CN104971295A - Traditional Chinese medicine composition and application thereof in preparing sargassum fusiforme and lotus seed nutritional wine - Google Patents
Traditional Chinese medicine composition and application thereof in preparing sargassum fusiforme and lotus seed nutritional wine Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine composition and an application thereof in preparing sargassum fusiforme and lotus seed nutritional wine. The traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10 parts of sargassum fusiforme, 3-8 parts of sea cucumber, 2-8 parts of oyster, 6-20 parts of lotus seeds, 8-18 parts of rehmannia, 4-9 parts of the fruits of Chinese wolfberry, 3-8 parts of angelica sinensis, 3-8 parts of liquorice, 3-8 parts of the root of red-rooted salvia, 4-6 parts of eucommia ulmoides, 4-8 parts of ligustrazine, 1-3 parts of cinnamon, 2-4 parts of old ginger, and 2-4 parts of amomum cardamomum. For the nutritional wine prepared by adopting the traditional Chinese medicine composition, the yield of crude polysaccharide is improved by 36.7%, the content of protein is improved by 16.3%, and the content of fat is improved by 14.5%.
Description
(1) technical field
The present invention relates to a kind of Chinese medicine composition and prepare the application of nutrition wine, can blood viscosity be reduced in particular to one, reduce thrombosis, cerebral hemorrhage risk, alleviate hypertensive patient symptom, keep fit brain-strengthening, improve the preparation method of the Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine of immunity.
(2) background technology
People require day by day to promote to life, for the needs of care concepts and highly intensive labour, day by day improve the requirement of the tonic of edible natural, nutrition.Current marine food is subject to the high praise of people day by day, although marine organisms quantity is a lot, but edible inconvenient.The kind can selected through the product of processing is few, and product on the market often carries inconvenience, and nutrition is single.Marine organisms and medicine food dual purpose plant are carried out reasonable compatibility by the present invention.Adopt modern processing to carry out polish, take into account in edible, nutrition and taste etc., each side comprehensive consideration reaches good effect.
Marine organisms such as Sargassum fusiforme (Harv.) Setch waste material produces ethanol, and as patent 200710014246, the method is that ethanol and feedstuff are produced in twice laid.Stichopus japonicus has the patent of direct processing and eating, is decomposed by High Temperature High Pressure as 201210397241.5, cooks medicated porridge, does multiple Stichopus japonicus fourth.There is the method for directly soaking, as the patent No. 200410066342.X detected, use Semen Nelumbinis as raw material.Carry out the technique of liquid fermentation alcoholic after immersion, but extract often incomplete, in the raw materials such as Sargassum fusiforme (Harv.) Setch, Stichopus japonicus, Concha Ostreae, Semen Nelumbinis, effective ingredient decomposes further therefore to adopt pectase, cellulase, rhizopus to promote; The medical material soaked and distiller grains are mixed the method for after fermentation, extract the active ingredient obtained more, make the delicate flavour material of wine body, fragrance ingredient abundanter simultaneously; Marine drug fishy smell is heavier, by with the mixing of distiller grains, a large amount of fishy smell material in marine organisms is absorbed by distiller grains, improves the mouthfeel of wine.Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine of the present invention can improve the immunocompetence of people, brain-care, and this Product Safety is high, practical and convenient.
(3) summary of the invention
The object of the invention is to provide a kind of Chinese medicine composition and prepares the application in Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine, Sargassum fusiforme (Harv.) Setch nutrition wine alcoholic strength of the present invention temperature compensation, comprehensive nutrition, clean taste, wine body are limpid, its effect to reduce blood viscosity, reduce thrombosis, cerebral hemorrhage risk, alleviate hypertensive patient's symptom, have and improve blood circulation of human body, brain-nourishing intelligence-benefiting, enhancing immunity etc. are powerful.
