stir
Mix emulsifying 20min, then carry out emulsifying 5min with homogenizer, add Flos Rosae Rugosae quintessence oil, stir, stand cooling 12～24 little
Time become cream, stop stirring, cooling, obtain Herba Dendrobii facial film.
In sum, owing to have employed technique scheme, the invention has the beneficial effects as follows:
1, Herba Dendrobii is soaked by the present invention, it is thus achieved that Herba Dendrobii filtrate and Herba Dendrobii, and merges milled processed,
This preparation method remains the effective ingredient of Herba Dendrobii as far as possible, extracts with iron-sheet dendrobe fresh product for raw material, effectively
Composition is difficult to be destroyed, polysaccharide, vitamin, chlorophyll, free amino acid equal size height in products obtained therefrom；
2, the present invention uses hydrocarbon oxidation bacteria microorganism, decomposes the wax coat on Herba Dendrobii surface, makes Herba Dendrobii and water fully connect
Touch, make effective ingredient rapid dispersion in Herba Dendrobii in water；
3, Herba Dendrobii is carried out by the present invention soak operation, by Herba Dendrobii pigment, polysaccharide, dendrobine, aminoacid maximum journey
Degree extracts, damage；Use activated carbon that Herba Dendrobii filtrate is decoloured, it is to avoid Chinese medicine color is the deepest simultaneously,
Affect the performance of drug effect, it is to avoid affect the using effect of facial film；
4, the scientific formulation, rationally of Herba Dendrobii facial film of the present invention, can produce cooperative effect, it is possible to significantly more efficient between composition
Give play to effect of polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract, and advantageously in skin absorption ferrum
Polysaccharide, chlorophyll, vitamin and protein in skin Herba Dendrobii extract.
Owing to current Herba Dendrobii product is many to take orally, Herba Dendrobii expanded by the Herba Dendrobii facial film in the present invention
Application, substantially more play its be worth.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, the following is embodiment explanation of the invention and
The invention is not limited in following example.
Herba Dendrobii face pack prescription: 60～68 parts of water；Herba Dendrobii extract after 5～8 parts of filtrations；8～11 parts of dipropyls
Glycol；5～7 parts of glycerol；2～4 parts of double-PEG-15 methyl ether dimethicone；5～7 parts of Mel；0.3～0.5 part of propylene
Aldehyde/acrylic copolymer；0.1～0.2 part of hydroxyethyl cellulose；The Flos Rosae Rugosae quintessence oil of 0.2～0.3 part；0.15～0.25 part of PEG-
40 castor oil hydrogenated and propylene glycol；0.2～0.4 part of allantoin；1～3 part of collagen protein；0.2～0.4 part of iodo propinyl butyl
The mixture of phthalein urea in carbamate and dihydroxymethyl dimethyl second.
Embodiment 1.
(1) sterilization processing is cleaned: root and the stipes of fresh Herba Dendrobii are rinsed 3 times with tap water, rush with pure water
Wash 2 times, with warm water " quenches " 3～5min, be cut into the segment of 0.5～1.5cm；
(2) soak: the Herba Dendrobii after sterilization is put in deionized water, and adds pseudomonas, stir, soak 10
My god, in the pigmentolysis of Herba Dendrobii to water；
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate:
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii extracting solution,
Put into refrigerator freezing；
(5) grinding step: Herba Dendrobii extracting solution that temperature is 2 DEG C and the Herba Dendrobii after filtering are placed in homogenizer, ferrum
The weight ratio of skin Herba Dendrobii and Herba Dendrobii extracting solution is 1:4, starts homogenizer and controls discharge fineness at 200～300 below m,
Obtain Herba Dendrobii extract；
(6) filter progress: soaked by 100 mesh nylon filtering cloths, is folded in 2 layers of funnel being laid in vacuum filtration, and edge is placed in
Outside funnel, open vacuum filtration machine, then Herba Dendrobii superfine grinding liquid poured in funnel, filter to liquid medicine storage tank,
Filtering residue thickness reaches cleaning when 0.5～lcm and once, collects filtering residue otherwise utilized；
Fine straining: start high speed tube centrifuge (rotating speed is 15000r/min) and peristaltic pump, set the rotating speed of peristaltic pump as 150～
250r/min, by feed pipe to coarse filtration liquid, starts centrifugal filtration to new liquid medicine storage tank.Every centrifugal filtration 200～300L
Cleaning filtering residue once, is collected by filtration filtering residue, merges with the filtering residue obtained in coarse filtration, otherwise utilized.The filter obtained after fine straining
Liquid is the Herba Dendrobii extract after filtering；
(7) emulsification process: by dipropylene glycol, glycerol, double-PEG-15 methyl ether dimethicone, Mel, PEG-40 hydrogenation
Oleum Ricini and propylene glycol, collagen protein are mixed and heated to 85 DEG C, maintain 30min sterilizing, it is thus achieved that obtain oil phase；By acrylic aldehyde/propylene
Acid copolymer, hydroxyethyl cellulose, allantoin are added to the water, and are heated with stirring to 90 DEG C, maintain 30min sterilizing, are cooled to 85
DEG C, it is thus achieved that aqueous phase；Oil phase is added to stirring and emulsifying in aqueous phase and obtains base material；When dropping to 40 DEG C at a temperature of base material, after filtering
Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl second in phthalein urea be added in base material,
Continue stirring and emulsifying 20min, then carry out emulsifying 5min with homogenizer, add Flos Rosae Rugosae quintessence oil, stir, stand cooling 12
Hour become cream, stop stirring, cooling, obtain Herba Dendrobii facial film.
