CN103992117B - 陶瓷粉末及其制备方法 - Google Patents
陶瓷粉末及其制备方法 Download PDFInfo
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- CN103992117B CN103992117B CN201410054143.0A CN201410054143A CN103992117B CN 103992117 B CN103992117 B CN 103992117B CN 201410054143 A CN201410054143 A CN 201410054143A CN 103992117 B CN103992117 B CN 103992117B
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- oxide
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- 239000000843 powder Substances 0.000 title claims abstract description 74
- 239000000919 ceramic Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title 1
- 239000000463 material Substances 0.000 claims abstract description 61
- 238000000576 coating method Methods 0.000 claims abstract description 57
- 238000000034 method Methods 0.000 claims abstract description 53
- 239000011248 coating agent Substances 0.000 claims abstract description 49
- 239000002245 particle Substances 0.000 claims abstract description 47
- 230000003628 erosive effect Effects 0.000 claims abstract description 31
- 239000000203 mixture Substances 0.000 claims description 77
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 60
- UZLYXNNZYFBAQO-UHFFFAOYSA-N oxygen(2-);ytterbium(3+) Chemical compound [O-2].[O-2].[O-2].[Yb+3].[Yb+3] UZLYXNNZYFBAQO-UHFFFAOYSA-N 0.000 claims description 36
- 229910003454 ytterbium oxide Inorganic materials 0.000 claims description 36
- 229940075624 ytterbium oxide Drugs 0.000 claims description 36
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 claims description 34
- 239000012535 impurity Substances 0.000 claims description 22
- 239000002244 precipitate Substances 0.000 claims description 7
- FKTOIHSPIPYAPE-UHFFFAOYSA-N samarium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[Sm+3].[Sm+3] FKTOIHSPIPYAPE-UHFFFAOYSA-N 0.000 claims description 7
- 229910001954 samarium oxide Inorganic materials 0.000 claims description 6
- 238000000975 co-precipitation Methods 0.000 claims description 5
- 229940075630 samarium oxide Drugs 0.000 claims description 5
- 238000005229 chemical vapour deposition Methods 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 230000002441 reversible effect Effects 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 3
- 150000002739 metals Chemical class 0.000 claims description 3
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 229910001928 zirconium oxide Inorganic materials 0.000 claims description 3
- 239000012720 thermal barrier coating Substances 0.000 description 48
- 239000010410 layer Substances 0.000 description 25
- 239000007789 gas Substances 0.000 description 17
- 239000007921 spray Substances 0.000 description 17
- 229910001233 yttria-stabilized zirconia Inorganic materials 0.000 description 14
- 238000000151 deposition Methods 0.000 description 9
- 239000000758 substrate Substances 0.000 description 8
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 6
- 239000012071 phase Substances 0.000 description 6
- 230000007704 transition Effects 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 description 5
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 239000002131 composite material Substances 0.000 description 4
- 239000000446 fuel Substances 0.000 description 4
- 238000007750 plasma spraying Methods 0.000 description 4
- 229910001122 Mischmetal Inorganic materials 0.000 description 3
- 241000968352 Scandia <hydrozoan> Species 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 3
- 239000000292 calcium oxide Substances 0.000 description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 3
- 229910010293 ceramic material Inorganic materials 0.000 description 3
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 description 3
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 239000002019 doping agent Substances 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000000395 magnesium oxide Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- HJGMWXTVGKLUAQ-UHFFFAOYSA-N oxygen(2-);scandium(3+) Chemical compound [O-2].[O-2].[O-2].[Sc+3].[Sc+3] HJGMWXTVGKLUAQ-UHFFFAOYSA-N 0.000 description 3