The technical solution used in the present invention is:
The invention provides a kind of Chinese medicine composition, described Chinese medicine composition is made up of the raw material of following weight proportion: Sargassum fusiforme (Harv.) Setch 10 parts, Stichopus japonicus 3 ~ 8 parts, Concha Ostreae 2 ~ 8 parts, 6 ~ 20 parts, Semen Nelumbinis, Radix Rehmanniae 8 ~ 18 parts, Fructus Lycii 4 ~ 9 parts, Radix Angelicae Sinensis 3 ~ 8 parts, 3 ~ 8 parts, Radix Glycyrrhizae, Radix Salviae Miltiorrhizae 3 ~ 8 parts, the Cortex Eucommiae 4 ~ 6 parts, ligustrazine 4 ~ 8 parts, 1 ~ 3 part, Cortex cinnamomi japonici (Ramulus Cinnamomi), old ginger 2 ~ 4 parts and Fructus Amomi Rotundus 2 ~ 4 parts.
Further, preferred described Chinese medicine composition is made up of the raw material of following weight proportion: Sargassum fusiforme (Harv.) Setch 10 parts, Stichopus japonicus 4 ~ 5 parts, Concha Ostreae 3 ~ 5 parts, 10 ~ 12 parts, Semen Nelumbinis, Radix Rehmanniae 10 ~ 12 parts, Fructus Lycii 4 ~ 6 parts, Radix Angelicae Sinensis 3 ~ 5 parts, 4 ~ 6 parts, Radix Glycyrrhizae, Radix Salviae Miltiorrhizae 3 ~ 4 parts, the Cortex Eucommiae 4 ~ 5 parts, ligustrazine 6 ~ 8 parts, 1 ~ 2 part, Cortex cinnamomi japonici (Ramulus Cinnamomi), old ginger 3 ~ 4 parts and Fructus Amomi Rotundus 2 ~ 3 parts.
The present invention also provides a kind of described Chinese medicine composition preparing the application in Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine, and concrete described application process is: (1), by the Chinese medicine composition soaking in Chinese liquor 7-10 days of formula ratio, filters, and obtains and soaks wine liquid and filtering residue; (2) as fermentation substrate after filtering residue step (1) obtained and lees of yellow wine mix, access pectase and cellulase, stirring and evenly mixing, be cooled to room temperature after 50 DEG C of maintenance 12h, access rhizopus, malt yeast and yeast wine, 50 DEG C keep 50 days, upper rice steamer distillation, obtains distillation wine liquid; Described filtering residue and lees of yellow wine weight ratio are 1:5 ~ 10 (preferred 1:7 ~ 10); Described pectase quality addition counts 1 ~ 1.5% (preferably 1 ~ 1.2%) with fermentation substrate weight, described cellulase quality addition counts 1 ~ 2% (preferably 1.2 ~ 1.8%) with fermentation substrate weight, and described rhizopus quality addition counts 0.8 ~ 1.5% (preferably 0.8 ~ 1.0%) with fermentation substrate weight, described malt yeast quality addition counts 1.0 ~ 2.5% (preferably 1.5 ~ 2.0%) with fermentation substrate weight, described yeast wine quality addition counts 2 ~ 4% (preferably 3.0 ~ 3.2%) with fermentation substrate weight; (3) filter after the immersion wine liquid that distillation wine liquid step (2) obtained and step (1) obtain mixes, get filtrate and namely obtain Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine.
Further, in preferred steps (1), soaking in Chinese liquor method is: first Chinese medicine composition Chinese liquor is carried out first time and soak, soak time is 7 days for the first time, filter, obtain filtrate and for the first time filtering residue for the first time, and then in first time filtering residue, add Chinese liquor carry out second time and soak, second time soak time is 3 days, filter, obtain second time filtrate and second time filtering residue, merge filtrate and second time filtrate for the first time and be immersion wine liquid, second time filtering residue is used for being mixed and made into fermentation substrate with lees of yellow wine; First time soaks Chinese liquor volumetric usage used and counts 5ml/g with Chinese medicine composition weight, and second time is soaked Chinese liquor volumetric usage used and counted 5ml/g with Chinese medicine composition weight, and described Chinese liquor is that grain is burnt.
Further, in preferred steps (1), Chinese liquor is that 53 ° of grains are burnt.
Further, described in preferred steps (2), filtering residue and lees of yellow wine weight ratio are 1:8.Distiller grains after lees of yellow wine can adopt yellow wine to squeeze, or burn the ripe distiller grains after distillation through grain, preferred lees of yellow wine is that grain burns single flash after-ripening distiller grains.
