CN103816092A - Traditional Chinese medicine extractive for washing hair as well as preparation method and raw material composition thereof - Google Patents

Traditional Chinese medicine extractive for washing hair as well as preparation method and raw material composition thereof Download PDF

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CN103816092A
CN103816092A CN201410100506.XA CN201410100506A CN103816092A CN 103816092 A CN103816092 A CN 103816092A CN 201410100506 A CN201410100506 A CN 201410100506A CN 103816092 A CN103816092 A CN 103816092A
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chinese medicine
radix
medicine extract
cortex
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CN103816092B (en
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李建华
肖蕾
陈宇
陈刚
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Infinitus China Co Ltd
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Abstract

The invention discloses a traditional Chinese medicine extractive for washing hair as well as a preparation method and a raw material composition thereof. The invention discloses the raw material composition of the traditional Chinese medicine extractive for washing hair, and the raw material composition consists of the following components in parts by weight: 1-5 parts of angelica sinensis, 1-30 parts of radix sophorae flavescentis, 5-15 parts of coptis chinensis, 5-15 parts of scutellaria baicalensis, 1-30 parts of fructus cnidii, 1-3 parts of fructus viticis, 1-5 parts of the root bark of white mulberry, 1-5 parts of ligusticum wallichii, 0.5-20 parts of radix stemonae, 0.5-20 parts of cortex dictamni and 1-5 parts of golden cypress. The traditional Chinese medicine extractive disclosed by the invention can be used for preparing daily chemical products such as liquid shampoo, paste shampoo and a hair conditioner, and achieving the excellent effects of inhibiting bacterium, eliminating dandruff and relieving itching.

Description

A kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash
Technical field
The present invention relates to a kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash.
Background technology
Along with growth in the living standard, health perception universal, the hair washing frequency of Chinese Urban Residents also starts more and more to approach developed country's level now, reaches 3~3.5 times/week.But want real and correct healthy philosophy of life to integrate with, it is far from being enough increasing simply hair washing number of times, we need to be appreciated that and how scientifically remove hair washing, hair care.In the environment that we depend on for existence at present, pollution follows industrialization development to reach unprecedented serious, dust, ultraviolet, chemicals and various microorganism (antibacterial, mycete/yeast) are not being attacked our hair all the time, bring out multiple class problem, as the dandruff, scalp are itched, hair bifurcated, hair be withered etc.
Dandruff is one of subject matter of puzzlement modern hair, and the principal element that dandruff produces is the breeding that occurs abnormal and pityrosporum furfur (chlosma) of head metabolism, grows.Find according to the research of China's Healthy Education Associations scalp health research center, owing to not noting skin of head health care, bad hygienic habit and lacking necessary anti-dandruff hair care knowledge, in the middle of Chinese adult, there is the male consumer of 59% female consumer and 63% to be all subject to the puzzlement of dandruff always.The common shampoo of simple use is had one's hair wash, and can clean at most dirt and temporarily take away the dandruff on hair top layer, but can not be really from basic solution dandruff problem.
Summary of the invention
Technical problem to be solved by this invention has been to provide a kind of and diverse Chinese medicine extract, its preparation method and the feedstock composition thereof for having one's hair wash of prior art.Chinese medicine extract of the present invention can be used for preparing the cosmeticses of everyday use such as shampoo, hair cream, hair conditioner, can reach the effect of excellent antibacterial, removing scurf and relieving itching.
The invention provides a kind of feedstock composition for the Chinese medicine extract of having one's hair wash, it is made up of following ingredients: Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1~5 part, Radix Sophorae Flavescentis is 1~30 part, and Rhizoma Coptidis is 5~15 parts, Radix Scutellariae is 5~15 parts, and Fructus Cnidii is 1~30 part, and Fructus Viticis is 1~3 part, and Cortex Mori is 1~5 part, Rhizoma Chuanxiong is 1~5 part, and the Radix Stemonae is 0.5~20 part, and Cortex Dictamni is 0.5~20 part, and Cortex Phellodendri is 1~5 part; Above umber is parts by weight.
