CN103816092B - A kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash - Google Patents
A kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash Download PDFInfo
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Abstract
The invention discloses a kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash.The invention discloses a kind of feedstock composition of the Chinese medicine extract for having one's hair wash, it is made up of following ingredients: Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1 ~ 5 part, Radix Sophorae Flavescentis is 1 ~ 30 part, and Rhizoma Coptidis is 5 ~ 15 parts, Radix Scutellariae is 5 ~ 15 parts, and Fructus Cnidii is 1 ~ 30 part, and Fructus Viticis is 1 ~ 3 part, and Cortex Mori is 1 ~ 5 part, Rhizoma Chuanxiong is 1 ~ 5 part, and the Radix Stemonae is 0.5 ~ 20 part, and Cortex Dictamni is 0.5 ~ 20 part, and Cortex Phellodendri is 1 ~ 5 part; Above number is parts by weight.Chinese medicine extract of the present invention can be used for preparing the cosmeticses of everyday use such as shampoo, hair cream, hair conditioner, can reach the effect of excellent antibacterial, removing scurf and relieving itching.
Description
Technical field
The present invention relates to a kind of Chinese medicine extract, its preparation method and feedstock composition thereof for having one's hair wash.
Background technology
Along with growth in the living standard, popularizing of health perception, the hair washing frequency of present Chinese Urban Residents also starts more and more close to developed country's level, reaches 3 ~ 3.5 times/week.But want real and correct healthy philosophy of life to integrate with, it is far from being enough for increasing shampoos simply, and how we are it is to be appreciated that scientifically to remove hair washing, hair care.In the environment that we depend on for existence at present, pollute and reach seriously unprecedented with industrialization development, dust, ultraviolet, chemicals and various microorganism (antibacterial, mycete/yeast) are not attacking our hair all the time, bring out multiple class problem, as the dandruff, scalp itch, hair bifurcated, hair dry up.
Dandruff is one of subject matter of puzzlement modern hair, and the principal element of dandruff generation is the breeding of head metabolism appearance exception and pityrosporum furfur (chlosma), grows.Find according to the research of China's Healthy Education Associations scalp health research center, owing to not noting skin of head health care, bad hygienic habit and lacking necessary anti-dandruff hair care knowledge, have in the middle of Chinese adult the female consumer of 59% and 63% male consumer be subject to the puzzlement of dandruff all always.Simple has one's hair wash with common shampoo, can clean at most dirt and temporarily take away the dandruff on hair top layer, but can not really from solution dandruff problem at all.
Summary of the invention
Technical problem to be solved by this invention there is provided a kind of Chinese medicine extract, its preparation method and feedstock composition thereof for have one's hair wash diverse with prior art.Chinese medicine extract of the present invention can be used for preparing the cosmeticses of everyday use such as shampoo, hair cream, hair conditioner, can reach the effect of excellent antibacterial, removing scurf and relieving itching.
The invention provides a kind of feedstock composition of the Chinese medicine extract for having one's hair wash, it is made up of following ingredients: Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1 ~ 5 part, Radix Sophorae Flavescentis is 1 ~ 30 part, and Rhizoma Coptidis is 5 ~ 15 parts, Radix Scutellariae is 5 ~ 15 parts, and Fructus Cnidii is 1 ~ 30 part, and Fructus Viticis is 1 ~ 3 part, and Cortex Mori is 1 ~ 5 part, Rhizoma Chuanxiong is 1 ~ 5 part, and the Radix Stemonae is 0.5 ~ 20 part, and Cortex Dictamni is 0.5 ~ 20 part, and Cortex Phellodendri is 1 ~ 5 part; Above number is parts by weight.
Preferably, in the feedstock composition of the described Chinese medicine extract for having one's hair wash: when being classified as 2 ~ 4 parts, Radix Sophorae Flavescentis is 2 ~ 4 parts, and Rhizoma Coptidis is 7 ~ 13 parts, Radix Scutellariae is 9 ~ 13 parts, Fructus Cnidii is 3 ~ 15 parts, and Fructus Viticis is 1 ~ 2 part, and Cortex Mori is 1 ~ 3 part, Rhizoma Chuanxiong is 2 ~ 3 parts, the Radix Stemonae is 3 ~ 15 parts, and Cortex Dictamni is 1 ~ 13 part, and Cortex Phellodendri is 1 ~ 3 part; Above number is parts by weight.
