CN104127341A - Dendrobium officinale mask and preparation method - Google Patents
Dendrobium officinale mask and preparation method Download PDFInfo
- Publication number
- CN104127341A CN104127341A CN201410354140.9A CN201410354140A CN104127341A CN 104127341 A CN104127341 A CN 104127341A CN 201410354140 A CN201410354140 A CN 201410354140A CN 104127341 A CN104127341 A CN 104127341A
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- CN
- China
- Prior art keywords
- herba dendrobii
- parts
- weight
- water
- facial film
- Prior art date
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- Granted
Links
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- 241001076416 Dendrobium tosaense Species 0.000 title abstract description 19
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 8
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Abstract
The invention relates to a Dendrobium officinale mask and its preparation method. Nowadays, there is no Dendrobium officinale mask, in which active ingredients in Dendrobium officinale can be retained, or a preparation method thereof. The Dendrobium officinale mask contains 5-8 parts by weight of a filtered Dendrobium officinale extract which contains polysaccharide, chlorophyll, vitamin and protein. The preparation method of the Dendrobium officinale mask comprises the following processes in order: A, pretreatment process; B, low-temperature ultramicro-grinding process: placing water of 2-10 DEG C and cut-off Dendrobium officinale into a homogenizer with the weight ratio of Dendrobium officinale to water being 1:6-1:8, starting the homogenizer and controlling discharging material fineness to below 200-300 microns so as to obtain a Dendrobium officinale extract; C, filtration process; and D, emulsification process. According to the invention, a Dendrobium officinale fresh product used as a raw material undergoes low-temperature extraction, and active ingredients in Dendrobium officinale can be retained as much as possible. The contents of polysaccharide, vitamin, chlorophyll, free amino acid and the like in the product obtained are high.
Description
Technical field
The present invention relates to a kind of facial film and preparation method thereof, especially relate to a kind of Herba Dendrobii facial film and preparation method thereof, belong to medicinal plants manufacture field.
Background technology
Herba Dendrobii is the fresh stem of orchid Herba Dendrobii (Dendrobium officinale Kimura et Migo), belongs to state guarantee plant, has precious health preserving and medical value.Because its epidermis is, ferrum is green gains the name Herba Dendrobii, successive dynasties Chinese medicine ancient books and records are all on the books, comprehensive < < Sheng Nong's herbal classic > >, < < Compendium of Materia Medica > >, pick up any lost article from the road > > and < < of < < detailed outline do not record the discussions of classical works to Herba Dendrobii such as > >, its main effect is reinforcing YIN-essence benefit essence, clearing away heat and promoting production of body fluid, can tonifying five ZANG-organs asthenia, thick the intestines and stomach, strong muscles and bones, the arresting convulsion of calming the nerves, make light of one's life by commiting suicide and prolong life.The health preserving classical works < < Taoist Scriptures > > of Taoist school is by Fu desert (Poria and Herba Cistanches), remote mountains Ganoderma, seabed Margarita and the Cordyceps of Herba Dendrobii, Herba Saussureae Involueratae, three double Radix Ginsengs, the hundred vicennial Radixs Polygoni Multiflori, cycle of sixty years and be called China's nine large Herba mesonae chinensis, and Herba Dendrobii ranks first.Herba Dendrobii nature and flavor: sweet, be slightly cold, enter stomach, kidney channel; Property belong to clear and rich, have benefit in clear, invigorating middle warmer has clearly.
The efficacy effect of Herba Dendrobii, successive dynasties well-known doctor respectively has discussion, specific as follows:
< < explaining abstruseness of the canon of materia medica > > cloud: " Herba Dendrobii, sweet energy is pleased spleen, salty can kidney tonifying; therefore many merits are dirty in water and soil two: but gas is wide slow; the merit of playing without victory, ancients with this tea, on very clear diaphragm in generation.”
< < A Supplement to the Compendium of Materia Medica > > cloud: " Herba Dendrobii clearing stomach except deficiency-heat, promote the production of body fluid and strain, with for tea, merit with ginseng stilbene.”
" for tea, promote the production of body fluid and wet one's whistle summer, and reinforcing YIN-essence is good for sufficient power in < < property of medicine > >, to record Herba Dendrobii." visible, Herba Dendrobii is long-standing as the high tonic being of illnesses and fitness.The traditional Chinese medical science thinks, Herba Dendrobii can extensive use in the disease treatments such as atrophic gastritis, tumor, diabetes, pharyngolaryngitis and cataract.Herba Dendrobii has multiple pharmacological effect, and as the immunocompetence of enhancing body, antioxidation, defying age, reduce blood glucose, YIN nourishing and the production of body fluid promoting etc.The traditional Chinese medical science is thought, " YIN and YANG in a relative equilibrium, life activities being normally maintained." as empty in cloudy body fluid deficiency, can not contain sun, sun is floating, and without system, equilibrium between yin and yang is destroyed, and all diseases are grown thickly.”
