CN103767032A - Processing technology of high-content polysaccharide and O-acetyl aloe juice product - Google Patents

Processing technology of high-content polysaccharide and O-acetyl aloe juice product Download PDF

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Publication number
CN103767032A
CN103767032A CN201410036669.6A CN201410036669A CN103767032A CN 103767032 A CN103767032 A CN 103767032A CN 201410036669 A CN201410036669 A CN 201410036669A CN 103767032 A CN103767032 A CN 103767032A
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CN
China
Prior art keywords
aloe
aloe gel
juice
juice product
acetyl group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201410036669.6A
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Chinese (zh)
Inventor
胡娟
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HAINAN ZHONGCHEN BIOLOGIC ENGINEERING Co Ltd
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HAINAN ZHONGCHEN BIOLOGIC ENGINEERING Co Ltd
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Priority to CN201410036669.6A priority Critical patent/CN103767032A/en
Publication of CN103767032A publication Critical patent/CN103767032A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/72Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a processing technology of a high-content polysaccharide and O-acetyl aloe juice product. The processing technology mainly comprises the following steps of preparing fresh aloe leaves, preparing aloe gel clear juice and preparing an aloe gel juice product. The process of the processing technology disclosed by the invention comprises the following steps: carrying out normal temperature/time-limited/sanitary processing without thermal/chemical/biological change and active substance separation, and carrying out HTST (High Temperature Short Time) sterilization, so that the physical properties, high-content chemical components and biological activity of the aloe gel juice product are reserved and original functions are effectively reserved. According to the prepared aloe gel juice product, the polysaccharide and O-acetyl contents can respectively reach up to 1,310mg/k and 1,450mg/kg, which are far higher than 400mg/kg and 350mg/kg as standard specified values in the aloe industry; meanwhile, the lactic acid is less than 3mg/L; therefore the aloe gel juice product has a favorable application prospect.