Better, in the feedstock composition of the described Chinese medicine extract for having one's hair wash: when being classified as 2 ~ 3 parts, Radix Sophorae Flavescentis is 3 ~ 4 parts, and Rhizoma Coptidis is 8 ~ 11 parts, Radix Scutellariae is 10 ~ 11 parts, Fructus Cnidii is 4 ~ 6 parts, and Fructus Viticis is 1 ~ 2 part, and Cortex Mori is 1 ~ 2 part, Rhizoma Chuanxiong is 3 parts, the Radix Stemonae is 5 ~ 8 parts, and Cortex Dictamni is 5 ~ 8 parts, and Cortex Phellodendri is 1 ~ 2 part; Above number is parts by weight.
In the present invention, the described feedstock composition for the Chinese medicine extract of having one's hair wash is the formula for the preparation of described Chinese medicine.As required, the feedstock composition of the Chinese medicine extract for having one's hair wash of the present invention can be a component form of all the components mixing, also can be each composition independent or each composition is divided into many components nested form of some groups.
In the present invention, described is obtained by the method preparing Chinese medicine extract of this area routine for the Chinese medicine extract of having one's hair wash.
Present invention also offers the preparation method of the above-mentioned Chinese medicine extract for having one's hair wash, it comprises the following step: mixed by the ethanol water of the feedstock composition of the above-mentioned Chinese medicine extract for having one's hair wash and the percent by volume 60% ~ 90% of 3 ~ 6 times of weight, reflux 1 ~ 3 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 ~ 3 time of the percent by volume 60% ~ 90% of 3 ~ 6 times of weight, each 1 ~ 3 hour, obtain filtrate; Merge above-mentioned all filtrate, be concentrated into relative density and be 1.2 ~ 1.25(60 DEG C and record), obtain extractum.
Present invention also offers the Chinese medicine extract for having one's hair wash that above-mentioned preparation method obtains.
As required, Chinese medicine extract of the present invention can mix with the adjuvant for the preparation of hair washing product of this area routine, makes the various product forms such as shampoo, hair cream or hair conditioner.Such as, above-mentioned Chinese medicine extract can be added in conventional shampoo formula, is prepared into shampoo; Wherein each Ingredient Amount is conventional amount used.
The feature of Chinese herbal medicine extract of the present invention is primary raw material with natural Chinese medicinal herb, utilizes various composition reasonable combination, Synergistic, reach antibacterial by number of ways, the effect of removing scurf and relieving itching.This extract, by traditional machining processes, can be widely used in the products such as shampoo, hair cream, hair conditioner, symptoms such as dandruff effectively can being suppressed to produce, alleviate scalp itch, hair is withered.Traditional Chinese medical theory is effectively combined with modern medicine study achievement by this extract, follows " endogenous cause of ill ", " exopathogenic factor " principle simultaneously, reaches inside and outside effect of minoring, and for comprehensively, thoroughly solving dandruff, head pruritus problem provides a referential approach.
Without prejudice to the field on the basis of common sense, above-mentioned each optimum condition, can combination in any, obtains the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material are all commercially.
Positive progressive effect of the present invention is: Chinese medicine extract of the present invention can be used for preparing the cosmeticses of everyday use such as shampoo, hair cream, hair conditioner, can reach the effect of excellent antibacterial, removing scurf and relieving itching, for comprehensively, thoroughly solving dandruff, head pruritus problem provides a referential approach.
Detailed description of the invention
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, conventionally and condition, or selects according to catalogue.
Preparation embodiment 1 ~ 6
The preparation of embodiment 1 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 1 part, Radix Sophorae Flavescentis is 1 part, and Rhizoma Coptidis is 5 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 1 part, Fructus Viticis 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 1 part, and the Radix Stemonae is 0.5 part, and Cortex Dictamni is 0.5 part, and Cortex Phellodendri is 1 part; Above number is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mix with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 hour of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 DEG C and record), obtain extractum.
The preparation of embodiment 2 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 5 parts, Radix Sophorae Flavescentis is 30 parts, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 15 parts, and Fructus Cnidii is 30 parts, and Fructus Viticis is 3 parts, and Cortex Mori is 5 parts, and Rhizoma Chuanxiong is 5 parts, 20 parts, Radix Stemonae position, and Cortex Dictamni is 20 parts, and Cortex Phellodendri is 5 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Be total to 1Kg after claiming above-mentioned raw materials to press number mixing, mix with the ethanol water of the percent by volume 90% of 6Kg, reflux 3 hours, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 3 times of the percent by volume 90% of 6 times of weight of filtering residue, each 3 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 DEG C and record), obtain extractum.