< < Ling Shu Miraculous Pivot or Divine Axis Benshen piece of writing > > says: " the main store essential substances person of the five internal organs also, can not hinder, and wound is fallen into enemy hands and the deficiency of YIN, and the deficiency of YIN is depletion of QI, and depletion of QI is dead." Herba Dendrobii Yin-nourishing and body fluid promoting key medicine just, between old friend, be referred to as " help Herba mesonae chinensis ".
< < Sheng Nong's herbal classic > >: main damaging the spleen and stomach, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards, tonifying five ZANG-organs asthenia weakness and emaciation, reinforcing YIN-essence, take thick the intestines and stomach for a long time.
< < Compendium of Materia Medica > >: reinforcing YIN-essence benefit essence.Take for a long time, thick the intestines and stomach, never sufficient in benefit, flat gastric qi, longue meat, by skin pathogenic heat miliaria gas, a little less than foot knee joint aches cold numbness, determines intelligence except frightened, makes light of one's life by commiting suicide and prolongs life.
The < < detailed outline > > that picks up any lost article from the road: clearing stomach is except deficiency-heat, the strain in the sixth of the twelve Earthly Branches of promoting the production of body fluid, with for tea, appetite promoting and the spleen strengthening.Wind is treated in arresting convulsion, energy town saliva expectorant, sweet fragrant sending down the abnormal ascending QI.
< < medicineization justice > >: control lung qi prolonged deficiency, cough is more than.
< < does not record > >: benefit essence is never sufficient in mending, flat gastric qi, and longue meat, by skin pathogenic heat gas, foot knee joint pain is weak, strong sun, the long-pending essence of the kidney invigorating.
< < Japan hanako materia medica > >: control deficient bad weak strengthening bone and muscle, warming the kidney, Fructus Alpiniae Oxyphyllae, flat gastric qi, by exogenous pathogen.
< < book on Chinese herbal medicine is new > > again: reason gastric qi, clearing stomach fire.Remove excessive thirst in the heart, treat kidney channel deficiency-heat, the arresting convulsion of calming the nerves, separates night sweat, and summer-heat can fall apart.
Herba Dendrobii also has external efficacy, modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free amino acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzyme, not only can pass through oral absorption, Herba Dendrobii can also stop blooding, promote wound healing, can be outward for repairing damaged skin.
The effect of polysaccharide in A, Herba Dendrobii to skin.
That Dendrobium officinale polysaccharide has is antibacterial, the function of anti-inflammatory effect, enhancing Cell-mediated Immunity, and external can be resisted the infringement to skin such as dirt demodicid mite, antibacterial; Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thereby promotes wound healing, repairs damaged skin tissue.Theory of Chinese medical science is thought, Herba Dendrobii cold nature is the holy product of YIN nourishing, and skin is grown skin sore, acne, small pox etc. and mostly is due to hyperactivity of fire caused by deficiency of YIN, therefore Herba Dendrobii can be used for above-mentioned skin problem.
The effect of free amino acid in B, Herba Dendrobii to skin.
Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, Sage Extract, is improved the antiallergic ability of sensitive skin, prevents the generation of wrinkle; Activate the activity of Skin Cell superoxide dismutase peroxide, the free radical of dispelling Skin Cell surplus, effectively delay skin aging; The phagocytic function of activating macrophage, strong lymphoid toxin expelling once, function of detoxification, effectively blocks the infringement of extraneous harmful substance to skin; Improve resisting skin allergy ability, and harmful substance in body and aged cells are decomposed to excretion.Can with bivalent metal ion generation chelatropic reaction in wheat bran, stop too much bivalent metal ion and the collagen protein generation crosslinked action in skin, maintain enough collagen fiber and elastic fibers, make soft and smooth, the fine and smooth high resilience of skin.
The major function of the vitamin A in C, Herba Dendrobii.
Vitamin A, in vivo from the oxidative damage of different link antagonism radical pair cells, is strengthened the oxidation resistance of health, the harm that alleviates free radical; Contribute to keep skin soft and plentiful, improve the lock water function of skin; There is significantly anti-cornified effect, and can delay skin aging, in division and the development of Skin Cell, have regulating action; Help acne carried out to topical therapeutic, and prevent that pachylosis from chapping, chilblain and dandruff etc.; Contribute to strengthen metabolism, make skin keep younger state.
Vitamin C in D, Herba Dendrobii and the vitamin E effect to skin.
Vitamin C, the effect of E aspect beauty and skin care are very important especially.Because the Oxidation of human body sebum is the one of the main reasons of skin aging, and vitamin E has antioxidation, thereby protected the moisture in sebum and cell membrane protein and skin; It can also promote regeneration and the vigor of human body cell, postpones the ageing process of cell.In addition, can also promote the utilization of human body to vitamin A; Can play synergism with vitamin C, the health of protection skin, reduces occurrence of skin infections; Collagen fiber in skin and elastic fibers are had to " moistening " effect, thereby improve and safeguard the elasticity of skin; Can promote the blood circulation in skin, make skin obtain sufficient nutrition and moisture, to maintain the tender and gloss of skin; Also can suppress the formation of pigmented spots, senile plaque, reduce facial wrinkles and pure white skin, prevent and treat acne.