Further, described in preferred steps (2), pectase quality addition counts 1% with fermentation substrate weight, and described cellulase quality addition counts 1.5% with fermentation substrate weight.
Further, rhizopus quality addition described in preferred steps (2) counts 0.8% with fermentation substrate weight, described malt yeast quality addition counts 1.8% with fermentation substrate weight, described yeast wine quality addition counts 3.0% with fermentation substrate weight.
Further, filtering in preferred steps (3) is that after being mixed with immersion wine liquid by distillation wine liquid, adopt 0.45 μm of organic micro-filtration membrane of micropore to carry out vacuum filtration, filtrate is Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine.
The enzyme of pectase of the present invention live 20000U/g, cellulase enzyme to live 16000U/g, the enzyme of rhizopus is lived 3500U/g, and live 15g/gh, saccharifying enzyme of the α-amylase of malt yeast is lived 800mg/gh, and yeast wine is made a living cooking wine mother.
Sargassum fusiforme (Harv.) Setch of the present invention is preferably Wenzhou City, Zhejiang Province Sargassum fusiforme (Harv.) Setch that is produced from Dongtou County, and described Stichopus japonicus is preferably Liaoning Province Stichopus japonicus that is produced from Daliang City, and described Concha Ostreae is preferably clean dried Concha Ostreae, and described grain is burnt preferably Shaoxing brewery and produced 53 ° of grain burnings.
Compared with prior art, beneficial effect of the present invention is mainly reflected in: the invention provides a kind of Chinese medicine composition and preparing the application in Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine, and in the nutrition wine adopting this Chinese medicine composition to prepare, crude polysaccharides yield improves 36.7% (adopting sulphuric acid-Herba Alii fistulosi ketone method), protein content improves 16.3% (adopting GB/T 5009.5-2010), fat content improves 14.5% (adopting GB/T5009.5-2003).Sargassum fusiforme (Harv.) Setch nutrition wine alcoholic strength of the present invention temperature compensation, comprehensive nutrition, clean taste, wine body are limpid, and its effect to reduce blood viscosity, reduce thrombosis, cerebral hemorrhage risk, alleviate hypertensive patient's symptom, have and improve blood circulation of human body, brain-nourishing intelligence-benefiting, enhancing immunity etc. are powerful.
(4) detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further, but protection scope of the present invention is not limited in this:
Sargassum fusiforme (Harv.) Setch described in the embodiment of the present invention is by being produced Sargassum fusiforme (Harv.) Setch in Dongtou County, Wenzhou City, Zhejiang Province, and described Stichopus japonicus is by being produced Stichopus japonicus in Daliang City of Liaoning Province, and described Concha Ostreae is clean dried Concha Ostreae, and described Chinese medicine all meets " Pharmacopoea Chinensis " requirement.
Described grain is burnt preferably Shaoxing brewery and is produced 53 ° of grain burnings, and lees of yellow wine burns the distiller grains after distilling preferably past once poor.
Embodiment 1:
(1) Traditional Chinese medicine composition formula: Sargassum fusiforme (Harv.) Setch 12g, Stichopus japonicus 5g, Concha Ostreae 5g, Semen Nelumbinis 14g, Radix Rehmanniae 16g, Fructus Lycii 7g, Radix Angelicae Sinensis 8g, Radix Glycyrrhizae 4g, Radix Salviae Miltiorrhizae 5g, Cortex Eucommiae 6g, ligustrazine 7g, Cortex cinnamomi japonici (Ramulus Cinnamomi) 2g, old ginger 3g, Fructus Amomi Rotundus 3g.
(2) pretreatment: according to step (1) formula ratio, clean Sargassum fusiforme (Harv.) Setch, Stichopus japonicus, Concha Ostreae are smashed; Semen Nelumbinis, Radix Rehmanniae, Fructus Lycii, Radix Angelicae Sinensis, Radix Glycyrrhizae, Radix Salviae Miltiorrhizae, the Cortex Eucommiae, ligustrazine, Cortex cinnamomi japonici (Ramulus Cinnamomi), old ginger, Fructus Amomi Rotundus are cleaned, smash, with Steam Heating sterilizing in 15 minutes, loads in cylinder.