Description

A kind of high-load polysaccharide and O-acetyl group asparagus juice product processing technique
Technical field
The present invention relates to aloe processing technique field, particularly relate to the process technology of a kind of high-load polysaccharide and O-acetyl group asparagus juice product.
Background technology
Aloe is Liliaceae Aloe perennial evergreen fleshiness torrid zone herbaceous plant, it is a kind of ancient medicinal plant, in Ancient Times in China medical book Shennong's Herbal, Compendium of Material Medica, all record the special medicinal efficacy of aloe, as existing more than the 4000 year history of medication among the people.
Aloe is the function that raw material is prepared health food; mainly contain anti-inflammatory, sterilization, promotion wound healing, strengthen immunity, anti-oxidant, give protection against cancer, contribute to improve gastrointestinal function, contribute to relieving sports fatigue, help lend some impetus to skin of face health, the effect such as clearing and protection stomach lining; aloe all has larger application in fields such as food, health products, cosmetics in recent years, and aloe development prospect is considerable.
The important activity composition of aloe is polysaccharide, and its aloe acetylated mannosan is study hotspot at home and abroad.Raw material aloe products quality standard is carried out QB/T2489-2007 " raw-food material aloe products " industry standard; the polysaccharide and O-acetyl group (detecting index as the acemannan) standard that in this standard, stipulate decolored aloe gel juice are respectively 400mg/kg and 350mg/kg; and aloe polysaccharide and O-acetyl group index are higher, show that this aloe products quality is higher.
At present, there is not yet that the relevant plant husbandry of domestic aloe and processing industry are paid close attention to the industrialization plantation of high-load polysaccharide and O-acetyl group aloe, also rarely seen aloe product processing industry is paid close attention to and produced the converted products of high-load aloe polysaccharide and O-acetyl group and high-load polysaccharide and the O-acetyl group aloe product of special concern and the direct production and processing of demand Fresh leaf of aloe.The known existing processing method of preparing high-load polysaccharide and O-acetyl group product; because being difficult to obtain high-load polysaccharide and O-acetyl group Fresh leaf of aloe; conventionally adopt the methods such as solvent extraction, Microwave Extraction, ultrasonic wave assisted extraction; or consuming timely longly make polysaccharide and O-acetyl group is oxidizable or it is lost activity or be assisted extraction through heating, all unsatisfactory.
Summary of the invention
For the problems referred to above, the invention provides the process technology of a kind of high-load polysaccharide and O-acetyl group aloe dry powder product, be intended to keep to greatest extent the polysaccharide of aloe condensed juice product and O-acetyl content with and biologically active.
The present invention for the technical scheme that its technical problem of solution adopts is:
A kind of high-load polysaccharide and O-acetyl group asparagus juice product processing technique, is characterized in that comprising the following steps:
Step 1: pluck the Fresh leaf of aloe of full age with for subsequent use;
Step 2: the Fresh leaf of aloe described in step 1 is cleaned successively, sterilizes, removed the peel, produce aloe gel sheet; Described aloe gel sheet is pulverized to grinding, centrifugation successively, produce the turbid juice of aloe gel; To the turbid juice of described aloe gel, decolorization filtering, diatomite filtration successively, produces the clear juice of aloe gel;
Step 3: the clear juice of aloe gel that step 2 is produced, carry out HTST sterilizing, sterile filling, produce high-load polysaccharide and O-acetyl group Aloe gel juice product.
As a further improvement on the present invention, in described step 1, Fresh leaf of aloe, from plucking to time≤4 hour in limited time that start processing, is plucked full age Fresh leaf of aloe/handling/transportation breakage-proof and sun-proof.
Further, in described step 2, Fresh leaf of aloe starts to be machined to and produces the clear juice process of aloe gel prescribe a time limit between time≤2 hour, operation temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g.
Further, produce in the process of aloe gel sheet in described step 2, further comprise Fresh leaf of aloe multiple tracks is cleaned, in the Naclo of 50ppm liquid, sterilized and clean, between operation, temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g, produce aloe gel sheet.
Further, produce in the process of the turbid juice of aloe gel in described step 2, further comprise and add pectase 200~300g/T aloe gel sheet, glue abrasive dust breakdown mill granularity≤50 μ m, centrifugation rotating speed≤3700r/min successively, between operation, temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g, produce the turbid juice of aloe gel.
Further, produce in the process of the clear juice of aloe gel in described step 2, further comprise and carry out successively that 80 order filter cloth sheet frame activated carbon decolorizings filter, diatomite refilters, temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g between operation, before HTST sterilizing, monitoring lactic acid≤3mg/L, produces the clear juice of aloe gel.