Now also have the effective ingredient in Herba Dendrobii is applied on skin and is recorded, if open day is on 08 14th, 2013, publication number is in the Chinese patent of CN103239471A, a kind of skin moistening external preparation is disclosed, this skin moistening external preparation is comprised of effective ingredient and medically acceptable adjuvant, described effective ingredient is that molecular weight is the Dendrobium officinale polysaccharide of 85-90KDa, only utilized the polysaccharide in Herba Dendrobii, the utilization rate of Herba Dendrobii is low, in addition, while extracting polysaccharide from Herba Dendrobii, adopted to decoct and extracted, these three kinds of methods of supersound extraction and enzymolysis and extraction at 50 ℃, these extracting method are for the vitamin of Herba Dendrobii, aminoacid, the destruction of the effective ingredient such as organized enzyme is comparatively serious.
Conventionally adopt at present the method decocting to extract the effective ingredient in Herba Dendrobii, traditional decoction extracting method can cause the destruction of the effective ingredient such as polysaccharide in Herba Dendrobii, vitamin, aminoacid, organized enzyme, polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are lower, greatly reduce the utilization rate of Herba Dendrobii.Now also there is no a kind of Herba Dendrobii facial film that can retain effective ingredient in Herba Dendrobii and preparation method thereof.
Summary of the invention
The object of the invention is to overcome above shortcomings in prior art, and provide a kind of Herba Dendrobii effective ingredient that retains as much as possible, expand Herba Dendrobii application, give full play to Herba Dendrobii facial film of Herba Dendrobii value and preparation method thereof, this Herba Dendrobii facial film and preparation method thereof be take iron-sheet dendrobe fresh product and is carried out low-temperature extraction as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, and the polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are high., Herba Dendrobii facial film and preparation method thereof.
The present invention addresses the above problem adopted technical scheme: the feature of this Herba Dendrobii facial film is: this Herba Dendrobii facial film comprises that parts by weight are the water of 65～68 parts; Parts by weight are the Herba Dendrobii extract after the filtration of 5～8 parts, in the Herba Dendrobii extract after this filtration, contain polysaccharide, chlorophyll, vitamin and protein; Parts by weight are the dipropylene glycol (DPG) of 8～11 parts; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 5～7 parts, and wherein, the weight ratio of polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 2:1:2; Parts by weight be 2～4 parts two-PEG-15 methyl ether polydimethylsiloxane; Parts by weight are the avenabeta glucosan of 5～7 parts; Parts by weight are the acrylic aldehyde/acrylic copolymer of 0.3～0.5 part; Parts by weight are the hydroxyethyl-cellulose of 0.1～0.2 part; Parts by weight are the triethanolamine of 0.1～0.2 part; Parts by weight are the butanediol, 1 of 0.2～0.3 part, 2-pentanediol and the benzoic mixture of para hydroxybenzene propionamido-, and this butanediol, 1,2-pentanediol and the benzoic weight ratio of para hydroxybenzene propionamido-are 3:2:1; Parts by weight are Cremophor RH40 and the propylene glycol of 0.15～0.25 part, and the weight ratio of this Cremophor RH40 and propylene glycol is 1:1; Parts by weight are the hyaluronate sodium of 0.2～0.4 part; Parts by weight are the allantoin of 0.2～0.4 part; Parts by weight are the EDETATE SODIUM of 0.04～0.06 part; Parts by weight are the IPBC (IPBC) of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC (IPBC) and dihydroxymethyl dimethyl hydantoin is 3:2.Make thus the scientific formulation of Herba Dendrobii facial film in the present invention, between composition, can produce synergism, can more effectively give play to the effect that contains polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract, and more be conducive to skin and absorb polysaccharide, chlorophyll, vitamin and the protein containing in Herba Dendrobii extract.
As preferably, Herba Dendrobii extract after filtration of the present invention is adopted with the following method and is made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, taking-up is placed in water cooling, then cut off, Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, the weight ratio of Herba Dendrobii and water is 1:6～1:8, start homogenizer and control discharge fineness below 200～300 μ m, obtain Herba Dendrobii extract, the Herba Dendrobii extract after Herba Dendrobii extract is filtered.
A preparation method for Herba Dendrobii facial film, its feature is: comprise successively following operation:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming;
B sterilization,
Fresh Herba Dendrobii after cleaning is placed in the boiling water 3～5min that sterilizes, take out be placed in water cooling;
C cutting,
By Herba Dendrobii cutting;
B low temperature superfine grinding operation,
Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, and the weight ratio of Herba Dendrobii and water is 1:6～1:8, starts homogenizer and controls discharge fineness below 200～300 μ m, obtains Herba Dendrobii extract;
C filter progress,
Herba Dendrobii extract after Herba Dendrobii extract is filtered, contains polysaccharide, chlorophyll, vitamin and protein in the Herba Dendrobii extract after this filtration;
D emulsification process,
The oil phase of formula ratio is heated to 85 ℃, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 ℃, maintain 30min sterilizing, be cooled to 85 ℃; Oil phase is added to stirring and emulsifying in water and obtains base material; When the temperature of base material drops to 40～45 ℃, Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl hydantoin after filtering are added in base material, continue stirring and emulsifying 20min, with homogenizer, carry out emulsifying 5min again, within standing cooling 12～24 hours, become cream, stop stirring, cooling, obtains Herba Dendrobii facial film;
E fill operation,
Herba Dendrobii facial film is carried out to fill.
