CN107058042A - A kind of yellow rose flowers and fruits vinegar and its manufacture method - Google Patents

A kind of yellow rose flowers and fruits vinegar and its manufacture method Download PDF

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Publication number
CN107058042A
CN107058042A CN201710082436.3A CN201710082436A CN107058042A CN 107058042 A CN107058042 A CN 107058042A CN 201710082436 A CN201710082436 A CN 201710082436A CN 107058042 A CN107058042 A CN 107058042A
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fermentation
flowers
fruits
yellow rose
vinegar
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CN107058042B (en
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宋高林
王晓燕
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SHANXI INSTITUTE OF MEDICINE AND LIFE SCIENCE
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SHANXI INSTITUTE OF MEDICINE AND LIFE SCIENCE
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    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/04Vinegar; Preparation or purification thereof from alcohol

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Abstract

The invention discloses a kind of yellow rose flowers and fruits vinegar and its manufacture method, following raw material is included:Yellow rose fruit, yellow rose, sugar, yeast, citric acid, acetic acid bacteria, pure water.There is provided a kind of flowers and fruits vinegar product of new varieties, sense organ is good, aromatic flavour, while being still belonged to the first time using yellow rose and yellow rose fruit come the flowers and fruits vinegar that ferments, stimulates the rise of new industry, can bring tangible economic interests to the local common people.

