CN103806267B - 一种在碳纤维表面制备碳化锆陶瓷界面相的方法 - Google Patents
一种在碳纤维表面制备碳化锆陶瓷界面相的方法 Download PDFInfo
- Publication number
- CN103806267B CN103806267B CN201310714558.1A CN201310714558A CN103806267B CN 103806267 B CN103806267 B CN 103806267B CN 201310714558 A CN201310714558 A CN 201310714558A CN 103806267 B CN103806267 B CN 103806267B
- Authority
- CN
- China
- Prior art keywords
- interface phase
- carbon
- vacuum
- fiber surface
- zirconium carbide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910026551 ZrC Inorganic materials 0.000 title claims abstract description 27
- OTCHGXYCWNXDOA-UHFFFAOYSA-N [C].[Zr] Chemical compound [C].[Zr] OTCHGXYCWNXDOA-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 239000000919 ceramic Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 26
- 229920000049 Carbon (fiber) Polymers 0.000 title claims abstract description 15
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 239000004917 carbon fiber Substances 0.000 title claims abstract description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 11
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920001568 phenolic resin Polymers 0.000 claims abstract description 8
- 239000000725 suspension Substances 0.000 claims abstract description 8
- 239000002270 dispersing agent Substances 0.000 claims abstract description 7
- 238000011065 in-situ storage Methods 0.000 claims abstract description 7
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims abstract description 5
- 238000001035 drying Methods 0.000 claims abstract description 5
- 239000003960 organic solvent Substances 0.000 claims abstract description 5
- 238000000498 ball milling Methods 0.000 claims abstract description 4
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000005011 phenolic resin Substances 0.000 claims description 5
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical group CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 claims description 5
- 239000012046 mixed solvent Substances 0.000 claims description 3
- 239000002131 composite material Substances 0.000 abstract description 14
- HPNSNYBUADCFDR-UHFFFAOYSA-N chromafenozide Chemical compound CC1=CC(C)=CC(C(=O)N(NC(=O)C=2C(=C3CCCOC3=CC=2)C)C(C)(C)C)=C1 HPNSNYBUADCFDR-UHFFFAOYSA-N 0.000 abstract description 13
- 230000002787 reinforcement Effects 0.000 abstract description 12
- 230000008569 process Effects 0.000 abstract description 4
- 230000007547 defect Effects 0.000 abstract description 2
- 238000006557 surface reaction Methods 0.000 abstract description 2
- 239000000835 fiber Substances 0.000 description 15
- 238000011156 evaluation Methods 0.000 description 11
- 229910010271 silicon carbide Inorganic materials 0.000 description 8
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 6
- 238000011160 research Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000011153 ceramic matrix composite Substances 0.000 description 3
- 238000005229 chemical vapour deposition Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Landscapes
- Ceramic Products (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310714558.1A CN103806267B (zh) | 2013-12-21 | 2013-12-21 | 一种在碳纤维表面制备碳化锆陶瓷界面相的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310714558.1A CN103806267B (zh) | 2013-12-21 | 2013-12-21 | 一种在碳纤维表面制备碳化锆陶瓷界面相的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103806267A CN103806267A (zh) | 2014-05-21 |
CN103806267B true CN103806267B (zh) | 2016-03-23 |
Family
ID=50703622
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310714558.1A Active CN103806267B (zh) | 2013-12-21 | 2013-12-21 | 一种在碳纤维表面制备碳化锆陶瓷界面相的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103806267B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104744880B (zh) * | 2015-03-02 | 2017-07-11 | 武汉理工大学 | 一种酚醛树脂‑碳化锆悬浊液的制备方法 |
CN106431499B (zh) * | 2016-10-06 | 2019-08-09 | 西北工业大学 | 一种ZrB2陶瓷的反应化学气相沉积制备方法 |