Make thus in the course of processing of the whole Herba Dendrobii extract of the present invention, except instantaneously sterilising, all at 30 ℃, complete below, even if in the course of processing of Herba Dendrobii facial film, its temperature is also controlled at below 45 ℃, has fully retained the various effective ingredient in Herba Dendrobii.
As preferably, in a Herba Dendrobii ingredient requirement of A pretreatment procedure of the present invention, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
As preferably, in the b sterilization of A pretreatment procedure of the present invention, in 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, by purified water, rinse 2 times again, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, take out in rearmounted purified water cooling.
As preferably, C filter progress of the present invention in turn includes the following steps:
A coarse filtration step,
100 order nylon filtering cloths are soaked, be folded in 2 layers of funnel that is laid in vacuum filtration, edge is placed in outside funnel, open vacuum filtration machine, vacuum is greater than 0.07MPa, Herba Dendrobii extract is poured in funnel again, filtered the coarse filtration liquid obtaining, when filtering residue thickness reaches 0.5～1cm, cleaning once;
B fine straining step,
Start high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump is 150～250r/min, by feed pipe to coarse filtration liquid, Herba Dendrobii extract after being filtered after centrifugal filtration, Herba Dendrobii extract after filtering is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue once.
As preferably, in D emulsification process of the present invention, described oil phase comprises polymethyl acid glyceride, propylene glycol and Gantrez AN-119, two-PEG-15 methyl ether polydimethylsiloxane, acrylic aldehyde/acrylic copolymer, hydroxyethyl-cellulose, triethanolamine, and, butanediol/1,2-pentanediol/para hydroxybenzene propionamido-benzoic acid.
As preferably, in D emulsification process of the present invention, described water comprises dipropylene glycol (DPG), avenabeta glucosan, propylene glycol, Cremophor RH40, hyaluronate sodium, allantoin and EDETATE SODIUM.
As preferably, in E fill operation of the present invention, get the packaging material that disinfect, with mastic automatic filling machine, the Herba Dendrobii facial film being up to the standards is carried out to fill, pouring process is controlled the loading amount of product, and overgauge is in 7.5%.
A Herba Dendrobii facial film, its feature is: this Herba Dendrobii facial film adopts above-mentioned preparation method to be prepared from.
The present invention compared with prior art, have the following advantages and effect: the iron-sheet dendrobe fresh product of take carries out low-temperature extraction as raw material, the course of processing of whole Herba Dendrobii extract, except instantaneously sterilising, all at 30 ℃, complete below, even if in the course of processing of Herba Dendrobii facial film, its temperature is also controlled at below 45 ℃, fully retained the various effective ingredient in Herba Dendrobii, saved the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed.Experimental results show that, adopt in the resulting Herba Dendrobii extract of preparation method of Herba Dendrobii facial film in the present invention, after giving money as a gift according to Herba Dendrobii extract, calculate, polyoses content reaches 60% (be traditional decoction extraction process 1.5～2 times), Vitamin C content reaches 50mg/100g (be traditional decoction extraction process 20 times), chlorophyll content reaches 60mg/100g (and traditional decoction extraction process almost makes chlorophyll composition all destroy), and protein content also reaches 8.9% (be about traditional decoction extraction process 1.2～1.5 times), and extraction yield also exceeds more than 1.5 times than traditional handicraft, therefore extraction process advantage of the present invention is very obvious, beneficial effect highly significant.The compositions such as the polysaccharide in Herba Dendrobii, chlorophyll, vitamin and protein can be absorbed by the body by skin, can be skin very abundant nutrition is provided, there is bibliographical information, Herba Dendrobii has hemostasis and promotes the effect of wound healing, external can be repaired damaged skin, the present invention has expanded the application of Herba Dendrobii, has boundless market prospect.
In the present invention, the preparation method of Herba Dendrobii facial film has retained the effective ingredient of Herba Dendrobii as much as possible, the iron-sheet dendrobe fresh product of take carries out low-temperature extraction as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, and polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are high; Adopt low-temperature extraction technology, Dendrobium officinale polysaccharide, dendrobine, aminoacid are at utmost extracted, protect the compositions such as Herba Dendrobii Determination of Chlorophyll, vitamin and organized enzyme to avoid high temperature simultaneously and destroy.
Because current Herba Dendrobii product is main mainly with taking orally, the Herba Dendrobii facial film in the present invention has been expanded the application of Herba Dendrobii, brings into play more fully its value.
Accompanying drawing explanation
Fig. 1 is the schematic flow sheet of the preparation method of Herba Dendrobii facial film in the embodiment of the present invention.