Preferably, the described feedstock composition for the Chinese medicine extract of having one's hair wash: when being classified as 2~4 parts, Radix Sophorae Flavescentis is 2~4 parts, and Rhizoma Coptidis is 7~13 parts, Radix Scutellariae is 9~13 parts, Fructus Cnidii is 3~15 parts, and Fructus Viticis is 1~2 part, and Cortex Mori is 1~3 part, Rhizoma Chuanxiong is 2~3 parts, the Radix Stemonae is 3~15 parts, and Cortex Dictamni is 1~13 part, and Cortex Phellodendri is 1~3 part; Above umber is parts by weight.
Better, the described feedstock composition for the Chinese medicine extract of having one's hair wash: when being classified as 2~3 parts, Radix Sophorae Flavescentis is 3~4 parts, and Rhizoma Coptidis is 8~11 parts, Radix Scutellariae is 10~11 parts, Fructus Cnidii is 4~6 parts, and Fructus Viticis is 1~2 part, and Cortex Mori is 1~2 part, Rhizoma Chuanxiong is 3 parts, the Radix Stemonae is 5~8 parts, and Cortex Dictamni is 5~8 parts, and Cortex Phellodendri is 1~2 part; Above umber is parts by weight.
In the present invention, the described feedstock composition for the Chinese medicine extract of having one's hair wash is the formula for the preparation of described Chinese medicine.As required, the feedstock composition for the Chinese medicine extract of having one's hair wash of the present invention can be the component form that all the components mixes, and also can be each composition independent or each composition is divided into many components nested form of some groups.
In the present invention, the described Chinese medicine extract for having one's hair wash can make by the method for preparing Chinese medicine extract of this area routine.
The present invention also provides the above-mentioned preparation method for the Chinese medicine extract of having one's hair wash, it comprises the following step: the above-mentioned ethanol water for the feedstock composition of Chinese medicine extract of having one's hair wash and the percent by volume 60%~90% of 3~6 times of weight is mixed, reflux 1~3 hour, filter, obtain filtrate; The continuation of gained filtering residue is mixed and refluxed 1~3 time with the ethanol water of the percent by volume 60%~90% of 3~6 times of weight, each 1~3 hour, obtain filtrate; Merge above-mentioned all filtrate, be concentrated into relative density and be 1.2~1.25(60 ℃ record), obtain extractum.
The Chinese medicine extract for having one's hair wash that the present invention also provides above-mentioned preparation method to make.
As required, Chinese medicine extract of the present invention can mix with the adjuvant for the preparation of hair washing product of this area routine, makes the various product forms such as shampoo, hair cream or hair conditioner.For example, above-mentioned Chinese medicine extract can be added in conventional shampoo formula, is prepared into shampoo; Wherein each composition consumption is conventional amount used.
The feature of Chinese herbal medicine extract of the present invention is take natural Chinese medicinal herb as primary raw material, utilizes various composition reasonable combination, Synergistic, reaches effect antibacterial, removing scurf and relieving itching by number of ways.This extract, by conventional machining technique, can be widely used in the products such as shampoo, hair cream, hair conditioner, can effectively suppress dandruff and produce, alleviates the symptoms such as scalp is itched, hair is withered.This extract, by Traditional Chinese medical theory and the effective combination of modern medicine study achievement, is followed " endogenous cause of ill ", " exopathogenic factor " principle simultaneously, reaches inside and outside effect of minoring, for comprehensively, thoroughly solving dandruff, head pruritus problem provides a referential approach.
Without prejudice to the field on the basis of common sense, above-mentioned each optimum condition, can combination in any, obtains the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material be commercially available obtaining all.
Positive progressive effect of the present invention is: Chinese medicine extract of the present invention can be used for preparing the cosmeticses of everyday use such as shampoo, hair cream, hair conditioner, can reach the effect of excellent antibacterial, removing scurf and relieving itching, for comprehensively, thoroughly solving dandruff, head pruritus problem provides a referential approach.
