CN103881628B - The fire-retardant Flock Adhesive stick of decabromodiphynly oxide - Google Patents
The fire-retardant Flock Adhesive stick of decabromodiphynly oxide Download PDFInfo
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- CN103881628B CN103881628B CN201410104369.7A CN201410104369A CN103881628B CN 103881628 B CN103881628 B CN 103881628B CN 201410104369 A CN201410104369 A CN 201410104369A CN 103881628 B CN103881628 B CN 103881628B
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- decabromodiphynly oxide
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- 239000000853 adhesive Substances 0.000 title claims abstract description 20
- 230000001070 adhesive effect Effects 0.000 title claims abstract description 20
- 239000003063 flame retardant Substances 0.000 title claims abstract description 13
- 244000144992 flock Species 0.000 title claims abstract description 6
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims abstract description 20
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims abstract description 11
- GWZMWHWAWHPNHN-UHFFFAOYSA-N 2-hydroxypropyl prop-2-enoate Chemical compound CC(O)COC(=O)C=C GWZMWHWAWHPNHN-UHFFFAOYSA-N 0.000 claims abstract description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000004342 Benzoyl peroxide Substances 0.000 claims abstract description 10
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims abstract description 10
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims abstract description 10
- 235000019400 benzoyl peroxide Nutrition 0.000 claims abstract description 10
- XXBDWLFCJWSEKW-UHFFFAOYSA-N dimethylbenzylamine Chemical compound CN(C)CC1=CC=CC=C1 XXBDWLFCJWSEKW-UHFFFAOYSA-N 0.000 claims abstract description 10
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims abstract description 10
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000002360 preparation method Methods 0.000 claims description 7
- 239000011343 solid material Substances 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000003822 epoxy resin Substances 0.000 claims description 3
- 229920000647 polyepoxide Polymers 0.000 claims description 3
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 claims 2
- 239000004593 Epoxy Substances 0.000 abstract description 8
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 description 14
- 238000005516 engineering process Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- 239000003292 glue Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000004375 Dextrin Substances 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- 229920001800 Shellac Polymers 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 238000004026 adhesive bonding Methods 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000005060 rubber Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 2
- 239000004208 shellac Substances 0.000 description 2
- 229940113147 shellac Drugs 0.000 description 2
- 235000013874 shellac Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 239000004831 Hot glue Substances 0.000 description 1
- VHOQXEIFYTTXJU-UHFFFAOYSA-N Isobutylene-isoprene copolymer Chemical group CC(C)=C.CC(=C)C=C VHOQXEIFYTTXJU-UHFFFAOYSA-N 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- MSAVICZWFPQFPO-UHFFFAOYSA-N acetic acid;ethene Chemical group C=C.C=C.CC(O)=O MSAVICZWFPQFPO-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229920001038 ethylene copolymer Polymers 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Adhesives Or Adhesive Processes (AREA)
Abstract
The fire-retardant Flock Adhesive stick of decabromodiphynly oxide of the present invention, is characterized in that: it is filled a prescription by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N-methacrylic 16-20 part, E-S1 epoxy number fat 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms; Have raw material to be easy to get, cost is low, and environmental protection is easy to use, effective advantage.
Description
Technical field
The invention belongs to a kind of tackiness agent.