Fig. 2 is the schematic flow sheet of Herba Dendrobii extract preparation technology in the embodiment of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing and by embodiment, the present invention is described in further detail, and following examples are explanation of the invention and the present invention is not limited to following examples.
Embodiment.
Referring to Fig. 1 to Fig. 2,
Table one Herba Dendrobii extraction process and major parameter
Be the proportioning of Herba Dendrobii extract and other components again, specifically refer to table two.
Table two Herba Dendrobii face pack prescription
Remarks: in table two, " CN Translation " hurdle ratio used is weight ratio.
Finally determine preparation technology and the parameter of Herba Dendrobii facial film.
In the present embodiment, the preparation method of Herba Dendrobii facial film comprises following operation successively.
(1) pre-treatment.
1, Herba Dendrobii ingredient requirement.
Select the Herba Dendrobii of 3 years trophophases, and gathered when (April～June) before blooming.The experiment proved that, be the most vigorous period of Growth of Dendrobium candidum before florescence, Dendrobium officinale polysaccharide, vitamin, free amino acid, chlorophyll and other organized enzyme content are the highest in the whole year, and its epidermis and stem are all ferrum green, fiber content is low, is beneficial to and improves product extraction yield.
2, sterilization.
In 200L caldron, add 150L purified water, heated and boiled, rinses tap water for Herba Dendrobii 3 times, then rinses 2 times by purified water, with the appropriate Herba Dendrobii of rustless steel gripping, puts the boiling water 3～5min that " quenches ", and taking-up is put in purified water cooling.
3, cutting.
Get the complete Herba Dendrobii of sterilization, with medicine cutter, carry out cutting, the speed control system of cutting is 150～180 times/min, and every segment length is controlled at 0.5～1.5cm, and the Herba Dendrobii section cutting is collected with the stainless steel cask of sterilizing, standby.
(2) low temperature superfine grinding technique and parameter.
First homogenizer all parts is cleaned, and the ethanol disinfection that is 75% by percent by volume, treat that ethanol volatilizes, erection unit, the gap of adjustment stator and rotor, makes it at 0.3～0.5mm, opens cooling water valve.Get appropriate cryogenic purincation water (2～10 ℃ of water temperatures), weigh, pour in homogenizer hopper, make purified water liquid level hopper 1/3～2/3 between.Get the Herba Dendrobii of the appropriate above-mentioned section of cutting again, weigh, the ratio that makes Herba Dendrobii and purified water is 1:6～1:8.Discharge valve is adjusted to " circulation ", starts homogenizing button, monitoring discharge fineness, is controlled at below 200～300 μ m particle diameter, and in Herba Dendrobii superfine grinding liquid use, turning barrel is collected, standby.
(3) filtering technique and parameter.
1, coarse filtration.
100 order nylon filtering cloths are soaked, be folded in 2 layers of funnel that is laid in vacuum filtration, edge is placed in outside funnel, open vacuum filtration machine, guarantee that vacuum is greater than 0.07Mpa, then Herba Dendrobii superfine grinding liquid is poured in funnel, be filtered in liquid medicine storage tank, when filtering residue thickness reaches 0.5～1cm, cleaning once, is collected filtering residue and is separately used as him.
2, fine straining.
Start high speed tube centrifuge (rotating speed is 15000r/min) and peristaltic pump, the rotating speed of setting peristaltic pump is 150～250r/min, and feed pipe, to coarse filtration liquid, is started to centrifugal filtration to new liquid medicine storage tank.Every centrifugal filtration 200～300L cleaning filtering residue once, filters and collects filtering residue, merges with the filtering residue obtaining in coarse filtration, is separately used as him.The filtrate obtaining after fine straining is the Herba Dendrobii extract after filtering.
(4) emulsifying process and parameter.
By formula ratio oil phase (comprise polymethyl acid glyceride (with) propylene glycol (with) Gantrez AN-119, two-PEG-15 methyl ether polydimethylsiloxane, acrylic aldehyde/acrylic copolymer, hydroxyethyl-cellulose, triethanolamine, butanediol/1,2-pentanediol/para hydroxybenzene propionamido-benzoic acid) be heated to 85 ℃, maintain 30min sterilizing; Water (comprising dipropylene glycol (DPG), avenabeta glucosan, Cremophor RH40/propylene glycol, hyaluronate sodium, allantoin and EDETATE SODIUM) raw material is added in deionized water, be heated with stirring to 90～100 ℃, maintain 30min sterilizing, be cooled to 85 ℃; Oil phase is slowly added to stirring and emulsifying in water, obtains base material; When temperature drops to 40～45 ℃, Herba Dendrobii extract, IPBC (IPBC)/dihydroxymethyl dimethyl hydantoin after filtering are added in base material, continue stirring and emulsifying 20min, with homogenizer, carry out emulsifying 5min, within standing cooling 12～24 hours, become cream, stop stirring, cooling, then censorship, discharging, obtains Herba Dendrobii facial film.