The specific embodiment
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, according to conventional method and condition, or selects according to catalogue.
Preparation Example 1~6
The preparation of embodiment 1 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1 part, Radix Sophorae Flavescentis is 1 part, and Rhizoma Coptidis is 5 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 1 part, 1 part of Fructus Viticis, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 1 part, and the Radix Stemonae is 0.5 part, and Cortex Dictamni is 0.5 part, Cortex Phellodendri is 1 part; Above umber is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mixes with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 1 hour with the ethanol water of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 ℃ record), obtain extractum.
The preparation of embodiment 2 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 5 parts, Radix Sophorae Flavescentis is 30 parts, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 15 parts, and Fructus Cnidii is 30 parts, and Fructus Viticis is 3 parts, and Cortex Mori is 5 parts, and Rhizoma Chuanxiong is 5 parts, 20 parts of Radix Stemonae positions, and Cortex Dictamni is 20 parts, Cortex Phellodendri is 5 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
1Kg altogether after claiming above-mentioned raw materials press umber to mix, mixes with the ethanol water of the percent by volume 90% of 6Kg, refluxes 3 hours, and filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 3 times with the ethanol water of the percent by volume 90% of 6 times of weight of filtering residue, each 3 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 ℃ record), obtain extractum.
The preparation of embodiment 3 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 2 parts, Radix Sophorae Flavescentis is 2 parts, and Rhizoma Coptidis is 7 parts, and Radix Scutellariae is 9 parts, and Fructus Cnidii is 3 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 2 parts, and the Radix Stemonae is 3 parts, and Cortex Dictamni is 1 part, and Cortex Phellodendri is 1 part; Above umber is parts by weight;
Concrete preparation process is as follows:
1Kg altogether after claiming above-mentioned raw materials press umber to mix, mixes with the ethanol water of the percent by volume 75% of 4.5Kg, refluxes 2 hours, and filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 2 times with the ethanol water of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 ℃ record), obtain extractum.
The preparation of embodiment 4 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 4 parts, Radix Sophorae Flavescentis is 4 parts, and Rhizoma Coptidis is 13 parts, and Radix Scutellariae is 13 parts, and Fructus Cnidii is 15 parts, and Fructus Viticis is 2 parts, and Cortex Mori is 3 parts, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 15 parts, and Cortex Dictamni is 13 parts, and Cortex Phellodendri is 3 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
1Kg altogether after claiming above-mentioned raw materials press umber to mix, mixes with the ethanol water of the percent by volume 75% of 4.5Kg, refluxes 2 hours, and filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 2 times with the ethanol water of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 ℃ record), obtain extractum.
The preparation of embodiment 5 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 2 parts, Radix Sophorae Flavescentis is 3 parts, and Rhizoma Coptidis is 8 parts, and Radix Scutellariae is 10 parts, and Fructus Cnidii is 4 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 5 parts, and Cortex Dictamni is 5 parts, and Cortex Phellodendri is 1 part; Above umber is parts by weight;
Concrete preparation process is as follows:
1Kg altogether after claiming above-mentioned raw materials press umber to mix, mixes with the ethanol water of the percent by volume 75% of 4.5Kg, refluxes 2 hours, and filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 2 times with the ethanol water of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 ℃ record), obtain extractum.
The preparation of embodiment 6 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 3 parts, Radix Sophorae Flavescentis is 4 parts, and Rhizoma Coptidis is 11 parts, and Radix Scutellariae is 11 parts, and Fructus Cnidii is 6 parts, and Fructus Viticis is 2 parts, and Cortex Mori is 2 parts, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 8 parts, and Cortex Dictamni is 8 parts, and Cortex Phellodendri is 2 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
1Kg altogether after claiming above-mentioned raw materials press umber to mix, mixes with the ethanol water of the percent by volume 75% of 4.5Kg, refluxes 2 hours, and filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 2 times with the ethanol water of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 ℃ record), obtain extractum.