(3) step (2) pretreated Chinese medicine composition is burnt immersion by every 100g 500ml 53 ° grain, soak at room temperature 7 days for the first time, filtrate and for the first time filtering residue is for the first time obtained by 5 layers of filtered through gauze, and then in first time filtering residue, add 500ml 53 ° of grains burn into row second time soak at room temperature 3 days, second time filtrate is obtained by 5 layers of filtered through gauze, merge filtrate and second time filtrate (namely soaking wine liquid) for the first time, get filtering residue stand-by;
(4) lees of yellow wine is cooled to 52 ~ 55 DEG C, step (3) filtering residue is made fermentation substrate with the mixing of 1:8 (filtering residue: lees of yellow wine mass ratio) ratio, by every 1000g fermentation substrate access 10g pectase (enzyme 20000U/g alive), 15g cellulase (enzyme 16000U/g alive), room temperature is cooled to after mixing 50 DEG C of maintenance 12h, access 8g rhizopus (enzyme 3500U/g alive) again, 18g malt yeast (α-amylase 15g/gh alive, saccharifying enzyme 800mg/gh alive), 30g yeast wine (raw material yeast wine).Within first 10 days, turn over even once a day, control temperature 32 ~ 35 DEG C, centre is turned over once even in 10 days every 2 days, keeps temperature 30 ~ 32 DEG C, within latter 10 days, leaves standstill and does not stir, and after 30 day time, upper rice steamer, obtains distillation wine liquid;
(5) distill wine liquid to mix with immersion wine liquid, then through the 0.45 μm of organic micro-filtration membrane of micropore (millipore) vacuum filtration, filtrate is Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine (wine base).
In nutrition wine, crude polysaccharides yield improves 36.7% (adopting sulphuric acid-Herba Alii fistulosi ketone method), protein content improves 16.3% (adopting GB/T 5009.5-2010), fat content improves 14.5% (adopting GB/T5009.5-2003).
Embodiment 2
Step (2), step (3) and step (5) method and operation with embodiment 1, unlike:
(1) Traditional Chinese medicine composition formula: take Sargassum fusiforme (Harv.) Setch 15g, Stichopus japonicus 8g, Concha Ostreae 6g, Semen Nelumbinis 10g, Radix Rehmanniae 14g, Fructus Lycii 7g, Radix Angelicae Sinensis 7g, Radix Glycyrrhizae 8g, Radix Salviae Miltiorrhizae 5g, Cortex Eucommiae 6g, ligustrazine 9g, Cortex cinnamomi japonici (Ramulus Cinnamomi) 2g, old ginger 5g, Fructus Amomi Rotundus 4g.
(4) get lees of yellow wine and be cooled to 52 ~ 55 DEG C, step (3) filtering residue is made fermentation substrate with the mixing of 1:10 (filtering residue: lees of yellow wine) ratio, by every 1000g fermentation substrate access pectase 12g (enzyme 20000U/g alive), cellulase 18g (enzyme 16000U/g alive), 25 DEG C are cooled to, access rhizopus 10g (enzyme 3500U/g alive), malt yeast 20g (α-amylase 15g/gh alive, saccharifying enzyme 800mg/gh alive), yeast wine 30g (raw material yeast wine) after mixing 50 DEG C of maintenance 12h.Within first 10 days, turn over even once a day, control temperature 32 ~ 35 DEG C, centre is turned over once even in 10 days every 2 days, keeps temperature 30 ~ 32 DEG C, within latter 10 days, leaves standstill and does not stir, and within latter 10 days, leaves standstill, and after 32 day time, upper rice steamer, obtains distillation wine liquid.
In nutrition wine, crude polysaccharides yield improves 34.5% (adopting sulphuric acid-Herba Alii fistulosi ketone method), protein content improves 15.2% (adopting GB/T 5009.5-2010), fat content improves 13.9% (adopting GB/T5009.5-2003).