- BPUBBGLMJRNUCC-UHFFFAOYSA-N oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ta+5] BPUBBGLMJRNUCC-UHFFFAOYSA-N 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- RUDFQVOCFDJEEF-UHFFFAOYSA-N yttrium(III) oxide Inorganic materials [O-2].[O-2].[O-2].[Y+3].[Y+3] RUDFQVOCFDJEEF-UHFFFAOYSA-N 0.000 description 3
- 229910000951 Aluminide Inorganic materials 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005328 electron beam physical vapour deposition Methods 0.000 description 2
- 229910000449 hafnium oxide Inorganic materials 0.000 description 2
- WIHZLLGSGQNAGK-UHFFFAOYSA-N hafnium(4+);oxygen(2-) Chemical compound [O-2].[O-2].[Hf+4] WIHZLLGSGQNAGK-UHFFFAOYSA-N 0.000 description 2
- 238000010286 high velocity air fuel Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000005240 physical vapour deposition Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910001936 tantalum oxide Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910021193 La 2 O 3 Inorganic materials 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 229920002873 Polyethylenimine Polymers 0.000 description 1
- 229910052772 Samarium Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000002547 anomalous effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 238000004299 exfoliation Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- CJNBYAVZURUTKZ-UHFFFAOYSA-N hafnium(iv) oxide Chemical compound O=[Hf]=O CJNBYAVZURUTKZ-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229910052746 lanthanum Inorganic materials 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000004901 spalling Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000005382 thermal cycling Methods 0.000 description 1
- 238000007751 thermal spraying Methods 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5436—Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01D—NON-POSITIVE DISPLACEMENT MACHINES OR ENGINES, e.g. STEAM TURBINES
- F01D5/00—Blades; Blade-carrying members; Heating, heat-insulating, cooling or antivibration means on the blades or the members
- F01D5/12—Blades
- F01D5/28—Selecting particular materials; Particular measures relating thereto; Measures against erosion or corrosion
- F01D5/288—Protective coatings for blades
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05D—INDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
- F05D2300/00—Materials; Properties thereof
- F05D2300/20—Oxide or non-oxide ceramics
- F05D2300/21—Oxide ceramics
- F05D2300/2118—Zirconium oxides
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05D—INDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
- F05D2300/00—Materials; Properties thereof
- F05D2300/60—Properties or characteristics given to material by treatment or manufacturing
- F05D2300/603—Composites; e.g. fibre-reinforced
- F05D2300/6033—Ceramic matrix composites [CMC]
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- Physics & Mathematics (AREA)
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- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Composite Materials (AREA)
- Thermal Sciences (AREA)
- Coating By Spraying Or Casting (AREA)
- Turbine Rotor Nozzle Sealing (AREA)
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- Chemical Vapour Deposition (AREA)
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Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/769538 | 2013-02-18 | ||
| US13/769,538 | 2013-02-18 | ||
| US13/769,538 US9139477B2 (en) | 2013-02-18 | 2013-02-18 | Ceramic powders and methods therefor |
Publications (2)
| Publication Number | Publication Date |
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| CN103992117A CN103992117A (zh) | 2014-08-20 |
| CN103992117B true CN103992117B (zh) | 2017-08-04 |