Background technology
Glued joint (bonding, bonding, cementing, gluing) and refer to the technology that homogeneity or heterogeneous body surface stick with glue agent and link together to there is stress distribution continuous, lightweight, or sealing, the features such as most technological temperature is low.Glued joint the connection being specially adapted to unlike material, different thickness, ultra-thin specification and complex component.Glued joint RECENT DEVELOPMENTS the fastest, application industry is extremely wide, and has great effect to high-and-new science and technology progress and people's daily life improvement.Therefore, study, all kinds of tackiness agent of development and production is very important.Tackiness agent (Bondingagent) is one of most important subsidiary material, applies very extensive in package handling.Tackiness agent is the sticking material of tool, the material that two kinds are separated can be linked together by its viscosity.The kind of tackiness agent is a lot.1. natural glue it be taken from the material of occurring in nature.Comprise the biological adhesives such as starch, protein, dextrin, gelatin, shellac, hide glue, rosin; Also the mineral binders such as pitch are comprised.2. artificial tackiness agent this be use made material, comprise the inorganic adhesives such as water glass, and the organic binder bond such as synthetic resins, synthetic rubber.Service performance divides 1. Watersoluble Adhesive to use water as the tackiness agent of solvent, mainly contains starch, dextrin, polyvinyl alcohol, carboxymethyl cellulose etc.2. Hotmelt Adhesive uses after making adhesive melts by heating, is a kind of solid binder.General thermoplastic resin all can use, as urethane, polystyrene, polyacrylic ester, ethene-acetate ethylene copolymer etc.3. Solvent Adhesive is water insoluble and be dissolved in the tackiness agent of certain solvent.As shellac, isoprene-isobutylene rubber etc.4. Emulsion Adhesive is many is suspension in water, as vinyl acetate resin, acrylic resin, chlorinated rubber etc.5. liquid non-solvent tackiness agent is at normal temperatures in thick liquid nano, as epoxy resin etc.Tackiness agent is the medium between label material and bonding substrates, plays link effect.Permanent and removable property two kinds can be divided into by its characteristic.It has multiple formulations, is applicable to different plane materiels and different occasions.Tackiness agent is the most important composition in adhesive material technology, is the key of label utilisation technology.Glued joint (bonding, bonding, cementing, gluing) and refer to the technology that homogeneity or heterogeneous body surface stick with glue agent and link together to there is stress distribution continuous, lightweight, or sealing, the features such as most technological temperature is low.Glued joint the connection being specially adapted to unlike material, different thickness, ultra-thin specification and complex component.Glued joint RECENT DEVELOPMENTS the fastest, application industry is extremely wide, and has great effect to high-and-new science and technology progress and people's daily life improvement.Therefore, study, all kinds of tackiness agent of development and production is very important.
Retrieve through Chinese publication, do not find the scheme identical with present patent application.
Summary of the invention:
The object of the invention is to; The fire-retardant Flock Adhesive stick of a kind of decabromodiphynly oxide is proposed.
The fire-retardant Flock Adhesive stick of decabromodiphynly oxide of the present invention, is characterized in that: it is filled a prescription by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N-methacrylic 16-20 part, E-S1 epoxy number fat 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms.
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N-methacrylic 16-20 part, E-S1 epoxy number fat 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Product of the present invention, can adapt to the use of various occasion, and bond strength reaches more than 2 times of prior art.
The present invention compared with prior art its beneficial effect is: have raw material and be easy to get, work simplification, is easy to manufacture, the advantages such as cost is low, environmental protection, easy to use, effective.
Embodiment:
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
Product of the present invention is raw materials used buys acquisition.