CN115477824B (zh) * | 2022-10-10 | 2024-03-26 | 华东理工大学 | 一种含表层原位自生抗烧蚀层的纳米孔树脂基复合材料的制备方法 |
CN115852293B (zh) * | 2022-10-13 | 2024-07-30 | 扬州大学 | 一种金属陶瓷自润滑复合耐磨涂层的制备方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101570443A (zh) * | 2009-06-02 | 2009-11-04 | 航天材料及工艺研究所 | 炭材料表面金属碳化物/碳复合涂层及其制备方法 |
CN101693628A (zh) * | 2009-10-20 | 2010-04-14 | 西北工业大学 | 纤维增强ZrC陶瓷基复合材料的制备方法 |
CN102530942A (zh) * | 2010-12-08 | 2012-07-04 | 中国科学院金属研究所 | 利用含锆有机物前驱体合成碳化锆粉体材料的制备方法 |
CN102924083A (zh) * | 2012-11-02 | 2013-02-13 | 武汉理工大学 | 一种碳化锆陶瓷粉体的制备方法 |
CN103193484A (zh) * | 2012-01-09 | 2013-07-10 | 中国科学院上海硅酸盐研究所 | 一种ZrC-SiC复相陶瓷材料的制备方法 |
CN103288469A (zh) * | 2013-05-15 | 2013-09-11 | 西北工业大学 | 碳/碳-碳化锆复合材料的制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2521795B2 (ja) * | 1988-10-21 | 1996-08-07 | 日本石油株式会社 | 耐酸化性を有する炭素繊維強化複合材料の製造法 |
-
2013
- 2013-12-21 CN CN201310714558.1A patent/CN103806267B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101570443A (zh) * | 2009-06-02 | 2009-11-04 | 航天材料及工艺研究所 | 炭材料表面金属碳化物/碳复合涂层及其制备方法 |
CN101693628A (zh) * | 2009-10-20 | 2010-04-14 | 西北工业大学 | 纤维增强ZrC陶瓷基复合材料的制备方法 |
CN102530942A (zh) * | 2010-12-08 | 2012-07-04 | 中国科学院金属研究所 | 利用含锆有机物前驱体合成碳化锆粉体材料的制备方法 |
CN103193484A (zh) * | 2012-01-09 | 2013-07-10 | 中国科学院上海硅酸盐研究所 | 一种ZrC-SiC复相陶瓷材料的制备方法 |
CN102924083A (zh) * | 2012-11-02 | 2013-02-13 | 武汉理工大学 | 一种碳化锆陶瓷粉体的制备方法 |
CN103288469A (zh) * | 2013-05-15 | 2013-09-11 | 西北工业大学 | 碳/碳-碳化锆复合材料的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN103806267A (zh) | 2014-05-21 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP3549926B1 (en) | Method for preparing c/c-sic composite material part | |
JP6411894B2 (ja) | セラミックマトリックス複合材を製造する方法およびそれによって形成されたセラミックマトリックス複合材 | |
EP1683771B1 (en) | Method for performing silicon melt infiltration of ceramic matrix composites | |
US10584070B2 (en) | Ceramic matrix composites having monomodal pore size distribution and low fiber volume fraction | |
CN102515870B (zh) | 一种C/SiC-ZrB2-ZrC超高温陶瓷基复合材料的制备方法 | |
CN103806267B (zh) | 一种在碳纤维表面制备碳化锆陶瓷界面相的方法 | |
CN103979974B (zh) | 一种C/SiC-HfB2-HfC超高温陶瓷基复合材料的制备方法 | |
US10450235B2 (en) | Method of producing an internal cavity in a ceramic matrix composite and mandrel therefor | |
CN101224990A (zh) | 耐超高温陶瓷基复合材料及其制备方法 | |
CN111825471B (zh) | 一种电泳沉积制备连续碳纤维增韧超高温陶瓷基复合材料的方法 | |
CN103724042B (zh) | 一种叠层混杂防热复合结构材料的制备方法 | |
CN112142486A (zh) | 抗烧蚀碳化硅纤维增强陶瓷基复合材料的制备方法 | |
US20160159695A1 (en) | Composite components with coated fiber reinforcements | |
CN106882976B (zh) | 一种C/HfC-ZrC-SiC复合材料的制备方法 | |
CN101348370A (zh) | 一种碳化物陶瓷的先驱体溶液、碳化物陶瓷及制备方法 | |
CN109608235A (zh) | 一种c/c复合材料异形件的凝胶熔渗陶瓷化改性方法 | |
CN103722784B (zh) | 一种叠层树脂填充混杂复合材料的制备方法 | |
US10723660B2 (en) | Carbon yielding resin for melt infiltration | |
CN104496506A (zh) | 一种C/C-TaC-ZrB2陶瓷基复合材料及其制备方法 | |
CA3049204C (en) | Melt infiltration with siga and/or siin alloys | |
CN110436955A (zh) | 一种钇改性SiCf/SiC陶瓷基复合材料及其制备方法 | |
US11845699B2 (en) | Methods for manufacturing coated composite materials | |
CN117945770A (zh) | 一种陶瓷基复合材料制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230414 Address after: 314511 West of the first floor of Building 1, No. 368 Zhongshan Road, Chongfu Town, Tongxiang City, Jiaxing City, Zhejiang Province Patentee after: Jiaxingrui innovative materials Co.,Ltd. Address before: 200050 No. 1295 Dingxi Road, Shanghai, Changning District Patentee before: SHANGHAI INSTITUTE OF CERAMICS, CHINESE ACADEMY OF SCIENCES |
|
EE01 | Entry into force of recordation of patent licensing contract | ||
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20140521 Assignee: Zhejiang Hangyin New Material Technology Co.,Ltd. Assignor: Jiaxingrui innovative materials Co.,Ltd. Contract record no.: X2024980006923 Denomination of invention: A method for preparing zirconium carbide ceramic interface phase on the surface of carbon fibers Granted publication date: 20160323 License type: Common License Record date: 20240611 |