Embodiment 2.
1) sterilization processing is cleaned: root and the stipes of fresh Herba Dendrobii are rinsed 3 times with tap water, rush with pure water
Wash 2 times, with warm water " quenches " 3～5min, be cut into the segment of 0.5～1.5cm；
(2) soak: the Herba Dendrobii after sterilization is put in deionized water, and adds acinetobacter calcoaceticus, stir, soak 15
My god, then ultrasonic wave concussion, in the pigmentolysis of Herba Dendrobii to water；
(3) filter: appeal soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate:
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, decolouring, filter and obtain Herba Dendrobii extracting solution,
Put into refrigerator freezing；
(5) grinding step: Herba Dendrobii extracting solution that temperature is 2 DEG C and the Herba Dendrobii after filtering are placed in homogenizer, ferrum
The weight ratio of skin Herba Dendrobii and Herba Dendrobii extracting solution is 1:9, starts homogenizer and controls discharge fineness at 200～300 below m,
Obtain Herba Dendrobii extract；
(6) filter progress: soaked by l00 mesh nylon filtering cloth, is folded in 2 layers of funnel being laid in vacuum filtration, and edge is placed in
Outside funnel, open vacuum filtration machine, then Herba Dendrobii superfine grinding liquid poured in funnel, filter to liquid medicine storage tank,
Filtering residue thickness reaches cleaning when 0.5～1cm and once, collects filtering residue otherwise utilized；
Fine straining: start high speed tube centrifuge (rotating speed is 15000r/min) and peristaltic pump, set the rotating speed of peristaltic pump as 150～
250r/min, by feed pipe to coarse filtration liquid, starts centrifugal filtration to new liquid medicine storage tank.Every centrifugal filtration 200～300L
Cleaning filtering residue once, is collected by filtration filtering residue, merges with the filtering residue obtained in coarse filtration, otherwise utilized.The filter obtained after fine straining
Liquid is the Herba Dendrobii extract after filtering；
(7) emulsification process: by dipropylene glycol, glycerol, double-PEG-15 methyl ether dimethicone, Mel, PEG-40 hydrogenation
Oleum Ricini and propylene glycol, collagen protein are mixed and heated to 85 DEG C, maintain 30min sterilizing, it is thus achieved that obtain oil phase；By acrylic aldehyde/propylene
Acid copolymer, hydroxyethyl cellulose, allantoin are added to the water, and are heated with stirring to 100 DEG C, maintain 30min sterilizing, are cooled to 85
DEG C, it is thus achieved that aqueous phase；Oil phase is added to stirring and emulsifying in aqueous phase and obtains base material；When dropping to 45 DEG C at a temperature of base material, after filtering
Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl second in phthalein urea be added in base material,
Continue stirring and emulsifying 20min, then carry out emulsifying 5min with homogenizer, add Flos Rosae Rugosae quintessence oil, stir, stand cooling 24
Hour become cream, stop stirring, cooling, obtain Herba Dendrobii facial film.
Claims (7)
1. a Herba Dendrobii facial film, it is characterised in that: this Herba Dendrobii facial film includes the raw material of following parts by weight: 60～68
Part water；5～8 parts of Herba Dendrobii extracts；8～11 parts of dipropylene glycol；5～7 parts of glycerol；2～4 parts of double-PEG-15 methyl ethers gather
Dimethyl siloxane；5～7 parts of Mel；0.3～0.5 part of acrylic aldehyde/acrylic copolymer；0.1～0.2 part of hydroxyethyl cellulose；
The Flos Rosae Rugosae quintessence oil of 0.2～0.3 part；0.15～0.25 part of Cremophor RH40 and propylene glycol；0.2～0.4 part of allantoin；1
～3 parts of collagen protein；In 0.2～0.4 part of IPBC and dihydroxymethyl dimethyl second, phthalein urea is mixed
Compound.