The course of processing of whole Herba Dendrobii extract, except instantaneously sterilising, all at 30 ℃, complete below, even if the course of processing at Herba Dendrobii facial film, its temperature is also controlled at below 45 ℃, fully retain the various effective ingredient in Herba Dendrobii, given full play to effect and the value of Herba Dendrobii.
In emulsion process, the concept of oil phase substance and aqueous phase substance, is common practise to those skilled in the art.
(5) fill.
Get the packaging material that disinfect, with mastic automatic filling machine, the Herba Dendrobii facial film being up to the standards is carried out to fill, pouring process is controlled the loading amount of product, and overgauge is in 7.5%.
Because current Herba Dendrobii product is main mainly with taking orally, the Herba Dendrobii facial film in the present invention has been expanded the application of Herba Dendrobii, brings into play more fully its value.
Embodiment 2.
Referring to Fig. 1 to Fig. 2, the Herba Dendrobii facial film in the present embodiment comprises that parts by weight are the water of 65～68 parts; Parts by weight are the Herba Dendrobii extract after the filtration of 5～8 parts, in the Herba Dendrobii extract after this filtration, contain polysaccharide, chlorophyll, vitamin and protein; Parts by weight are the dipropylene glycol (DPG) of 8～11 parts; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 5～7 parts, and wherein, the weight ratio of polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 2:1:2; Parts by weight be 2～4 parts two-PEG-15 methyl ether polydimethylsiloxane; Parts by weight are the avenabeta glucosan of 5～7 parts; Parts by weight are the acrylic aldehyde/acrylic copolymer of 0.3～0.5 part; Parts by weight are the hydroxyethyl-cellulose of 0.1～0.2 part; Parts by weight are the triethanolamine of 0.1～0.2 part; Parts by weight are the butanediol, 1 of 0.2～0.3 part, 2-pentanediol and the benzoic mixture of para hydroxybenzene propionamido-, and this butanediol, 1,2-pentanediol and the benzoic weight ratio of para hydroxybenzene propionamido-are 3:2:1; Parts by weight are Cremophor RH40 and the propylene glycol of 0.15～0.25 part, and the weight ratio of this Cremophor RH40 and propylene glycol is 1:1; Parts by weight are the hyaluronate sodium of 0.2～0.4 part; Parts by weight are the allantoin of 0.2～0.4 part; Parts by weight are the EDETATE SODIUM of 0.04～0.06 part; Parts by weight are the IPBC (IPBC) of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC (IPBC) and dihydroxymethyl dimethyl hydantoin is 3:2.
Wherein, Herba Dendrobii extract after filtration is adopted with the following method and is made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, taking-up is placed in water cooling, then cut off, Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, the weight ratio of Herba Dendrobii and water is 1:6～1:8, start homogenizer and control discharge fineness below 200～300 μ m, obtain Herba Dendrobii extract, the Herba Dendrobii extract after Herba Dendrobii extract is filtered.
The scientific formulation of Herba Dendrobii facial film, reasonable in the present embodiment, between composition, can produce cooperative effect, the effect of polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract be can more effectively give play to, and polysaccharide, chlorophyll, vitamin and protein in skin absorption Herba Dendrobii extract have more been conducive to.
Below the consumption of each composition in Herba Dendrobii facial film of the present invention is illustrated again, referring to table three.
Table three
Remarks: each material amount used in table three is parts by weight; " title " hurdle ratio used is weight ratio.
In the present embodiment, the preparation method of Herba Dendrobii facial film comprises following operation successively:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming, this Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
B sterilization,
In 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, then rinses 2 times by purified water, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, takes out in rearmounted purified water cooling.
C cutting,
By Herba Dendrobii cutting;
B low temperature superfine grinding operation,
Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, and the weight ratio of Herba Dendrobii and water is 1:6～1:8, and for example the weight ratio of Herba Dendrobii and water can be 1:6,1:6.5,1:7,1:7.5,1:8,1:6.3,1:6.8,1:7.2,1:7.7 etc., start homogenizer and control discharge fineness below 200～300 μ m, obtain Herba Dendrobii extract.
C filter progress, in turn includes the following steps:
A coarse filtration step,
100 order nylon filtering cloths are soaked, be folded in 2 layers of funnel that is laid in vacuum filtration, edge is placed in outside funnel, open vacuum filtration machine, vacuum is greater than 0.07MPa, Herba Dendrobii extract is poured in funnel again, filtered the coarse filtration liquid obtaining, when filtering residue thickness reaches 0.5～1cm, cleaning once;
B fine straining step,
Start high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump is 150～250r/min, by feed pipe to coarse filtration liquid, Herba Dendrobii extract after being filtered after centrifugal filtration, contains polysaccharide, chlorophyll, vitamin and protein in the Herba Dendrobii extract after this filtration.Herba Dendrobii extract after filtering is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue once.
D emulsification process,
The oil phase of formula ratio is heated to 85 ℃, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 ℃, maintain 30min sterilizing, be cooled to 85 ℃; Oil phase is added to stirring and emulsifying in water and obtains base material; When the temperature of base material drops to 40～45 ℃, Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl hydantoin after filtering are added in base material, continue stirring and emulsifying 20min, with homogenizer, carry out emulsifying 5min again, within standing cooling 12～24 hours, become cream, stop stirring, cooling, obtains Herba Dendrobii facial film.
