CN1589677A - Cleaning production method of colourless transparent debittered stable aloe jelly juice - Google Patents

Cleaning production method of colourless transparent debittered stable aloe jelly juice Download PDF

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Publication number
CN1589677A
CN1589677A CN 200410021416 CN200410021416A CN1589677A CN 1589677 A CN1589677 A CN 1589677A CN 200410021416 CN200410021416 CN 200410021416 CN 200410021416 A CN200410021416 A CN 200410021416A CN 1589677 A CN1589677 A CN 1589677A
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aloe
filter
juice
clean
heat exchanger
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CN 200410021416
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CN1284485C (en
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王长海
常秀莲
冯咏梅
刘兆普
金赞敏
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Dalian University of Technology
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Dalian University of Technology
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Publication of CN1284485C publication Critical patent/CN1284485C/en
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  • Cosmetics (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

A process for preparing the color-less transparent aloe gel with high stability, no bitter taste for improving immunity, preventing and treating cancer, AIDS and diabetes, and protecting skin features no use of organic solvent, stabilizer, antioxidizing agent, acid and alkali.

Description

The water white transparency debitterize is stablized the clean preparation method of Aloe gel juice
Technical field
The invention belongs to technical field of biochemical industry, relate to the production of stablizing juice, the clean preparation method of the Aloe gel juice that especially a kind of water white transparency debitterize is stable.
Background technology
Aloe is the perennial fleshiness woody plant of Liliaceae (Liliaceae) Aloe (Aloe).Aloe vulgaris is because of its strain height, and blade is long and thick, and it is many to contain mesophyll, is at present domestic and international implant mass and the principal item that is used for processing.Aloe polysaccharide has repairing and nursing face, uvioresistant, and the effect of preserving moisture and protecting skin can improve body immunity, has antitumor, anticancer, anti-AIDS and prevents and treats effects such as diabetes.Contain more than 20 kind of anthraquinone analog compounds such as Barbaloin, aloe-emodin, Aloe resin B in the fresh aloe, though this class material has effects such as sterilization, antiinflammatory, promotion wound healing, but most consumers dislike the bitterness that they present in the oral cavity, small part consumer groups produce anaphylaxis, suffer from diarrhoea as the eater, skin allergy appears in beauty treatment person, should not contain anthraquinone analog compound in the aloe products of using as food or cosmetic material.Therefore the Aloe glue of decolouring (or debitterize), concentrated Aloe glue, Aloe dry powder are present domestic the most salable aloe products.
At present, clarify stable Aloe gel juice and adopt the enzymolysis pour point depression more, the method that adds antioxidant and stabilizing agent prepares, as application number be: 01111407 (denomination of invention: a kind of manufacture method of aloe products) and application number be as described in the patent application of 01128675 (denomination of invention: biological pourpoint depression and nano concentration process for extracting aloe juice), what adopt all is to add the method that pectase carries out the enzymolysis pour point depression, application number is: 01114503 (denomination of invention: the stabilization method of Aloe gel) add antioxidant and edetic acid, and use the Fructus Citri Limoniae acid for adjusting pH value, and final product also will charge into nitrogen with isolated and air.Early stage patent of the U.S., the patent No. is: 3892853 (1975), adopt at 40-50 ℃ and drip hydrogen peroxide down, oxidative decoloration also will add ascorbic acid then as antioxidant, adds sorbitol and hexadecanol as stabilizing agent.People such as Gao Yixiang remove and add antioxidant and surfactant (it is heterogeneous to prevent that system from occurring); also add buffer solution (Gao Yixiang; Jia Jicheng. the extraction of medicinal aloe gel natural juice and stability contrast thereof. weaving colleges and universities basic science journal, 1997,12 (1): 36~40).Also have to adopt and add vitamin C, Na 2SO 4Or method such as citric acid improve Aloe juice stability (Xu Ling, Li Cuixia wait the people clearly in will. the development and use of aloe food. storage processing, 2002,2:28~29).There is the deficiency of following several respects in the above method:
(1) adopt enzyme-added pour point depression method, need to use pectase and/or cellulase, these two kinds of enzymes cost an arm and a leg, and process cost is increased greatly, and the introducing of enzyme preparation, and the part degraded also can take place the active polysaccharide in the Aloe, cause the product reduction of tiring.
(2) add the balance that compositions such as antioxidant and stabilizing agent have changed the original system component of Aloe, introduce abnormal flavour and may cause anaphylactic reaction.
(3) adopt the method oxidative decoloration that adds hydrogen peroxide, partial oxidation also can take place in the active component in the Aloe, causes loss of active ingredients.
