CN103819898A - 一种碳纤维复合芯用耐高温氰酸酯树脂配方及其制备方法 - Google Patents
一种碳纤维复合芯用耐高温氰酸酯树脂配方及其制备方法 Download PDFInfo
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- CN103819898A CN103819898A CN201410063447.3A CN201410063447A CN103819898A CN 103819898 A CN103819898 A CN 103819898A CN 201410063447 A CN201410063447 A CN 201410063447A CN 103819898 A CN103819898 A CN 103819898A
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- cyanate ester
- ester resin
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- 229920005989 resin Polymers 0.000 title claims abstract description 111
- 239000011347 resin Substances 0.000 title claims abstract description 111
- 239000004643 cyanate ester Substances 0.000 title claims abstract description 71
- 229920000049 Carbon (fiber) Polymers 0.000 title claims abstract description 47
- 239000004917 carbon fiber Substances 0.000 title claims abstract description 47
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims description 9
- 239000007788 liquid Substances 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 18
- 239000011159 matrix material Substances 0.000 claims abstract description 11
- 229920001971 elastomer Polymers 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 239000005060 rubber Substances 0.000 claims abstract description 7
- 239000003054 catalyst Substances 0.000 claims abstract description 5
- 239000003292 glue Substances 0.000 claims description 20
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 claims description 19
- 239000004593 Epoxy Substances 0.000 claims description 16
- 239000000178 monomer Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 13
- 229920000459 Nitrile rubber Polymers 0.000 claims description 12
- -1 phenolic aldehyde Chemical class 0.000 claims description 12
- 229930185605 Bisphenol Natural products 0.000 claims description 11
- 238000012360 testing method Methods 0.000 claims description 9
- AHZMUXQJTGRNHT-UHFFFAOYSA-N [4-[2-(4-cyanatophenyl)propan-2-yl]phenyl] cyanate Chemical compound C=1C=C(OC#N)C=CC=1C(C)(C)C1=CC=C(OC#N)C=C1 AHZMUXQJTGRNHT-UHFFFAOYSA-N 0.000 claims description 8
- 238000002844 melting Methods 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- IGFHQQFPSIBGKE-UHFFFAOYSA-N 4-nonylphenol Chemical compound CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 claims description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 6
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 6
- 238000009472 formulation Methods 0.000 claims description 6
- 229910052723 transition metal Inorganic materials 0.000 claims description 6
- 108010010803 Gelatin Proteins 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 229920003986 novolac Polymers 0.000 claims description 5
- 239000000853 adhesive Substances 0.000 claims description 4
- 230000001070 adhesive effect Effects 0.000 claims description 4
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000011651 chromium Substances 0.000 claims description 4
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- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims description 3
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 claims description 2
- SYEWHONLFGZGLK-UHFFFAOYSA-N 2-[1,3-bis(oxiran-2-ylmethoxy)propan-2-yloxymethyl]oxirane Chemical compound C1OC1COCC(OCC1OC1)COCC1CO1 SYEWHONLFGZGLK-UHFFFAOYSA-N 0.000 claims description 2
- KUAUJXBLDYVELT-UHFFFAOYSA-N 2-[[2,2-dimethyl-3-(oxiran-2-ylmethoxy)propoxy]methyl]oxirane Chemical compound C1OC1COCC(C)(C)COCC1CO1 KUAUJXBLDYVELT-UHFFFAOYSA-N 0.000 claims description 2