Oil phase comprises polymethyl acid glyceride, propylene glycol and Gantrez AN-119, two-PEG-15 methyl ether polydimethylsiloxane, acrylic aldehyde/acrylic copolymer, hydroxyethyl-cellulose, triethanolamine, and, butanediol/1,2-pentanediol/para hydroxybenzene propionamido-benzoic acid; Water comprises dipropylene glycol (DPG), avenabeta glucosan, propylene glycol, Cremophor RH40, hyaluronate sodium, allantoin and EDETATE SODIUM.
Formula ratio in the present invention refers to that parts by weight are the water of 65～68 parts; Parts by weight are the Herba Dendrobii extract after the filtration of 5～8 parts, in the Herba Dendrobii extract after this filtration, contain polysaccharide, chlorophyll, vitamin and protein; Parts by weight are the dipropylene glycol of 8～11 parts; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 5～7 parts, and wherein, the weight ratio of polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 2:1:2; Parts by weight be 2～4 parts two-PEG-15 methyl ether polydimethylsiloxane; Parts by weight are the avenabeta glucosan of 5～7 parts; Parts by weight are the acrylic aldehyde/acrylic copolymer of 0.3～0.5 part; Parts by weight are the hydroxyethyl-cellulose of 0.1～0.2 part; Parts by weight are the triethanolamine of 0.1～0.2 part; Parts by weight are the butanediol, 1 of 0.2～0.3 part, 2-pentanediol and the benzoic mixture of para hydroxybenzene propionamido-, and this butanediol, 1,2-pentanediol and the benzoic weight ratio of para hydroxybenzene propionamido-are 3:2:1; Parts by weight are Cremophor RH40 and the propylene glycol of 0.15～0.25 part, and the weight ratio of this Cremophor RH40 and propylene glycol is 1:1; Parts by weight are the hyaluronate sodium of 0.2～0.4 part; Parts by weight are the allantoin of 0.2～0.4 part; Parts by weight are the EDETATE SODIUM of 0.04～0.06 part; Parts by weight are the IPBC of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC and dihydroxymethyl dimethyl hydantoin is 3:2.
E fill operation,
Get the packaging material that disinfect, with mastic automatic filling machine, the Herba Dendrobii facial film being up to the standards is carried out to fill, pouring process is controlled the loading amount of product, and overgauge is in 7.5%.
The invention still further relates to a kind of Herba Dendrobii facial film being made by above-mentioned preparation method, adopt the Herba Dendrobii facial film that above-mentioned preparation method makes can be directly used on skin, the compositions such as the polysaccharide in Herba Dendrobii, chlorophyll, vitamin and protein can be absorbed by the body by skin, can be skin very abundant nutrition is provided, expand the application of Herba Dendrobii, brought into play more fully its value.
The course of processing of whole Herba Dendrobii extract in the present embodiment, except instantaneously sterilising, all at 30 ℃, complete below, even if in the course of processing of Herba Dendrobii facial film, its temperature is also controlled at below 45 ℃, has fully retained the various effective ingredient in Herba Dendrobii.The preparation method of this Herba Dendrobii facial film has retained the effective ingredient of Herba Dendrobii as much as possible, the iron-sheet dendrobe fresh product of take carries out low-temperature extraction as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, and polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are high; Adopt low-temperature extraction technology, Dendrobium officinale polysaccharide, dendrobine, aminoacid are at utmost extracted, protect the compositions such as Herba Dendrobii Determination of Chlorophyll, vitamin and organized enzyme to avoid high temperature simultaneously and destroy.
Although the present invention with embodiment openly as above; but it is not in order to limit protection scope of the present invention; any technical staff who is familiar with this technology, not departing from change and the retouching of doing in the spirit and scope of the present invention, all should belong to protection scope of the present invention.
Claims (10)
1. a Herba Dendrobii facial film, is characterized in that: this Herba Dendrobii facial film comprises that parts by weight are the water of 65～68 parts; Parts by weight are the Herba Dendrobii extract after the filtration of 5～8 parts, in the Herba Dendrobii extract after this filtration, contain polysaccharide, chlorophyll, vitamin and protein; Parts by weight are the dipropylene glycol of 8～11 parts; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 5～7 parts, and wherein, the weight ratio of polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 2:1:2; Parts by weight be 2～4 parts two-PEG-15 methyl ether polydimethylsiloxane; Parts by weight are the avenabeta glucosan of 5～7 parts; Parts by weight are the acrylic aldehyde/acrylic copolymer of 0.3～0.5 part; Parts by weight are the hydroxyethyl-cellulose of 0.1～0.2 part; Parts by weight are the triethanolamine of 0.1～0.2 part; Parts by weight are the butanediol, 1 of 0.2～0.3 part, 2-pentanediol and the benzoic mixture of para hydroxybenzene propionamido-, and this butanediol, 1,2-pentanediol and the benzoic weight ratio of para hydroxybenzene propionamido-are 3:2:1; Parts by weight are Cremophor RH40 and the propylene glycol of 0.15～0.25 part, and the weight ratio of this Cremophor RH40 and propylene glycol is 1:1; Parts by weight are the hyaluronate sodium of 0.2～0.4 part; Parts by weight are the allantoin of 0.2～0.4 part; Parts by weight are the EDETATE SODIUM of 0.04～0.06 part; Parts by weight are the IPBC of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC and dihydroxymethyl dimethyl hydantoin is 3:2.