In addition, in described step 3, Aloe gel juice carries out 116 ℃ of HTST temperature, time 10S sterilizing, sterile filling, produces Aloe gel juice product.
The invention has the beneficial effects as follows: the present invention relates to a kind of high-load polysaccharide and O-acetyl group asparagus juice product processing technique, mainly comprise preparation Fresh leaf of aloe, prepare the clear juice of aloe gel, and the several steps of Aloe gel juice product, preparation method's machining process provided by the invention is normal temperature/in limited time/health processing, separate generation with active material without calorifics/chemistry/biological variation, again through lower temperature HTST sterilizing in short-term, make Aloe gel juice product keep its physical characteristic and high-load chemical composition to keep its biologically active simultaneously, realize product and effectively retain that it is former powerful, the Aloe gel juice product of preparation, polysaccharide and O-acetyl content are the highest can reach respectively 1310mg/kg and 1450mg/kg, considerably beyond the aloe industry standard setting of 400mg/kg and 350mg/kg, lactic acid < 3mg/L simultaneously, therefore possesses good application prospect.
The specific embodiment
Below by the specific embodiment, high-load polysaccharide of the present invention and O-acetyl group asparagus juice product processing technique are further described:
A kind of high-load polysaccharide and O-acetyl group asparagus juice product processing technique, is characterized in that comprising the following steps: step 1: pluck the Fresh leaf of aloe of full age with for subsequent use; Step 2: the Fresh leaf of aloe described in step 1 is cleaned successively, sterilizes, removed the peel, produce aloe gel sheet; Described aloe gel sheet is pulverized to grinding, centrifugation successively, produce the turbid juice of aloe gel; To the turbid juice of described aloe gel, decolorization filtering, diatomite filtration successively, produces the clear juice of aloe gel; Step 3: the clear juice of aloe gel that step 2 is produced, carry out HTST sterilizing, sterile filling, produce high-load polysaccharide and O-acetyl group Aloe gel juice product.
Particularly, pluck in limited time/handling/transportation operation: Fresh leaf of aloe 24T/ day, early within 4 o'clock, start to pluck full age Fresh leaf of aloe, dress basket pluck/load and unload/be transported to the process that starts processing to complete 3.5~4 hours/car, two car operation 6T/ train number, 2 train numbers/vehicle shift time in limited time; In limited time normal temperature is produced the clear juice operation of aloe gel: arrive and add building site to 1.5~2 hours process time in limited time that is processed as the clear juice of aloe gel from Fresh leaf of aloe, production line processing fresh leaf 3.5T/h, the first T of the clear juice process time≤1.9h/ of aloe, process time≤0.6h/T thereafter; Carry out successively cleaning and sterilizing, peeling, pulverizing grinding, centrifugation, decolouring, filtration, between operation, temperature is 20~22 ℃, occupational health condition monitoring total plate count≤100cfu/g, produce the clear juice 12T of aloe gel, wherein, produce aloe gel sheet operation: Fresh leaf of aloe rinses/rolls scrub/rinsing/sterilization (the Naclo liquid of 50ppm)/spray through 5 road interlock cleaning machines successively and washes, occupational health condition monitoring total plate count≤100cfu/g, produce aloe gel sheet, process monitoring O-acetyl group 1610mg/kg; Produce the turbid juice operation of aloe gel: add successively pectase (enzyme work >=30000U/g) 250g/T aloe gel sheet, 3 glue abrasive dust breakdown mill granularity≤50, road μ m, centrifugation rotating speed≤3700r/min, produce the turbid juice of aloe gel; Produce the clear juice operation of aloe gel: add successively the turbid juice of active carbon 5kg/T aloe gel through 80 keevil frame decolorization filterings, add every batch of diatomite 7kg/ (formation filter cake) through 80 order plate-frame filterings, produce the clear juice 12T of aloe gel, to process monitoring lactic acid < 3mg/L before HTST sterilizing; 116 ℃/10S of HTST sterilization process: HTST (high temperature, short time) sterilizing, sterile filling, produce Aloe gel juice product 12T; Aloe gel juice examination and test of products operation: wherein; high-load polysaccharide and O-acetyl group are respectively 1310mg/kg and 1450mg/kg, lactic acid < 3mg/L; the on-site verification monitoring index keeping as product biologically active, can on-site verification from prescribe a time limit activity duration and the occupational health accordance of plucking converted products operation overall process.
Above better enforcement of the present invention is illustrated; certainly; the present invention can also adopt form different from the embodiment described above; and close field; these do not form any restriction to present embodiment; the conversion being equal to that those of ordinary skill in the art do under the prerequisite without prejudice to spirit of the present invention or accordingly change, all should belong to protection scope of the present invention.