Description

A kind of yellow rose flowers and fruits vinegar and its manufacture method
Technical field
The present invention relates to plant technology and brewing technology, more particularly to a kind of yellow rose flowers and fruits vinegar and its manufacture method.
Background technology
Through generaI investigation, the wild yellow rose area in Shanxi Province is about 400~5,000,000 mu.Exemplified by closing Supreme Being mountain, from total biomass From the point of view of constituting, shrub is had comparative advantage (account for biological total amount 67%) with yellow rose, and sea-buckthorn takes second place (11%).Because yellow rose exists Investigation (has substantial amounts of distribution) on Taihang mountain range, Luiliang Mountains, Zhongtiao Shan Mountain, Wutai Mountain, pass Supreme Being mountain and other places extensively, and Quality is high, yield is big, and resource is enriched very much.Again due to being rich in a variety of nutrition, functional component in yellow rose fruit, it is a kind of valuable Food, the homologous fully natural green health food resource of medicine, it would be highly desirable to develop.
Due to being rich in a variety of nutrition, functional component in rose hip, so it is homologous pure natural of a kind of valuable food, medicine Green health care food resource.In March, 2002, what the Ministry of Public Health sent《Further specification healthy food material management》In, rose will be pierced Fruit has been included in " article that can be used for health food " list.
At present, the fruit vinegar kind occurred in China market has Hawthorn Vinegar, apple vinegar, grape vinegar, winter jujube vinegar, persimmon The series of products such as vinegar, papaya ester, Chinese gooseberry vinegar, pears vinegar, honey peach fruit vinegar, raspberry fruit vinegar, momordica grosvenori vinegar, mulberry fruit vinegar, sea-buckthorn vinegar, Greatly meet demand of the people to various nutrition and health care fruit vinegar beverages.It has been observed that all fruit vinegars can not be presented completely The color or lighter of the fruit itself, sense organ are poor, influence its market sale share.Current in the market yet there are no utilization Yellow rose or the flowers and fruits vinegar product that yellow rose fruit is raw material.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of good, the nutritious yellow rose flowers and fruits vinegar of sense organ and its system Make method.
The present invention solves the technical scheme that is used of above-mentioned technical problem:
A kind of yellow rose flowers and fruits vinegar, includes following raw material:Yellow rose fruit, yellow rose, sugar, yeast, citric acid, acetic acid Bacterium, pure water.Described yellow rose fruit is fresh fruit or frozen fruit, and described yellow rose is fresh flower or jelly fresh flower, described sugar For sucrose, maltose or xylitol, described yeast is angel's Active Dry Yeast, and described acetic acid bacteria is dealt out the cards wine for enlightening Vinegar acetic acid bacteria.
A kind of manufacture method of yellow rose flowers and fruits vinegar, comprises the following steps:Raw material selection, washing, broken, mashing, alcohol extracting Pigment, heat treatment, ferment treatment, sterilizing, activated yeast, composition adjustment, alcoholic fermentation, acetic fermentation plus salt after-ripening, new vinegar are adjusted Match somebody with somebody, ageing, finished product allotment, filling, once sterilization, sealing, re-pasteurization, inspection, labeling.
It is preferred that, a kind of manufacture method of yellow rose flowers and fruits vinegar comprises the following steps:
Step 1: raw material selection, washing:Select the ninety percent ripe above, no disease and pests harm, without go mouldy and mechanical damage yellow rose Really, impurities removing, rinses the dirt and debris of fruit surface, selection yellow rose petal or just open yellow rose;
Step 2: broken and mashing:Yellow rose fruit is used into roll crushing crusher machine, yellow rose is added when crushing, finally Obtain flowers and fruits slurry;
Step 3: alcohol extracting pigment:The pigment of yellow rose fruit and flower is extracted with 70% ethanol water, according to ethanol solution With flowers and fruits slurry 5:1 ratio, extracts 2h, filters to obtain alcohol extract, reclaims ethanol by rotary film evaporator and is concentrated to give Huang The pigment of rose hip and flower extracts concentrate, refrigerates standby;
Step 4: heat treatment and ferment treatment:A small amount of pure water is added in the flowers and fruits slurry of alcohol extracted, no more than flowers and fruits slurry The 10% of weight, is then kept for 3-5 minutes in 80-90 DEG C of water-bath, and is rapidly cooled to 45-55 DEG C, with the dissolving of a small amount of water Pectase, then adds flowers and fruits slurry by enzyme liquid, is incubated and is stirred continuously, enzyme action time is 1h;
Step 5: sterilizing:SO2 or potassium metabisulfite is added to suppress harmful microbe vigor and polyphenol oxidase Activity, suppresses the activity of other yeast, and addition is pressed adds liquid SO per in 1Kg flowers and fruits slurry250mg or by every 1Kg flowers and fruits starch in Potassium metabisulfite 120mg is added, is stirred, sealing is placed about 2 hours;