The preparation of embodiment 3 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 2 parts, Radix Sophorae Flavescentis is 2 parts, and Rhizoma Coptidis is 7 parts, and Radix Scutellariae is 9 parts, and Fructus Cnidii is 3 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 2 parts, and the Radix Stemonae is 3 parts, and Cortex Dictamni is 1 part, and Cortex Phellodendri is 1 part; Above number is parts by weight;
Concrete preparation process is as follows:
Be total to 1Kg after claiming above-mentioned raw materials to press number mixing, mix with the ethanol water of the percent by volume 75% of 4.5Kg, reflux 2 hours, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 2 times of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 DEG C and record), obtain extractum.
The preparation of embodiment 4 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 4 parts, Radix Sophorae Flavescentis is 4 parts, and Rhizoma Coptidis is 13 parts, and Radix Scutellariae is 13 parts, and Fructus Cnidii is 15 parts, and Fructus Viticis is 2 parts, and Cortex Mori is 3 parts, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 15 parts, and Cortex Dictamni is 13 parts, and Cortex Phellodendri is 3 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Be total to 1Kg after claiming above-mentioned raw materials to press number mixing, mix with the ethanol water of the percent by volume 75% of 4.5Kg, reflux 2 hours, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 2 times of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 DEG C and record), obtain extractum.
The preparation of embodiment 5 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 2 parts, Radix Sophorae Flavescentis is 3 parts, and Rhizoma Coptidis is 8 parts, and Radix Scutellariae is 10 parts, and Fructus Cnidii is 4 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 5 parts, and Cortex Dictamni is 5 parts, and Cortex Phellodendri is 1 part; Above number is parts by weight;
Concrete preparation process is as follows:
Be total to 1Kg after claiming above-mentioned raw materials to press number mixing, mix with the ethanol water of the percent by volume 75% of 4.5Kg, reflux 2 hours, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 2 times of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 DEG C and record), obtain extractum.
The preparation of embodiment 6 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 3 parts, Radix Sophorae Flavescentis is 4 parts, and Rhizoma Coptidis is 11 parts, and Radix Scutellariae is 11 parts, and Fructus Cnidii is 6 parts, and Fructus Viticis is 2 parts, and Cortex Mori is 2 parts, and Rhizoma Chuanxiong is 3 parts, and the Radix Stemonae is 8 parts, and Cortex Dictamni is 8 parts, and Cortex Phellodendri is 2 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Be total to 1Kg after claiming above-mentioned raw materials to press number mixing, mix with the ethanol water of the percent by volume 75% of 4.5Kg, reflux 2 hours, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 2 times of the percent by volume 75% of 4.5 times of weight of filtering residue, each 2 hours, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.25(60 DEG C and record), obtain extractum.
The preparation of comparative example 1 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 35 parts, and Rhizoma Coptidis is 2 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 5 parts, and Fructus Viticis is 1 part, and Cortex Mori is 1 part, and Rhizoma Chuanxiong is 2 parts, and the Radix Stemonae is 23 parts, and Cortex Dictamni is 22 parts, and Cortex Phellodendri is 6 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mix with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 hour of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 DEG C and record), obtain extractum.
The preparation of comparative example 2 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis and Cortex Mori; Wherein, when being classified as 1 part, Radix Sophorae Flavescentis is 1 part, and Rhizoma Coptidis is 5 parts, and Radix Scutellariae is 5 parts, and Fructus Cnidii is 2 parts, and Cortex Mori is 2 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mix with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 hour of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 DEG C and record), obtain extractum.
The preparation of comparative example 3 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 0.5 part, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 3 parts, and Fructus Cnidii is 4 parts, Fructus Viticis 5 parts, and Cortex Mori is 6 parts, and Rhizoma Chuanxiong is 7 parts, and the Radix Stemonae is 0.3 part, and Cortex Dictamni is 22 parts, and Cortex Phellodendri is 1 part; Above number is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mix with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 hour of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 DEG C and record), obtain extractum.
The preparation of comparative example 4 Chinese medicine extract
The material combination composition formula of Chinese medicine extract is as follows:
Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 7 parts, Radix Sophorae Flavescentis is 33 parts, and Rhizoma Coptidis is 15 parts, and Radix Scutellariae is 17 parts, and Fructus Cnidii is 0.5 part, Fructus Viticis 5 parts, and Cortex Mori is 6 parts, and Rhizoma Chuanxiong is 0.5 part, and the Radix Stemonae is 0.2 part, and Cortex Dictamni is 0.2 part, and Cortex Phellodendri is 6 parts; Above number is parts by weight;
Concrete preparation process is as follows:
Claim above-mentioned raw materials 1Kg, mix with the ethanol water of the percent by volume 60% of 3Kg, reflux 1 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 hour of the percent by volume 60% of 3 times of weight of filtering residue, obtain filtrate; Merge all filtrate, be concentrated into relative density and be 1.2(60 DEG C and record), obtain extractum.