2. Herba Dendrobii facial film according to claim 1, it is characterized in that: the Herba Dendrobii extract after described filtration is adopted with the following method and made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, taking-up is placed in water cooling, then cut off, Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, the weight ratio of Herba Dendrobii and water is 1:6～1:8, start homogenizer and control discharge fineness below 200～300 μ m, obtain Herba Dendrobii extract, Herba Dendrobii extract after Herba Dendrobii extract is filtered.
3. a preparation method for Herba Dendrobii facial film, is characterized in that: comprise successively following operation:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming;
B sterilization,
Fresh Herba Dendrobii after cleaning is placed in the boiling water 3～5min that sterilizes, take out be placed in water cooling;
C cutting,
By Herba Dendrobii cutting;
B low temperature superfine grinding operation,
Herba Dendrobii by the water of 2～10 ℃ of water temperatures and after cutting off is placed in homogenizer, and the weight ratio of Herba Dendrobii and water is 1:6～1:8, starts homogenizer and controls discharge fineness below 200～300 μ m, obtains Herba Dendrobii extract;
C filter progress,
Herba Dendrobii extract after Herba Dendrobii extract is filtered, contains polysaccharide, chlorophyll, vitamin and protein in the Herba Dendrobii extract after this filtration;
D emulsification process,
The oil phase of formula ratio is heated to 85 ℃, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 ℃, maintain 30min sterilizing, be cooled to 85 ℃; Oil phase is added to stirring and emulsifying in water and obtains base material; When the temperature of base material drops to 40～45 ℃, Herba Dendrobii extract, IPBC and dihydroxymethyl dimethyl hydantoin after filtering are added in base material, continue stirring and emulsifying 20min, with homogenizer, carry out emulsifying 5min again, within standing cooling 12～24 hours, become cream, stop stirring, cooling, obtains Herba Dendrobii facial film;
E fill operation,
Herba Dendrobii facial film is carried out to fill.
4. the preparation method of Herba Dendrobii facial film according to claim 3, is characterized in that: in a Herba Dendrobii ingredient requirement of described A pretreatment procedure, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
5. the preparation method of Herba Dendrobii facial film according to claim 3, it is characterized in that: in the b sterilization of described A pretreatment procedure, in 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, by purified water, rinse 2 times again, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, take out in rearmounted purified water cooling.
6. the preparation method of Herba Dendrobii facial film according to claim 3, is characterized in that: described C filter progress in turn includes the following steps:
A coarse filtration step,
100 order nylon filtering cloths are soaked, be folded in 2 layers of funnel that is laid in vacuum filtration, edge is placed in outside funnel, open vacuum filtration machine, vacuum is greater than 0.07MPa, Herba Dendrobii extract is poured in funnel again, filtered the coarse filtration liquid obtaining, when filtering residue thickness reaches 0.5～1cm, cleaning once;
B fine straining step,
Start high speed tube centrifuge and peristaltic pump, the rotating speed of high speed tube centrifuge is 15000r/min, the rotating speed of peristaltic pump is 150～250r/min, by feed pipe to coarse filtration liquid, Herba Dendrobii extract after being filtered after centrifugal filtration, Herba Dendrobii extract after filtering is placed in liquid medicine storage tank, and every centrifugal filtration 200～300L cleaning filtering residue once.
7. the preparation method of Herba Dendrobii facial film according to claim 3, it is characterized in that: in described D emulsification process, described oil phase comprises polymethyl acid glyceride, propylene glycol and Gantrez AN-119, two-PEG-15 methyl ether polydimethylsiloxane, acrylic aldehyde/acrylic copolymer, hydroxyethyl-cellulose, triethanolamine, and, butanediol/1,2-pentanediol/para hydroxybenzene propionamido-benzoic acid.
8. the preparation method of Herba Dendrobii facial film according to claim 3, it is characterized in that: in described D emulsification process, described water comprises dipropylene glycol, avenabeta glucosan, propylene glycol, Cremophor RH40, hyaluronate sodium, allantoin and EDETATE SODIUM.
9. the preparation method of Herba Dendrobii facial film according to claim 3, it is characterized in that: in described E fill operation, get the packaging material that disinfect, with mastic automatic filling machine, the Herba Dendrobii facial film being up to the standards is carried out to fill, pouring process is controlled the loading amount of product, and overgauge is in 7.5%.
10. a Herba Dendrobii facial film, is characterized in that: this Herba Dendrobii facial film adopts the preparation method as described in claim 3-9 to be prepared from.
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