CN103958566B - 通过均相催化醇胺化提高聚亚烷基多胺的摩尔质量 - Google Patents

通过均相催化醇胺化提高聚亚烷基多胺的摩尔质量 Download PDF

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Publication number
CN103958566B
CN103958566B CN201280057850.4A CN201280057850A CN103958566B CN 103958566 B CN103958566 B CN 103958566B CN 201280057850 A CN201280057850 A CN 201280057850A CN 103958566 B CN103958566 B CN 103958566B
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reaction
water
catalyst
process according
solvent
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Chinese (zh)
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CN103958566A (zh
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J·斯特劳特曼
T·绍布
S·许弗
R·帕切洛
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/02—Polyamines
    • C08G73/0206—Polyalkylene(poly)amines
    • C08G73/0213—Preparatory process
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Paints Or Removers (AREA)
  • Adhesives Or Adhesive Processes (AREA)
CN201280057850.4A 2011-11-25 2012-11-19 通过均相催化醇胺化提高聚亚烷基多胺的摩尔质量 Expired - Fee Related CN103958566B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11190837.2 2011-11-25
EP11190837 2011-11-25
PCT/EP2012/072942 WO2013076023A1 (de) 2011-11-25 2012-11-19 Erhöhung der molaren masse von polyalkylenpolyaminen durch homogen-katalysierte alkohol-aminierung

Publications (2)

Publication Number Publication Date
CN103958566A CN103958566A (zh) 2014-07-30
CN103958566B true CN103958566B (zh) 2016-05-04

Family

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CN201280057850.4A Expired - Fee Related CN103958566B (zh) 2011-11-25 2012-11-19 通过均相催化醇胺化提高聚亚烷基多胺的摩尔质量

Country Status (8)

Country Link
US (1) US20140309460A1 (https=)
EP (1) EP2782947A1 (https=)
JP (1) JP6042446B2 (https=)
KR (1) KR20140098193A (https=)
CN (1) CN103958566B (https=)
BR (1) BR112014012580A2 (https=)
IN (1) IN2014CN03843A (https=)
WO (1) WO2013076023A1 (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6124911B2 (ja) * 2011-11-25 2017-05-10 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アルコールの均一系接触アミノ化による親油性ポリアルキレンポリアミン
JP6209169B2 (ja) 2012-02-20 2017-10-04 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ポリマーを用いた殺生物剤の抗微生物活性の増強
US8853400B2 (en) 2012-07-23 2014-10-07 Basf Se Process for the homogeneously catalyzed amination of alcohols with ammonia in the presence of a complex catalyst which comprises no anionic ligands
CN109996783A (zh) * 2016-11-30 2019-07-09 巴斯夫欧洲公司 使用mor骨架结构的铜改性沸石将单乙醇胺转化成乙二胺的方法
US11091425B2 (en) * 2016-11-30 2021-08-17 Basf Se Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst
CN108484451B (zh) * 2018-04-28 2020-05-19 华中科技大学 一种一锅法制备1,2-氨基醇类化合物的方法
GB202214770D0 (en) * 2022-10-07 2022-11-23 Sun Chemical Corp Primers for digital printing

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3708539A (en) 1970-02-06 1973-01-02 Union Oil Co Condensation of ammonia or a primary or secondary amine with an alcohol
JPS5316401B2 (https=) * 1974-06-11 1978-06-01
US4032480A (en) * 1975-07-11 1977-06-28 David Solomonovich Zhuk Method of producing linear polyethylenimine
EP0034480A3 (en) 1980-02-14 1982-01-13 Grigg, Ronald Ernest Alkylation of amines
CA1228449A (en) * 1982-04-30 1987-10-20 William B. Herdle Preparation of polyalkylene polyamines
US4888425A (en) * 1982-04-30 1989-12-19 Union Carbide Chemicals And Plastics Company Inc. Preparation of polyalkylene polyamines
US4745190A (en) 1984-07-25 1988-05-17 Air Products And Chemicals, Inc. Selective synthesis of substituted amines
EP0169547B1 (en) * 1984-07-25 1988-09-21 Air Products And Chemicals, Inc. Selective syntheses of substituted amines
IN172191B (https=) * 1985-03-14 1993-05-01 Lubrizol Corp
JP2971979B2 (ja) * 1991-05-24 1999-11-08 花王株式会社 線状ポリ第３級アミンの製造方法
US5637745A (en) * 1995-01-30 1997-06-10 Elf Atochem North America, Inc. Organometallic compounds and polymers made therefrom
JP2001122947A (ja) * 1999-10-28 2001-05-08 Tosoh Corp エポキシ樹脂用硬化促進剤及びそれを用いてなるエポキシ樹脂組成物
WO2009112379A1 (de) * 2008-03-04 2009-09-17 Basf Se Verwendung von alkoxylierten polyalkanolaminen zum spalten von öl-wasser-emulsionen
CN101786019B (zh) * 2010-02-26 2011-12-07 中国石油天然气股份有限公司 一种含环戊二烯基的过渡金属催化剂及其制备和应用
US8697834B2 (en) * 2010-05-31 2014-04-15 Basf Se Polyalkylenepolyamines by homogeneously catalyzed alcohol amination
US8877977B2 (en) * 2011-11-25 2014-11-04 Basf Se Synthesis of polyalkylenepolyamines having a low color index by homogeneously catalyzed alcohol amination in the presence of hydrogen
BR112014012568A2 (pt) * 2011-11-25 2017-06-06 Basf Se processo para a preparação de polialquileno poliaminas alcoxiladas, polialquileno poliamina alcoxilada, e, uso de polialquileno poliaminas alcoxiladas

Also Published As

Publication number Publication date
CN103958566A (zh) 2014-07-30
JP6042446B2 (ja) 2016-12-14
KR20140098193A (ko) 2014-08-07
JP2015505864A (ja) 2015-02-26
BR112014012580A2 (pt) 2017-06-06
WO2013076023A1 (de) 2013-05-30
EP2782947A1 (de) 2014-10-01
IN2014CN03843A (https=) 2015-09-04
US20140309460A1 (en) 2014-10-16

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