Fungistatic effect embodiment
1, test specimen
By above-described embodiment 1 ~ 6, and the Chinese medicine extract that comparative example 1 ~ 4 obtains adds in the commercial shampoos of a routine respectively, and this shampoo formula is as follows:
The weight ratio of Chinese medicine extract and this shampoo is 0.2%, and mix homogeneously, is numbered A, B, C, D, E, F(embodiment 1 ~ 6 respectively), H, I, J, K(comparative example 1 ~ 4); BW is the well-known Chinese herbal medicine concept dandruff control shampoo containing that market is sold;
Above-mentioned conventional shampoo is numbered G, does not namely add the blank shampoo of Chinese medicine extract of the present invention.
2, test index
Inhibition zone diameter (mm); Minimum inhibitory concentration (MIC, %);
3, result of the test
3.1 broad spectrum activity bacteriostatic test results
Note: D value * is the inhibition zone diameter sum to three kinds of strain subjects, and antibacterial bacterial concentration is about 5.0 × 10
7cfu/ml, mycete and yeast liquid concentration are about 3.5 × 10
6cfu/ml.
According to test data, except G, other 7 kinds of shampoos are to strain subject all comparatively responsive (D > 27.0), and wherein the fungistatic effect of E, F is best.
3.2 feature bacterium bacteriostatic test results
Note: the activity of chlosma bacterium liquid is about 4.0 × 10
5cfu/ml.
According to test data, the present invention's 7 kinds of shampoos and BW all have certain inhibitory action to strain subject, and the fungistatic effect that wherein with the addition of the shampoo of Chinese medicine extract of the present invention is obviously better than un-added shampoo G, and H, I, J, K.
Human efficiency's effect example
For shampoo sample A, B, C, D, E, F, G and BW in above-mentioned fungistatic effect embodiment, applicant carried out the test of human body antidandruff efficacy validation, result of the test is as follows:
1. experiment material
1.1 test specimen
Totally 8 kinds of shampoos, are numbered A, B, C, D, E, F, G and BW(the same).
1.2 subjects
Inclusive criteria is: the non-pathologic dandruff phenomenon of medium or medium above degree, left and right sides dandruff gradient of infection is roughly the same.
1.3 test numbers
Choose 26 volunteers altogether to test, be divided into 2 groups, actually complete number 20 people, wherein male 10 people, female 10 people, 20 ~ 50 years old age.
2. experimental design and method
2.1 objective image analyses
Respectively the right and left dandruff is combed on glass plate according to the operation sequence of standard, then cover with the glass plate that another block is onesize, seal and preserve.In 14 days, graphical analysis is carried out to glass plate.
Under cold light source lighting condition, under black background, gather glass plate image with monochromatic CCD camera and preserve.By analysis software, picture is analyzed, calculate the area percentage (%) of dandruff.
2.2 subjective assessment dandruff amounts
Technical staff marks to the dandruff amount of the right and left respectively according to standards of grading:
0 ... without dandruff; 1 ... fragmentary dandruff; 2 ... a small amount of dandruff; 3 ... moderate dandruff; 4 ... a large amount of dandruff.
2.3 adaptation of product evaluations
Technical staff and volunteer carry out the Adaptability Evaluation of product respectively to the right and left, Adaptability Evaluation parameter comprises the rubescent situation of scalp, scalp itch and burn feeling, and wherein the rubescent situation of scalp is evaluated by technical staff; Scalp itch, burn feeling are evaluated by volunteer.
Scalp is rubescent, scalp itch, burn feeling situation rating scale:
0 ... nothing; 1 ... slightly; 2 ... medium; 3 ... seriously; 4 ... very serious.
3. experimental result
3.1 objective image analyses
Objective image analytical data is as follows:
Wherein, average is that after the different shampoo of the lasting use of 20 samples, (frequency, consumption are identical.Frequency is use once every day), at the Average area percentages (%) of the dandruff of different time.
From analytical data on the whole, BW group and A ~ F group dandruff amount reduce with the increase of service time substantially.Product uses the later stage (the 14th day) compared with use early stage (the 0th day), and the dandruff amount of A group ~ F group shows as significance and reduces; The dandruff amount of BW group is on a declining curve, but there was no significant difference, G group dandruff amount declines slowly.