The preparation of comparative example's 1 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 35 parts, and Rhizoma Coptidis is 2 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 5 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 2 parts, and the Radix Stemonae is 23 parts, and Cortex Dictamni is 22 parts, and Cortex Phellodendri is 6 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mixes with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 1 hour with the ethanol water of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 ℃ record), obtain extractum.
The preparation of comparative example's 2 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis and Cortex Mori; Wherein, when being classified as 1 part, Radix Sophorae Flavescentis is 1 part, and Rhizoma Coptidis is 5 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 2 parts, and Cortex Mori is 2 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mixes with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 1 hour with the ethanol water of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 ℃ record), obtain extractum.
The preparation of comparative example's 3 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 0.5 part, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 3 parts, and Fructus Cnidii is 4 parts, 5 parts of Fructus Viticises, and Cortex Mori is 6 parts, and Rhizoma Chuanxiong is 7 parts, and the Radix Stemonae is 0.3 part, and Cortex Dictamni is 22 parts, Cortex Phellodendri is 1 part; Above umber is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mixes with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 1 hour with the ethanol water of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 ℃ record), obtain extractum.
The preparation of comparative example's 4 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 33 parts, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 17 parts, and Fructus Cnidii is 0.5 part, 5 parts of Fructus Viticises, and Cortex Mori is 6 parts, and Rhizoma Chuanxiong is 0.5 part, and the Radix Stemonae is 0.2 part, and Cortex Dictamni is 0.2 part, Cortex Phellodendri is 6 parts; Above umber is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mixes with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filtration, obtains filtrate; The continuation of gained filtering residue is mixed and refluxed 1 hour with the ethanol water of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 ℃ record), obtain extractum.
Fungistatic effect embodiment
1, test specimen
By above-described embodiment 1~6, and the Chinese medicine extract that comparative example 1~4 makes adds to respectively in the commercially available shampoo of a routine, and this shampoo formula is as follows:
Figure BDA0000478313460000081
The weight ratio of Chinese medicine extract and this shampoo is 0.2%, and mix homogeneously is numbered respectively A, B, C, D, E, F(embodiment 1~6), H, I, J, K(comparative example 1~4); BW is the well-known Chinese herbal medicine concept dandruff control shampoo containing of selling on market;
Above-mentioned conventional shampoo is numbered G, does not add the blank shampoo of Chinese medicine extract of the present invention.
2, test index
Inhibition zone diameter (mm); Minimum inhibitory concentration (MIC, %);
3, result of the test
3.1 broad spectrum activity bacteriostatic test results
Figure BDA0000478313460000082
Figure BDA0000478313460000091
Figure BDA0000478313460000101
Note: D value * is the inhibition zone diameter sum to three kinds of strain subjects, and antibacterial bacterial concentration is about 5.0 × 10 7cfu/ml, mycete and yeast liquid concentration are about 3.5 × 10 6cfu/ml.
Known according to test data, except G, other 7 kinds of shampoos are to all comparatively responsive (D > 27.0) of strain subject, and wherein the fungistatic effect of E, F is best.
3.2 feature bacterium bacteriostatic test results
Figure BDA0000478313460000111
Note: the activity of chlosma bacterium liquid is about 4.0 × 10 5cfu/ml.
Known according to test data, 7 kinds of shampoos of the present invention and BW all have certain inhibitory action to strain subject, and the fungistatic effect that has wherein added the shampoo of Chinese medicine extract of the present invention is obviously better than un-added shampoo G, and H, I, J, K.
Human efficiency's effect embodiment
For shampoo sample A, B, C, D, E, F, G and BW in above-mentioned fungistatic effect embodiment, applicant has carried out human body antidandruff effect demonstration test, and result of the test is as follows:
1. experiment material
1.1 test specimen
Totally 8 kinds of shampoos, are numbered A, B, C, D, E, F, G and BW(the same).
1.2 subjects
Inclusive criteria is: the non-pathologic dandruff phenomenon of medium or medium above degree, left and right sides dandruff gradient of infection is roughly the same.