- UUODQIKUTGWMPT-UHFFFAOYSA-N 2-fluoro-5-(trifluoromethyl)pyridine Chemical compound FC1=CC=C(C(F)(F)F)C=N1 UUODQIKUTGWMPT-UHFFFAOYSA-N 0.000 claims description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 2
- 239000005977 Ethylene Substances 0.000 claims description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 2
- 125000002723 alicyclic group Chemical group 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims description 2
- 239000010941 cobalt Substances 0.000 claims description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 230000003301 hydrolyzing effect Effects 0.000 claims description 2
- 229910052748 manganese Inorganic materials 0.000 claims description 2
- 238000005259 measurement Methods 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- 230000004048 modification Effects 0.000 claims description 2
- JAYXSROKFZAHRQ-UHFFFAOYSA-N n,n-bis(oxiran-2-ylmethyl)aniline Chemical compound C1OC1CN(C=1C=CC=CC=1)CC1CO1 JAYXSROKFZAHRQ-UHFFFAOYSA-N 0.000 claims description 2
- 125000005609 naphthenate group Chemical group 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 235000015598 salt intake Nutrition 0.000 claims description 2
- 238000005070 sampling Methods 0.000 claims description 2
- 239000004020 conductor Substances 0.000 abstract description 14
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000004034 viscosity adjusting agent Substances 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 description 14
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 14
- 239000002131 composite material Substances 0.000 description 14
- 238000006116 polymerization reaction Methods 0.000 description 10
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 5
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 4
- 238000007711 solidification Methods 0.000 description 4
- 230000008023 solidification Effects 0.000 description 4
- 230000007704 transition Effects 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- SZKXDURZBIICCF-UHFFFAOYSA-N cobalt;pentane-2,4-dione Chemical compound [Co].CC(=O)CC(C)=O SZKXDURZBIICCF-UHFFFAOYSA-N 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 230000007774 longterm Effects 0.000 description 3
- 238000010008 shearing Methods 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N SnO2 Inorganic materials O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- IJXOTFQNCKFWBH-UHFFFAOYSA-N cyanic acid;phenol Chemical compound OC#N.OC1=CC=CC=C1.OC1=CC=CC=C1 IJXOTFQNCKFWBH-UHFFFAOYSA-N 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 230000009970 fire resistant effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 230000003014 reinforcing effect Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- RCXHRHWRRACBTK-UHFFFAOYSA-N 3-(oxiran-2-ylmethoxy)propane-1,2-diol Chemical compound OCC(O)COCC1CO1 RCXHRHWRRACBTK-UHFFFAOYSA-N 0.000 description 1
- YBRVSVVVWCFQMG-UHFFFAOYSA-N 4,4'-diaminodiphenylmethane Chemical compound C1=CC(N)=CC=C1CC1=CC=C(N)C=C1 YBRVSVVVWCFQMG-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
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- 235000011187 glycerol Nutrition 0.000 description 1
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- VYKXQOYUCMREIS-UHFFFAOYSA-N methylhexahydrophthalic anhydride Chemical compound C1CCCC2C(=O)OC(=O)C21C VYKXQOYUCMREIS-UHFFFAOYSA-N 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
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- 238000007493 shaping process Methods 0.000 description 1
- JBQYATWDVHIOAR-UHFFFAOYSA-N tellanylidenegermanium Chemical compound [Te]=[Ge] JBQYATWDVHIOAR-UHFFFAOYSA-N 0.000 description 1