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| CN201410054143.0A Active CN103992117B (zh) | 2013-02-18 | 2014-02-18 | 陶瓷粉末及其制备方法 |
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| EP (1) | EP2767525B1 (cg-RX-API-DMAC7.html) |
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| US20160010471A1 (en) * | 2013-03-11 | 2016-01-14 | General Electric Company | Coating systems and methods therefor |
| JP2018040017A (ja) * | 2015-05-13 | 2018-03-15 | エリコンメテコジャパン株式会社 | 溶射用粉末、溶射方法及び溶射皮膜 |
| CA3002295A1 (en) * | 2017-06-21 | 2018-12-21 | Rolls-Royce Corporation | Impurity barrier layer for ceramic matrix composite substrate |
| US11976013B2 (en) | 2017-09-27 | 2024-05-07 | Rolls-Royce Corporation | Composite coating layer for ceramic matrix composite substrate |
| CN110304919A (zh) * | 2019-08-16 | 2019-10-08 | 湘潭大学 | 一种陶瓷材料的制备方法和热障涂层的制备方法 |
| CA3197043A1 (en) * | 2021-01-05 | 2022-07-14 | Oerlikon Metco (Us) Inc. | Thermally stable thermal barrier coatings that exhibit improved thermal conductivity and erosion resistance |
| US20220290285A1 (en) * | 2021-03-09 | 2022-09-15 | General Electric Company | High entropy ceramic thermal barrier coating |
| CN115341181B (zh) * | 2022-07-29 | 2024-04-09 | 中国航发北京航空材料研究院 | 一种镧钐锆氧热障涂层材料及其制备方法 |
| CN116082039B (zh) * | 2022-12-22 | 2023-10-20 | 哈尔滨工业大学 | 一种不等价离子掺杂的高发射率低热导功能复合陶瓷或涂层制备的方法 |
| CN119755672B (zh) * | 2024-12-30 | 2025-10-21 | 沈阳航空航天大学 | 一种具有点火功能的滑动弧等离子体-碰撞交叉结构的强化燃烧装置 |
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| CN1502663A (zh) * | 2002-11-22 | 2004-06-09 | г | 用于制造在高温下仍能耐热的绝热层的喷涂粉末 |
| US6756119B1 (en) * | 2003-04-07 | 2004-06-29 | Ensci Inc | Thin film metal oxyanion coated substrates |
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| JPS6141757A (ja) * | 1984-08-01 | 1986-02-28 | Hitachi Ltd | しや熱コ−テイング用ＺｒＯ２系粉末 |
| EP0705911B1 (en) | 1994-10-04 | 2001-12-05 | General Electric Company | Thermal barrier coating |
| US5897921A (en) | 1997-01-24 | 1999-04-27 | General Electric Company | Directionally solidified thermal barrier coating |
| US6047539A (en) | 1998-04-30 | 2000-04-11 | General Electric Company | Method of protecting gas turbine combustor components against water erosion and hot corrosion |
| US6306515B1 (en) | 1998-08-12 | 2001-10-23 | Siemens Westinghouse Power Corporation | Thermal barrier and overlay coating systems comprising composite metal/metal oxide bond coating layers |
| CA2431310C (en) | 2000-12-08 | 2009-11-24 | Sulzer Metco (Us) Inc. | Pre-alloyed stabilized zirconia powder and improved thermal barrier coating |
| US6893994B2 (en) | 2002-08-13 | 2005-05-17 | Saint-Gobain Ceramics & Plastics, Inc. | Plasma spheroidized ceramic powder |
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| US7255940B2 (en) | 2004-07-26 | 2007-08-14 | General Electric Company | Thermal barrier coatings with high fracture toughness underlayer for improved impact resistance |
| US7166373B2 (en) | 2004-08-19 | 2007-01-23 | General Electric Company | Ceramic compositions for thermal barrier coatings with improved mechanical properties |
| JP2006104577A (ja) | 2004-10-04 | 2006-04-20 | United Technol Corp <Utc> | セグメント化ガドリニアジルコニア被膜およびその形成方法、セグメント化セラミック被覆システムならびに被膜部品 |
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- 2013-02-18 US US13/769,538 patent/US9139477B2/en active Active
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| CN1502663A (zh) * | 2002-11-22 | 2004-06-09 | г | 用于制造在高温下仍能耐热的绝热层的喷涂粉末 |
| US6756119B1 (en) * | 2003-04-07 | 2004-06-29 | Ensci Inc | Thin film metal oxyanion coated substrates |
Also Published As
| Publication number | Publication date |
|---|---|
| US9139477B2 (en) | 2015-09-22 |
| US20140235426A1 (en) | 2014-08-21 |
| EP2767525A1 (en) | 2014-08-20 |
| EP2767525B1 (en) | 2020-08-26 |
| JP2014166949A (ja) | 2014-09-11 |
| CN103992117A (zh) | 2014-08-20 |
| JP6386740B2 (ja) | 2018-09-05 |
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