1.3 test numbers
Choose altogether 26 volunteers and test, be divided into 2 groups, actual completing number 20 people, wherein male 10 people, female 10 people, 20~50 years old age.
2. experimental design and method
2.1 objective image analyses
Respectively the right and left dandruff is combed to glass plate according to the operation sequence of standard, then covered with the onesize glass plate of another piece, seal and preserve.In 14 days, glass plate is carried out to graphical analysis.
Under cold light source lighting condition, under black background, gather glass plate image with monochromatic CCD camera and also preserve.By analysis software, picture is analyzed, calculated the area percentage (%) of dandruff.
2.2 subjective assessment dandruff amounts
Technical staff marks to the dandruff amount of the right and left respectively according to standards of grading:
0 ... without dandruff; 1 ... fragmentary dandruff; 2 ... a small amount of dandruff; 3 ... moderate dandruff; 4 ... a large amount of dandruffs.
2.3 adaptation of product evaluations
Technical staff and volunteer carry out respectively the Adaptability Evaluation of product to the right and left, Adaptability Evaluation parameter comprises the rubescent situation of scalp, scalp itch and burn feeling, and wherein the rubescent situation of scalp is evaluated by technical staff; Scalp itch, burn feeling are evaluated by volunteer.
Scalp is rubescent, scalp itch, burn feeling situation grading standard:
0 ... nothing; 1 ... slightly; 2 ... medium; 3 ... seriously; 4 ... very serious.
3. experimental result
3.1 objective image analyses
Objective image analytical data is as follows:
Wherein, average is that 20 samples continue to use after different shampoo that (frequency, consumption are identical.Frequency is to use once every day), at the average area percentage ratio (%) of the dandruff of different time.
Figure BDA0000478313460000121
From analytical data on the whole, BW group reduces with the increase of service time substantially with A~F group dandruff amount.Product uses the later stage (the 14th day) compared with use early stage (the 0th day), and the dandruff amount of A group~F group shows as significance and reduces; The dandruff amount of BW group is on a declining curve, but there was no significant difference, G group dandruff amount declines slowly.
3.2 subjective assessment
Subjective analysis data are as follows:
Wherein, average is that 20 samples continue to use after different shampoo that (frequency, consumption are identical.Frequency is to use once every day), in the scoring of different time.
Figure BDA0000478313460000131
From subjective data entirety, BW group reduces with the increase of service time substantially with A~F group dandruff amount.Product uses the later stage (the 14th day) compared with use early stage (the 0th day), and the dandruff amount of A group~F group shows as significance and reduces; The dandruff amount of BW group is on a declining curve, but there was no significant difference, G group dandruff amount declines slowly.
3.3 adaptation of product evaluations
Adaptability Evaluation data are as follows:
Wherein, meansigma methods is that 20 samples continue to use after different shampoo that (frequency, consumption are identical.Frequency is to use once every day), mark at different time.
Rubescent and the burning sensation result of scalp itch, scalp
The situation such as rubescent and burn feeling for scalp itch, scalp, all shows mitigation largely after using BW group and A~F group, and G group alleviation degree is poor.
4. brief summary
Use after shampoo A~F group a period of time, by objective analysis and subjective assessment, dandruff amount is all trend of obvious reduced, and to scalp itch, scalp, the situation such as rubescent and burn feeling also has mitigation to a certain degree.

Claims (5)

1. for a feedstock composition for the Chinese medicine extract of having one's hair wash, it is characterized in that: it is made up of following ingredients: Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1~5 part, Radix Sophorae Flavescentis is 1~30 part, and Rhizoma Coptidis is 5~15 parts, Radix Scutellariae is 5~15 parts, and Fructus Cnidii is 1~30 part, and Fructus Viticis is 1~3 part, and Cortex Mori is 1~5 part, Rhizoma Chuanxiong is 1~5 part, and the Radix Stemonae is 0.5~20 part, and Cortex Dictamni is 0.5~20 part, and Cortex Phellodendri is 1~5 part; Above umber is parts by weight.