(4) behind the adding vitamin C, oxidation reaction slowly can take place with oxygen in vitamin C, and its colour changed into yellow is then deepened gradually.
Summary of the invention
The clean preparation method that the purpose of this invention is to provide the stable Aloe gel juice of a kind of water white transparency debitterize solves unstable, variable color in the Aloe gel juice manufacturing process, the problem that polysaccharide degraded that the introducing of foreign substance causes and cost increase.
The production process that technical solution of the present invention adopted is: aloe leaf---removes the peel and---pulverizes and---filter------decolouring---filtration---fine straining---sterilization---cooling---packing that hot polymerization is heavy.Do not add organic solvent in process of production, do not add stabilizing agent, antioxidant, do not add acid, alkali, keep the nature pH value, adopt thermoprecipitation to remove the unstability composition, activated carbon decolorizing, the removal efficiency of anthraquinone class bitter substance reaches more than 99.99% in the Aloe.
Concrete route is: pluck healthy and strong full aloe leaf of 3 terms, simply clean with tap water, drop is clean, peeling, be ground into serosity, filter then gel juice, gel juice is heated to 50 ℃~130 ℃, keeps under 50 ℃~130 ℃ 10 minutes~10 hours, is cooled to 30 ℃-60 ℃, with 0.5%~1% powdered activated carbon decoloring 0.5 hour, remove by filter active carbon then, the further again fine straining of the clear liquor that decolours is removed residual activity charcoal and other microgranule, and water white transparency liquid is through sterilizing for 15 seconds down at 130 ℃, be cooled to 60 ℃ rapidly, carry out vacuum packaging.
Effect benefit of the present invention is:
(1) Aloe gel juice product water white transparency, outward appearance is like water, and the removal efficiency of anthraquinones is more than 99.99%.Original a little sharp aroma of Aloe disappears, and gel juice taste is soft, light perfume (or spice).Product does not contain antioxidant, does not contain stabilizing agent, does not add acid, alkali, keeps the nature pH value.Under the condition of adding preservative agent not, can stablize for 20 ℃ and preserve more than 90 days, add a small amount of antiseptic, can stablize and preserve more than 1 year.
(2) the fresh aloe blade of Cai Zhaiing does not need disinfectant to soak, and gets final product with simple cleaning of tap water.In the Aloe juice pour point depression process, need not add enzyme preparation, under the condition of heating, the unstability macromole that utilizes stock solution self as: cellulose, hemicellulose, pectin, protein etc. are in the coagulation process, bridge formation flocculates and precipitates each other, do not add any flocculating agent and flocculating agent, keep the original natural environment of solution, and greatly reduce the process production cost.
(3) the stable Aloe gel juice of the water white transparency debitterize of this method production reaches the concentrated glue, the debitterize Aloe powder that obtain thus and can offer raw material or the auxiliary material of food industry as goods such as beverage, milk product, confections, can be used for producing other health functional food; Can be applicable to cosmetic industry, for middle and high shelves cosmetics, skin care item are supplied raw materials or auxiliary material; Can be industries such as articles for washing and medication health article supplies raw materials or auxiliary material; Also can be prepared into various dosage forms, comprising oral liquid, capsule (hard capsule, soft capsule, microcapsule and nanocapsule), tablet, granule, electuary, drop pill, micropill, beverage and injection type.
The specific embodiment
Below in conjunction with technical scheme, be described in detail concrete production stage of the present invention:
(1) squeeze the juice: carefully extract healthy and strong full aloe leaf of 3 terms with blade along root of blade, simply clean with tap water, drop is clean, does not need to add disinfectant and detergent in the cleaning process; With the peeling machine peeling,, little then to the production process influence if peeling not exclusively thoroughly; The reuse pulverizer is ground into serosity, then through flame filter press or bag filter filter gel juice.
(2) hot polymerization is heavy: gel juice is heated to 50 ℃~130 ℃ rapidly through plate type heat exchanger, change under 50 ℃~130 ℃ in the coagulation jar and kept 6 minutes~24 hours, coil heat exchanger is equipped with in coagulation pipe inside, make the unstability composition as: cellulose, hemicellulose, pectin, protein etc. settle down fully.
(3) decolouring: with sedimentation aloe juice completely, be cooled to 30 ℃~60 ℃ rapidly, change in the bleacher, stir decolouring 0.5 hour, anthraquinones is removed totally with 0.5%~1% powdered activated carbon with plate type heat exchanger.
(4) filter: said mixture is removed by filter active carbon through flame filter press or bag filter, and the decolouring clear liquor is removed residual activity charcoal and other microgranule through stainless (steel) wire strainer or the further fine straining of diatomite filter again, obtains water white Aloe gel juice.
(5) sterilization packaging: water white transparency liquid was sterilized for 15 seconds down at 130 ℃ through Thin plate heat exchanger again, was cooled to 60 ℃ rapidly, adopted vacuum tank installation carrying out vacuum packaging.