Embodiment 1
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N-methacrylic 16-20 part, E-S1 epoxy number fat 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Embodiment 2
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 525 parts, Propylene glycol monoacrylate 186 parts, ethyl propenoate 260 parts, 9 parts, vinylformic acid, N-methacrylic 16 parts, 190 parts, E-S1 epoxy number fat, benzoyl peroxide 11 parts, N, N-dimethyl benzylamine 11 parts, vinyl acetate 350 parts, decabromodiphynly oxide 9 parts, sodium polyacrylate 7 parts, 3 parts, Tai-Ace S 150 composition, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Embodiment 3
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 550 parts, Propylene glycol monoacrylate 210 parts, ethyl propenoate 300 parts, 15 parts, vinylformic acid, N-methacrylic 20 parts, 220 parts, E-S1 epoxy number fat, benzoyl peroxide 15 parts, N, N-dimethyl benzylamine 13 parts, vinyl acetate 380 parts, decabromodiphynly oxide 15 parts, sodium polyacrylate 12 parts, 5 parts, Tai-Ace S 150 composition, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Embodiment 4
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 525 parts, Propylene glycol monoacrylate 210 parts, ethyl propenoate 260 parts, 15 parts, vinylformic acid, N-methacrylic 16 parts, 220 parts, E-S1 epoxy number fat, benzoyl peroxide 11 parts, N, N-dimethyl benzylamine 13 parts, vinyl acetate 350 parts, decabromodiphynly oxide 9 parts, sodium polyacrylate 12 parts, 3 parts, Tai-Ace S 150 composition, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Embodiment 5
The fire-retardant flocking adhesive preparation method of decabromodiphynly oxide of the present invention, it is characterized in that: its formula by weight, by methyl acrylate 550 parts, Propylene glycol monoacrylate 186 parts, ethyl propenoate 300 parts, 9 parts, vinylformic acid, N-methacrylic 20 parts, 190 parts, E-S1 epoxy number fat, benzoyl peroxide 15 parts, N, N-dimethyl benzylamine 11 parts, vinyl acetate 380 parts, decabromodiphynly oxide 9 parts, sodium polyacrylate 12 parts, 3 parts, Tai-Ace S 150 composition, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Product specification of the present invention, quality: solid content more than 80%, its 1% solution pH value is 7.0-7.5; Viscosity 120-130 centipoise.
Claims (2)
1. the fire-retardant Flock Adhesive stick of decabromodiphynly oxide, is characterized in that: it is filled a prescription by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N methacrylamide 16-20 part, E-S1 epoxy resin 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms.
2. the fire-retardant flocking adhesive preparation method of decabromodiphynly oxide, it is characterized in that: its formula by weight, by methyl acrylate 525-550 part, Propylene glycol monoacrylate 186-210 part, ethyl propenoate 260-300 part, vinylformic acid 9-15 part, N methacrylamide 16-20 part, E-S1 epoxy resin 190-220 part, benzoyl peroxide 11-15 part, N, N-dimethyl benzylamine 11-13 part, vinyl acetate 350-380 part, decabromodiphynly oxide 9-15 part, sodium polyacrylate 7-12 part, Tai-Ace S 150 3-5 part forms, after solid materials ethanol is dissolved at 70-75 DEG C, be diluted to the ethanolic soln of 15%, whole material is added, at room temperature stirring reaction 12-22 hour, obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410104369.7A CN103881628B (en) | 2014-03-20 | 2014-03-20 | The fire-retardant Flock Adhesive stick of decabromodiphynly oxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410104369.7A CN103881628B (en) | 2014-03-20 | 2014-03-20 | The fire-retardant Flock Adhesive stick of decabromodiphynly oxide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103881628A CN103881628A (en) | 2014-06-25 |
| CN103881628B true CN103881628B (en) | 2016-03-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410104369.7A Active CN103881628B (en) | 2014-03-20 | 2014-03-20 | The fire-retardant Flock Adhesive stick of decabromodiphynly oxide |
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| Country | Link |
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| CN (1) | CN103881628B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109517404B (en) * | 2018-11-13 | 2021-04-13 | 大自然科技股份有限公司 | Adhesive for plant fiber sheet production and use method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1032617B1 (en) * | 1997-11-20 | 2003-05-28 | Lucent Technologies Inc. | Pressure-sensitive flame retardant adhesive |
| CN103525345A (en) * | 2013-10-10 | 2014-01-22 | 杨毅 | Flocking bonding agent |
| CN103525341A (en) * | 2013-10-10 | 2014-01-22 | 杨毅 | Acrylate bonding agent |
-
2014
- 2014-03-20 CN CN201410104369.7A patent/CN103881628B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1032617B1 (en) * | 1997-11-20 | 2003-05-28 | Lucent Technologies Inc. | Pressure-sensitive flame retardant adhesive |
| CN103525345A (en) * | 2013-10-10 | 2014-01-22 | 杨毅 | Flocking bonding agent |
| CN103525341A (en) * | 2013-10-10 | 2014-01-22 | 杨毅 | Acrylate bonding agent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103881628A (en) | 2014-06-25 |
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