2. the feedstock composition for the Chinese medicine extract of having one's hair wash as claimed in claim 1, it is characterized in that: the described feedstock composition for the Chinese medicine extract of having one's hair wash: when being classified as 2~4 parts, Radix Sophorae Flavescentis is 2~4 parts, and Rhizoma Coptidis is 7~13 parts, Radix Scutellariae is 9~13 parts, Fructus Cnidii is 3~15 parts, and Fructus Viticis is 1~2 part, and Cortex Mori is 1~3 part, Rhizoma Chuanxiong is 2~3 parts, the Radix Stemonae is 3~15 parts, and Cortex Dictamni is 1~13 part, and Cortex Phellodendri is 1~3 part; Above umber is parts by weight.
3. the feedstock composition for the Chinese medicine extract of having one's hair wash as claimed in claim 2, it is characterized in that: the described feedstock composition for the Chinese medicine extract of having one's hair wash: when being classified as 2~3 parts, Radix Sophorae Flavescentis is 3~4 parts, and Rhizoma Coptidis is 8~11 parts, Radix Scutellariae is 10~11 parts, Fructus Cnidii is 4~6 parts, and Fructus Viticis is 1~2 part, and Cortex Mori is 1~2 part, Rhizoma Chuanxiong is 3 parts, the Radix Stemonae is 5~8 parts, and Cortex Dictamni is 5~8 parts, and Cortex Phellodendri is 1~2 part; Above umber is parts by weight.
4. the preparation method for the Chinese medicine extract of having one's hair wash, it is characterized in that comprising the following step: the ethanol water for the feedstock composition of Chinese medicine extract of having one's hair wash and the percent by volume 60%~90% of 3~6 times of weight described in claim 1~3 any one is mixed, reflux 1~3 hour, filter, obtain filtrate; The continuation of gained filtering residue is mixed and refluxed 1~3 time with the ethanol water of the percent by volume 60%~90% of 3~6 times of weight, each 1~3 hour, obtain filtrate; Merge above-mentioned all filtrate, be concentrated into relative density and be 1.2~1.25(60 ℃ record), obtain extractum.
5. the Chinese medicine extract for having one's hair wash that preparation method as claimed in claim 4 makes.
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CN105395401A (en) * 2015-11-30 2016-03-16 黄春美 Liquid shampoo with hair caring function
CN105534877A (en) * 2016-03-18 2016-05-04 三株福尔制药有限公司 Fermentation traditional Chinese medicine combination for liquid shampoo and preparation method and application of combination
CN105534877B (en) * 2016-03-18 2018-03-23 三株福尔制药有限公司 A kind of fermented tcm composition for shampoo and its preparation method and application
CN108403611A (en) * 2018-06-04 2018-08-17 云南健牛生物科技有限公司 A kind of efficient sterilizing anticreep promotees hair tonic shampoo and preparation method thereof
CN109528588A (en) * 2018-12-21 2019-03-29 佛山市南海施乐华化妆品有限公司 Shampoo of anti-dandruff and itching-relieving and preparation method thereof
CN110051606A (en) * 2019-05-27 2019-07-26 肖海存 A kind of oil-control, the formula of anti-dandruff, antipruritic pure Chinese medicine shampoo and preparation method thereof
CN110327271A (en) * 2019-08-26 2019-10-15 章华化妆品科技有限公司 A kind of anti-dandruff and itching-relieving plant composition, preparation method and application
CN114404335A (en) * 2022-01-29 2022-04-29 王二秀 Preparation method of foam anti-dandruff shampoo
CN114681365A (en) * 2022-04-29 2022-07-01 福建片仔癀化妆品有限公司 Shampoo with oil control and mite removal effects and preparation method thereof
CN114681365B (en) * 2022-04-29 2023-10-27 福建片仔癀化妆品有限公司 Shampoo with oil control and mite removal effects and preparation method thereof

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