Claims (7)

1. high-load polysaccharide and an O-acetyl group asparagus juice product processing technique, is characterized in that comprising the following steps:
The Fresh leaf of aloe of step 1, harvesting full age is with for subsequent use;
Step 2, the Fresh leaf of aloe described in step 1 is cleaned successively, sterilizes, removed the peel, produce aloe gel sheet; Described aloe gel sheet is pulverized to grinding, centrifugation successively, produce the turbid juice of aloe gel; To the turbid juice of described aloe gel, decolorization filtering, diatomite filtration successively, produces the clear juice of aloe gel;
Step 3, the clear juice of the aloe gel that step 2 is produced, carry out HTST sterilizing, sterile filling, produces high-load polysaccharide and O-acetyl group Aloe gel juice product.
2. high-load polysaccharide according to claim 1 and O-acetyl group asparagus juice product processing technique; it is characterized in that: in described step 1, Fresh leaf of aloe, from plucking to time≤4 hour in limited time that start processing, is plucked full age Fresh leaf of aloe/handling/transportation breakage-proof and sun-proof.
3. high-load polysaccharide according to claim 1 and O-acetyl group asparagus juice product processing technique, is characterized in that: in described step 2, Fresh leaf of aloe starts to be machined between time≤2 in limited time hour, operation of producing the clear juice process of aloe gel temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g.
4. high-load polysaccharide according to claim 1 and 2 and O-acetyl group asparagus juice product processing technique; it is characterized in that: produce in the process of aloe gel sheet in described step 2; further comprise Fresh leaf of aloe multiple tracks is cleaned, in the Naclo of 50ppm liquid, sterilized and clean; between operation, temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g, produce aloe gel sheet.
5. high-load polysaccharide according to claim 1 and 2 and O-acetyl group asparagus juice product processing technique; it is characterized in that: produce in the process of the turbid juice of aloe gel in described step 2; further comprise and add pectase 200~300g/T aloe gel sheet; glue abrasive dust breakdown mill granularity≤50 μ m, centrifugation rotating speed≤3700r/min successively; between operation, temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g, produce the turbid juice of aloe gel.
6. high-load polysaccharide according to claim 1 and 2 and O-acetyl group asparagus juice product processing technique; it is characterized in that: produce in the process of the clear juice of aloe gel in described step 2; further comprise and carry out successively that 80 order filter cloth sheet frame activated carbon decolorizings filter, diatomite refilters; temperature≤23 ℃, occupational health condition monitoring total plate count≤100cfu/g between operation; before HTST sterilizing, monitoring lactic acid≤3mg/L, produces the clear juice of aloe gel.
7. high-load polysaccharide according to claim 1 and O-acetyl group asparagus juice product processing technique, is characterized in that: in described step 3, Aloe gel juice carries out 116 ℃ of HTST temperature, time 10S sterilizing, sterile filling, produces Aloe gel juice product.
CN201410036669.6A 2014-01-26 2014-01-26 Processing technology of high-content polysaccharide and O-acetyl aloe juice product Pending CN103767032A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11547719B2 (en) 2018-03-28 2023-01-10 Herbalife International Of America, Inc. Acetylation of aloe polysaccharides

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1173354A (en) * 1997-02-14 1998-02-18 北京轻工业学院海口技工贸实业开发公司 Method for prepn. of aloe products, and products obtained thereby
CN1216232A (en) * 1997-10-31 1999-05-12 黄小周 Extraction of aloe extract
JP3099120B1 (en) * 1999-04-19 2000-10-16 株式会社ヴァルト Method for producing aloe juice
CN1589677A (en) * 2004-03-16 2005-03-09 大连理工大学 Cleaning production method of colourless transparent debittered stable aloe jelly juice
US20060134238A1 (en) * 2004-12-16 2006-06-22 Dnyaneshwar Agashe M Process of manufacturing clear juice from the leaves of the aloe vera plant
CN1817208A (en) * 2006-02-28 2006-08-16 李亚萍 Stoste processing method of food decoloured aloe gel in proportion of 1:1

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1173354A (en) * 1997-02-14 1998-02-18 北京轻工业学院海口技工贸实业开发公司 Method for prepn. of aloe products, and products obtained thereby
CN1216232A (en) * 1997-10-31 1999-05-12 黄小周 Extraction of aloe extract
JP3099120B1 (en) * 1999-04-19 2000-10-16 株式会社ヴァルト Method for producing aloe juice
CN1589677A (en) * 2004-03-16 2005-03-09 大连理工大学 Cleaning production method of colourless transparent debittered stable aloe jelly juice
US20060134238A1 (en) * 2004-12-16 2006-06-22 Dnyaneshwar Agashe M Process of manufacturing clear juice from the leaves of the aloe vera plant
CN1817208A (en) * 2006-02-28 2006-08-16 李亚萍 Stoste processing method of food decoloured aloe gel in proportion of 1:1

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11547719B2 (en) 2018-03-28 2023-01-10 Herbalife International Of America, Inc. Acetylation of aloe polysaccharides

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Application publication date: 20140507