Embodiment 3
Step (2), step (3) and step (5) method and operation with embodiment 1, unlike:
(1) Traditional Chinese medicine composition formula: take Sargassum fusiforme (Harv.) Setch 10g, Stichopus japonicus 4g, Concha Ostreae 4g, Semen Nelumbinis 16g, Radix Rehmanniae 18g, Fructus Lycii 8g, Radix Angelicae Sinensis 7g, Radix Glycyrrhizae 4g, Radix Salviae Miltiorrhizae 5g, Cortex Eucommiae 6g, ligustrazine 7g, Cortex cinnamomi japonici (Ramulus Cinnamomi) 2g, old ginger 3g, Fructus Amomi Rotundus 3g.
(4) get lees of yellow wine and be cooled to 52 ~ 55 DEG C, step (3) filtering residue is made fermentation substrate with the mixing of weight ratio 1:7 (filtering residue: lees of yellow wine) ratio, by every 1000g fermentation substrate access pectase 10g (enzyme 20000U/g alive), cellulase 12g (enzyme 16000U/g alive), mixing, room temperature is cooled to after 50 DEG C of maintenance 12h, then rhizopus 8g (enzyme 3500U/g alive) is accessed, malt yeast 15g (α-amylase 15g/gh alive, saccharifying enzyme 800mg/gh alive), yeast wine 32g (raw material yeast wine), first 10 day every day turned over once even, control temperature 32 ~ 35 DEG C, centre is turned over once even in 10 days every 2 days, keep temperature 30 ~ 32 DEG C, within latter 10 days, leave standstill and do not stir, upper rice steamer after 30 day time, wine liquid must be distilled.
In nutrition wine, crude polysaccharides yield improves 37.8% (adopting sulphuric acid-Herba Alii fistulosi ketone method), protein content improves 17.5% (adopting GB/T 5009.5-2010), fat content improves 15.3% (adopting GB/T5009.5-2003).
Case 1
Lee's ××, man 53 years old, dizziness, the deficiency of vital energy, neurasthenia.Daily this nutrition wine (prepared by embodiment 1) 75 ~ 100 milliliters, is clearly better after three months, has no untoward reaction.
Case 2
Gong's ××, female 38 years old, dizzy, tinnitus, weak, daily this nutrition wine (prepared by embodiment 2) 50 ~ 100 milliliters.Symptom takes a turn for the better after two months.
Case 3
Open ××, female 45 years old, the deficiency of vital energy, fear of cold, cardiopalmus are weak.Daily this nutrition wine (prepared by embodiment 2) 75 ~ 100 milliliters.Symptom has been had obviously to improve after three months.
Case 4
In ××, man 65 years old, liver-fire rising, with hypertension symptom, daily this nutrition wine (prepared by embodiment 3) 50 ~ 100 milliliters, has had after six months and has been clearly better.Upper blood pressure reduces to 128mmHg by 157mmHg, and lower blood pressure reduces to 83mmHg by 114mmHg.
The patient suffering from the symptoms such as neurasthenia, dizzy, tinnitus, hypertension with 80 is for taking object, after oral nutrition wine of the present invention 80 ~ 88% patient recovery from illness or symptom be clearly better, there is certain improvement in the patient of 7% ~ 12%, the patient outcome of 5% ~ 8% is general.
Claims (10)
1. a Chinese medicine composition, is characterized in that described Chinese medicine composition is made up of the raw material of following weight proportion: Sargassum fusiforme (Harv.) Setch 10 parts, Stichopus japonicus 3 ~ 8 parts, Concha Ostreae 2 ~ 8 parts, 6 ~ 20 parts, Semen Nelumbinis, Radix Rehmanniae 8 ~ 18 parts, Fructus Lycii 4 ~ 9 parts, Radix Angelicae Sinensis 3 ~ 8 parts, 3 ~ 8 parts, Radix Glycyrrhizae, Radix Salviae Miltiorrhizae 3 ~ 8 parts, the Cortex Eucommiae 4 ~ 6 parts, ligustrazine 4 ~ 8 parts, 1 ~ 3 part, Cortex cinnamomi japonici (Ramulus Cinnamomi), old ginger 2 ~ 4 parts and Fructus Amomi Rotundus 2 ~ 4 parts.