3.2 subjective assessment
Subjective analysis data are as follows:
Wherein, average is that after the different shampoo of the lasting use of 20 samples, (frequency, consumption are identical.Frequency is use once every day), in the scoring of different time.
From subjective data entirety, BW group and A ~ F group dandruff amount reduce with the increase of service time substantially.Product uses the later stage (the 14th day) compared with use early stage (the 0th day), and the dandruff amount of A group ~ F group shows as significance and reduces; The dandruff amount of BW group is on a declining curve, but there was no significant difference, G group dandruff amount declines slowly.
3.3 adaptation of product evaluations
Adaptability Evaluation data are as follows:
Wherein, meansigma methods is that after the different shampoo of the lasting use of 20 samples, (frequency, consumption are identical.Frequency is use once every day), mark at different time.
Rubescent and the burning sensation result of scalp itch, scalp
The situation such as rubescent and burn feeling for scalp itch, scalp, all show mitigation largely after using BW group and A ~ F group, G group alleviation degree is poor.
4. brief summary
Use after shampoo A ~ F group a period of time, by objective analysis and subjective assessment, dandruff amount is all in trend of obvious reduced, and to scalp itch, scalp, the situation such as rubescent and burn feeling also has mitigation to a certain degree.
Claims (4)
1. the feedstock composition of Chinese medicine extract for having one's hair wash, is characterized in that: it is made up of following ingredients: Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Coptidis, Radix Scutellariae, Fructus Cnidii, Fructus Viticis, Cortex Mori, Rhizoma Chuanxiong, the Radix Stemonae, Cortex Dictamni and Cortex Phellodendri; Wherein, when being classified as 2 ~ 4 parts, Radix Sophorae Flavescentis is 2 ~ 4 parts, and Rhizoma Coptidis is 7 ~ 13 parts, Radix Scutellariae is 9 ~ 13 parts, and Fructus Cnidii is 3 ~ 15 parts, and Fructus Viticis is 1 ~ 2 part, and Cortex Mori is 1 ~ 3 part, Rhizoma Chuanxiong is 2 ~ 3 parts, and the Radix Stemonae is 3 ~ 15 parts, and Cortex Dictamni is 1 ~ 13 part, and Cortex Phellodendri is 1 ~ 3 part; Above number is parts by weight.
2. the feedstock composition of the Chinese medicine extract for having one's hair wash as claimed in claim 1, it is characterized in that: in the feedstock composition of the described Chinese medicine extract for having one's hair wash: when being classified as 2 ~ 3 parts, Radix Sophorae Flavescentis is 3 ~ 4 parts, and Rhizoma Coptidis is 8 ~ 11 parts, Radix Scutellariae is 10 ~ 11 parts, Fructus Cnidii is 4 ~ 6 parts, and Fructus Viticis is 1 ~ 2 part, and Cortex Mori is 1 ~ 2 part, Rhizoma Chuanxiong is 3 parts, the Radix Stemonae is 5 ~ 8 parts, and Cortex Dictamni is 5 ~ 8 parts, and Cortex Phellodendri is 1 ~ 2 part; Above number is parts by weight.
3. the preparation method of Chinese medicine extract for having one's hair wash, it is characterized in that comprising the following step: the ethanol water mixing of the feedstock composition of the Chinese medicine extract that being used for described in claim 1 or 2 is had one's hair wash and the percent by volume 60% ~ 90% of 3 ~ 6 times of weight, reflux 1 ~ 3 hour, filter, obtain filtrate; Gained filtering residue is continued, with the ethanol water mixing backflow 1 ~ 3 time of the percent by volume 60% ~ 90% of 3 ~ 6 times of weight, each 1 ~ 3 hour, obtain filtrate; Merge above-mentioned all filtrate, be concentrated into relative density and be 1.2 ~ 1.25,60 DEG C and record, obtain extractum.
4. the Chinese medicine extract for having one's hair wash that obtains of a preparation method as claimed in claim 3.
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| CN105395401A (en) * | 2015-11-30 | 2016-03-16 | 黄春美 | Liquid shampoo with hair caring function |
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| CN110051606A (en) * | 2019-05-27 | 2019-07-26 | 肖海存 | A kind of oil-control, the formula of anti-dandruff, antipruritic pure Chinese medicine shampoo and preparation method thereof |
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| CN114404335A (en) * | 2022-01-29 | 2022-04-29 | 王二秀 | Preparation method of foam anti-dandruff shampoo |
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