Claims (1)

1. a water white transparency debitterize is stablized the clean preparation method of Aloe gel juice, it is characterized in that: pluck healthy and strong full aloe leaf of 3 terms, clean with tap water, drop is clean, remove the peel with peeling machine, the reuse pulverizer is ground into serosity, then through flame filter press or bag filter filter gel juice, gel juice is heated to 50 ℃~130 ℃ through plate type heat exchanger, change under 50 ℃~130 ℃ in the coagulation jar and kept 10 minutes~10 hours, be cooled to 30 ℃~60 ℃ through plate type heat exchanger then, transfer to bleacher and stir decolouring 0.5 hour with 0.5%~1% powdered activated carbon, remove by filter active carbon through flame filter press or bag filter, the decolouring clear liquor is removed residual activity charcoal and other microgranule through stainless (steel) wire strainer or the further fine straining of diatomite filter again, water white transparency liquid was sterilized for 15 seconds down at 130 ℃ through Thin plate heat exchanger, was cooled to 60 ℃ rapidly, adopted vacuum tank installation carrying out vacuum packaging.
CN 200410021416 2004-03-16 2004-03-16 Cleaning production method of colourless transparent debittered stable aloe jelly juice Expired - Fee Related CN1284485C (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102247512A (en) * 2010-12-21 2011-11-23 刘青 Preparation method of aloe stock solution
CN103025340A (en) * 2010-07-23 2013-04-03 北德克萨斯医学联合会 Anti-viral properties of aloe vera and acquired immune deficiency syndrome (aids) treatment
CN103767032A (en) * 2014-01-26 2014-05-07 海南钟晨生物工程有限责任公司 Processing technology of high-content polysaccharide and O-acetyl aloe juice product

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103025340A (en) * 2010-07-23 2013-04-03 北德克萨斯医学联合会 Anti-viral properties of aloe vera and acquired immune deficiency syndrome (aids) treatment
CN103025340B (en) * 2010-07-23 2014-12-24 北德克萨斯医学联合会 Aloe vera, anti-viral properties of aloe vera and acquired immune deficiency syndrome (aids) treatment
CN102247512A (en) * 2010-12-21 2011-11-23 刘青 Preparation method of aloe stock solution
CN103767032A (en) * 2014-01-26 2014-05-07 海南钟晨生物工程有限责任公司 Processing technology of high-content polysaccharide and O-acetyl aloe juice product

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Granted publication date: 20061115