2. Chinese medicine composition as claimed in claim 1, is characterized in that described Chinese medicine composition is made up of the raw material of following weight proportion: Sargassum fusiforme (Harv.) Setch 10 parts, Stichopus japonicus 4 ~ 5 parts, Concha Ostreae 3 ~ 5 parts, 10 ~ 12 parts, Semen Nelumbinis, Radix Rehmanniae 10 ~ 12 parts, Fructus Lycii 4 ~ 6 parts, Radix Angelicae Sinensis 3 ~ 5 parts, 4 ~ 6 parts, Radix Glycyrrhizae, Radix Salviae Miltiorrhizae 3 ~ 4 parts, the Cortex Eucommiae 4 ~ 5 parts, ligustrazine 6 ~ 8 parts, 1 ~ 2 part, Cortex cinnamomi japonici (Ramulus Cinnamomi), old ginger 3 ~ 4 parts and Fructus Amomi Rotundus 2 ~ 3 parts.
3. Chinese medicine composition described in a claim 1 is preparing the application in Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine.
4. apply as claimed in claim 3, it is characterized in that described application process is: (1), by the Chinese medicine composition soaking in Chinese liquor 7-10 days of formula ratio, filters, and obtains and soaks wine liquid and filtering residue; (2) as fermentation substrate after filtering residue step (1) obtained and lees of yellow wine mix, access pectase and cellulase, stirring and evenly mixing, be cooled to room temperature after 50 DEG C of maintenance 12h, then access rhizopus, malt yeast and yeast wine, 50 DEG C keep 50 days, upper rice steamer distillation, obtains distillation wine liquid; Described filtering residue and lees of yellow wine weight ratio are 1:5 ~ 10; Described pectase quality addition counts 1 ~ 1.5% with fermentation substrate weight, described cellulase quality addition counts 1 ~ 2% with fermentation substrate weight, and described rhizopus quality addition counts 0.8 ~ 1.5% with fermentation substrate weight, described malt yeast quality addition counts 1.0 ~ 2.5% with fermentation substrate weight, described yeast wine quality addition counts 2 ~ 4% with fermentation substrate weight; (3) filter after the immersion wine liquid that distillation wine liquid step (2) obtained and step (1) obtain mixes, get filtrate and namely obtain Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine.
5. apply as claimed in claim 4, it is characterized in that in step (1), soaking in Chinese liquor method is: first Chinese medicine composition Chinese liquor is carried out first time and soak, soak time is 7 days for the first time, filter, obtain first time filtrate and first time filtering residue, and then in first time filtering residue, add Chinese liquor carry out second time immersion, second time soak time is 3 days, filter, acquisition second time filtrate and second time filtering residue, merge filtrate and second time filtrate for the first time and be immersion wine liquid; First time soaks Chinese liquor volumetric usage used and counts 5ml/g with Chinese medicine composition weight, and second time is soaked Chinese liquor volumetric usage used and counted 5ml/g with Chinese medicine composition weight, and described Chinese liquor is that grain is burnt.
6. apply as claimed in claim 4, it is characterized in that in step (1), Chinese liquor is that 53 ° of grains are burnt.
7. apply as claimed in claim 4, it is characterized in that described in step (2), filtering residue and lees of yellow wine weight ratio are 1:8, described lees of yellow wine is the ripe distiller grains after grain burns single flash.
8. apply as claimed in claim 4, it is characterized in that described in step (2), pectase quality addition counts 1% with fermentation substrate weight, described cellulase quality addition counts 1.5% with fermentation substrate weight.
9. apply as claimed in claim 4, it is characterized in that rhizopus quality addition described in step (2) counts 0.8% with fermentation substrate weight, described malt yeast quality addition counts 1.8% with fermentation substrate weight, described yeast wine quality addition counts 3.0% with fermentation substrate weight.
10. apply as claimed in claim 4, it is characterized in that filtering in step (3) is that after being mixed with immersion wine liquid by distillation wine liquid, adopt 0.45 μm of organic micro-filtration membrane of micropore to carry out vacuum filtration, filtrate is Sargassum fusiforme (Harv.) Setch nutritious lotus seed wine.
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