Herba Dendrobii facial film the most according to claim 1, it is characterised in that: the preparation method bag of described Herba Dendrobii extract
Include following steps:
(1) pretreatment: root and the stipes of fresh Herba Dendrobii are cleaned sterilization processing；
(2) soak: Herba Dendrobii is put in deionized water, and add the microorganism fungus kind sloughing wax coat, stir, leaching
Steep 10～30 days；
(3) filter: above-mentioned soak is filtered, obtains Herba Dendrobii and Herba Dendrobii filtrate；
(4) decolouring: activated carbon is added above-mentioned steps (3) Herba Dendrobii filtrate, stirring, decolouring, filter acquisition Herba Dendrobii and carry
Take liquid, deliver to fridge freshness retaining；
(5) grinding step: temperature 2～the Herba Dendrobii extracting solution of 10 DEG C and Herba Dendrobii are placed in homogenizer, Herba Dendrobii
Be 1:4～1:9 with the weight ratio of Herba Dendrobii extracting solution, start homogenizer and control discharge fineness at 200～300 below m,
Obtain Herba Dendrobii extract；
(6) filter progress: thick Herba Dendrobii extract is filtrated to get the Herba Dendrobii extract after filtration.
Herba Dendrobii facial film the most according to claim 2, it is characterised in that the microorganism fungus kind sloughing wax coat described in: is hydrocarbon
Oxidation bacteria be pseudomonas, acinetobacter calcoaceticus, sporeformer, bud pole bacterium, vibrio, micrococcus luteus or arthrobacterium.
Herba Dendrobii facial film the most according to claim 2, it is characterised in that slough the microorganism fungus kind quality of wax coat described in:
Account for the 0.05～0.5% of Herba Dendrobii quality.
Herba Dendrobii facial film the most according to claim 2, it is characterised in that: quality of activated carbon accounts for Herba Dendrobii filtrate quality
1～3%.
Herba Dendrobii facial film the most according to claim 2, it is characterised in that: described step (6) filters and includes coarse filtration step
With fine straining step；Described coarse filtration uses 100 mesh nylon filtering cloths to soak filtration；Described fine straining step uses high speed tube centrifuge,
Rotating speed is 15000r/min.
7. a Herba Dendrobii facial film preparation method, it is characterised in that: this preparation method comprises the following steps:
By dipropylene glycol, glycerol, double-PEG-15 methyl ether dimethicone, Mel, Cremophor RH40 and the third two
Alcohol, collagen protein are mixed and heated to 85 DEG C, maintain 30min sterilizing, it is thus achieved that obtain oil phase；By acrylic aldehyde/acrylic copolymer, hydroxyl second
Base cellulose, allantoin are added to the water, and are heated with stirring to 90～100 DEG C, maintain 30min sterilizing, are cooled to 85 DEG C, it is thus achieved that water
Phase；Oil phase is added to stirring and emulsifying in aqueous phase and obtains base material；Iron sheet when dropping to 40～45 DEG C at a temperature of base material, after filtering
In Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl second, phthalein urea is added in base material, continues to stir
Mix emulsifying 20min, then carry out emulsifying 5min with homogenizer, add Flos Rosae Rugosae quintessence oil, stir, stand cooling 12～24 little
Time become cream, stop stirring, cooling, obtain Herba Dendrobii facial film.
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| CN109157475A (en) * | 2018-10-16 | 2019-01-08 | 皖西学院 | Dendrobium candidum facial mask and preparation method thereof |
| CN110664720A (en) * | 2019-11-04 | 2020-01-10 | 菲朗生物科技(湖北)有限公司 | Dendrobium officinale essence lotion and preparation method thereof |
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| CN108014062A (en) * | 2018-01-03 | 2018-05-11 | 浙江东来天然生物制品有限公司 | Facial mask containing dendrobium candidum active ingredient |
| CN109157475A (en) * | 2018-10-16 | 2019-01-08 | 皖西学院 | Dendrobium candidum facial mask and preparation method thereof |
| CN110664720A (en) * | 2019-11-04 | 2020-01-10 | 菲朗生物科技(湖北)有限公司 | Dendrobium officinale essence lotion and preparation method thereof |
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Application publication date: 20161026 |