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
- C08L79/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/20—Applications use in electrical or conductive gadgets
- C08L2203/202—Applications use in electrical or conductive gadgets use in electrical wires or wirecoating
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Reinforced Plastic Materials (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Abstract
Description
Claims (7)
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CN201410063447.3A CN103819898B (zh) | 2014-02-25 | 2014-02-25 | 一种碳纤维复合芯用耐高温氰酸酯树脂配方及其制备方法 |
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CN201410063447.3A CN103819898B (zh) | 2014-02-25 | 2014-02-25 | 一种碳纤维复合芯用耐高温氰酸酯树脂配方及其制备方法 |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104575825A (zh) * | 2014-12-29 | 2015-04-29 | 江苏亨通电力特种导线有限公司 | 架空电力传输用铝型绞线 |
CN105694453A (zh) * | 2016-03-21 | 2016-06-22 | 航天材料及工艺研究所 | 一种邻苯二甲腈复合材料电缆罩及其制备方法 |
CN107001628A (zh) * | 2014-06-06 | 2017-08-01 | 通用电气公司 | 用于电机的可固化组合物和相关方法 |
CN108122639A (zh) * | 2016-11-29 | 2018-06-05 | 江苏河阳电气有限公司 | 一种碳纤维耐超高温电缆及其制备方法 |
CN108122631A (zh) * | 2016-11-29 | 2018-06-05 | 江苏河阳电气有限公司 | 一种防弹丝超耐磨电缆及其制备方法 |
CN108314991A (zh) * | 2018-02-12 | 2018-07-24 | 成都理工大学 | 一种耐180℃高温胶粘剂及其制备方法 |
Citations (2)
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CN1467244A (zh) * | 2003-03-07 | 2004-01-14 | 梁国正 | 用于氰酸酯树脂固化反应中的有机锡化合物及其制备方法 |
CN102030985A (zh) * | 2010-09-30 | 2011-04-27 | 长安大学 | 一种碳纤维增强氰酸酯树脂基复合材料的制备方法 |
-
2014
- 2014-02-25 CN CN201410063447.3A patent/CN103819898B/zh active Active
Patent Citations (2)
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CN1467244A (zh) * | 2003-03-07 | 2004-01-14 | 梁国正 | 用于氰酸酯树脂固化反应中的有机锡化合物及其制备方法 |
CN102030985A (zh) * | 2010-09-30 | 2011-04-27 | 长安大学 | 一种碳纤维增强氰酸酯树脂基复合材料的制备方法 |
Non-Patent Citations (3)
Title |
---|
任鹏刚,梁国正: "高模量碳纤维增强改性氰酸酯树脂基复合材料研究", 《宇航材料工艺》 * |
任鹏刚等: "氰酸酯树脂及其碳纤维复合材料研究", 《中国塑料》 * |
任鹏刚等: "氰酸酯树脂及其碳纤维复合材料研究", 《中国塑料》, vol. 18, no. 5, 31 May 2004 (2004-05-31) * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107001628A (zh) * | 2014-06-06 | 2017-08-01 | 通用电气公司 | 用于电机的可固化组合物和相关方法 |
US10370569B2 (en) | 2014-06-06 | 2019-08-06 | General Electric Company | Composition for bonding windings or core laminates in an electrical machine, and associated method |
CN107001628B (zh) * | 2014-06-06 | 2020-01-07 | 通用电气公司 | 用于电机的可固化组合物和相关方法 |
CN104575825A (zh) * | 2014-12-29 | 2015-04-29 | 江苏亨通电力特种导线有限公司 | 架空电力传输用铝型绞线 |
CN105694453A (zh) * | 2016-03-21 | 2016-06-22 | 航天材料及工艺研究所 | 一种邻苯二甲腈复合材料电缆罩及其制备方法 |
CN105694453B (zh) * | 2016-03-21 | 2017-11-07 | 航天材料及工艺研究所 | 一种邻苯二甲腈复合材料电缆罩及其制备方法 |
CN108122639A (zh) * | 2016-11-29 | 2018-06-05 | 江苏河阳电气有限公司 | 一种碳纤维耐超高温电缆及其制备方法 |
CN108122631A (zh) * | 2016-11-29 | 2018-06-05 | 江苏河阳电气有限公司 | 一种防弹丝超耐磨电缆及其制备方法 |
CN108314991A (zh) * | 2018-02-12 | 2018-07-24 | 成都理工大学 | 一种耐180℃高温胶粘剂及其制备方法 |
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Inventor after: Wang Zhaohua Inventor after: Cheng Ran Inventor after: Liang Hongping Inventor before: Wang Zhaohua Inventor before: Die Qiuping |
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Effective date of registration: 20200511 Address after: 430100 No.61, Changlu street, Zhashan street, Caidian economic and Technological Development Zone, Wuhan City, Hubei Province Patentee after: Wuhan Cable Co.,Ltd. Address before: 430035 Hubei Province in Qiaokou District of Wuhan city Gutian Road No. 2 Patentee before: AEROSPACE ELECTRIC GROUP Co.,Ltd. |
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