Step 6: activated yeast and composition adjustment, by pure water:Flowers and fruits slurry=10:1 ratio calculates the gross weight of zymotic fluid Amount, sugar and yeast consumption are determined according to zymotic fluid gross weight, and sugar accounts for zymotic fluid gross weight 30%, then, first takes appropriate amount of purified water, 20% sugar is added, 35-40 DEG C is warming up to, then yeast is added in syrup and constitutes yeast soln 1~2h of activation, yeast accounts for fermentation Liquid gross weight 10%, then adds purified water remainder in flowers and fruits slurry, while sugar is added in flowers and fruits slurry, the sugared content for starching flowers and fruits Reach 20% and stir, the yeast soln activated is added be well mixed in the flowers and fruits slurry stirred afterwards, finally, The citric acid of addition 0.1%~0.15% starts fermentation to Ph3.5-4.0;
Step 7: alcoholic fermentation:Remaining sugar is separately added into for three parts according to total amount point in earlier fermentation, mid-term and later stage;
(1) primary fermentation:After the fermentation of step 6 zymotic fluid is vigorous (pol drops to 7%~9%), 1/3 sugar is added Continue to ferment, 22-25 DEG C of fermentation temperature ferments 10-12 days or so;
(2) fermented in:Primary fermentation terminates, that is, after primary fermentation zymotic fluid adds sugar, ferment again it is vigorous after (sugar Degree drops to 7%~9%), 1/3 sugar is added, second of fermentation (middle fermentation) is carried out, 22-25 DEG C of fermentation temperature ferments 10-12 days or so;
(3) after fermentation:After middle fermentation ends, that is, (pol drops to 7% after zymotic fluid fermentation is vigorous for middle fermentation ~9%), remaining 1/3 sugar is added, after fermentation is carried out, 13-15 DEG C of fermentation temperature ferments one month;
After three phases fermentation ends, original wine (raw wine) is filtered to obtain, alcoholic strength reaches 18--25 degree;
Step 8: acetic fermentation:Acetic acid bacteria activation medium is prepared, the slant tube of inoculation is put into incubator, with 30 DEG C are incubated 3 days, and the alcohol of 2-3 drops 95% is added dropwise in culture dish, reinjecting acetic acid bacteria isolation medium in sterile working, After well mixed, flat board is settled into, the strain that culture is dipped with oese carries out line separation, with 30 DEG C of cultures, from culture medium In transfer single bacterium kind, again on acetic acid bacteria isolation medium carry out line separation, with 30 DEG C culture 3 days after transfer single bacterium Drop into row microscopy;When alcoholic strength reaches 8 or so in yellow rose fruit wine, it is 3% to adjust its pol, is added in 10% ratio through expanding Big cultured acetic acid bacteria, at 30-33 DEG C, the 150r/min enterprising row of shaking table carries out acetic fermentation 4 days, determines acetic acid content and reaches During to 6% or so, show that acetic fermentation terminates;
Step 9: plus salt after-ripening:After acetic fermentation terminates, to avoid acetic acid from being oxidized to CO2And H2O should add food in time Salt after-ripening, salt adding amount is the 1.5-2.2% of acetic acid weight, mixes placement 2 days thoroughly;
Step 10: new vinegar allotment, ageing:Flowers and fruits vinegar is obtained after fermentation ends, concentrate is extracted according to pigment:Flowers and fruits vinegar= 1:4 ratio is allocated, then ageing, refined filtration;
Step 11: finished product allotment, it is filling:According to final physical and chemical index, yellow rose flowers and fruits vinegar is added by a certain percentage pure Water purification dilutes, sugar addition, acidity, after mixing clarifying treatment, you can filling;
Step 12: once sterilizing:Once sterilize, using high-temperature instantaneous sterilization, 120 DEG C, 3s;
Step 13: sealing and re-pasteurization:Yellow rose flowers and fruits vinegar after once sterilizing is bottled sealing in time, notes packing The sterilizing of bottle, re-pasteurization:Sterilized using bar formula, 90 DEG C, 10min, cooling:Less than 40 DEG C are rapidly cooled to after re-pasteurization;
Step 14: inspection, labeling:The abnormalities such as breakage, foreign matter are checked for, after qualified products are labelled i.e. Into finished product.
It is preferred that, in the step 7, each sugaring makes the pol of zymotic fluid control in 15%-30%.
It is preferred that, in the step 2, in the vitamin c solution that fruit surface spray concentration is 0.1 ‰ before crushing, to prevent Only its oxidizing brown stain.
Compared with prior art, the present invention has following beneficial effect:
The invention of this reality is produced there is provided a kind of yellow rose flowers and fruits vinegar and its manufacture method there is provided a kind of flowers and fruits vinegar of new varieties Product, sense organ is good, aromatic flavour, while being still belonged to the first time using yellow rose and yellow rose fruit come the flowers and fruits vinegar that ferments, stimulates emerging production The rise of industry, can bring tangible economic interests to the local common people.
Embodiment
The present invention is described in further detail below by specific embodiment, various ratios of the invention are weight Than.
Embodiment 1
A kind of yellow rose flowers and fruits vinegar, includes following raw material:Yellow rose fruit, yellow rose, sugar, yeast, citric acid, acetic acid Bacterium, pure water.Described yellow rose fruit is fresh fruit or frozen fruit, and described yellow rose is fresh flower or jelly fresh flower, described sugar For sucrose, maltose or xylitol, described yeast is angel's Active Dry Yeast, and described acetic acid bacteria is dealt out the cards wine for enlightening Vinegar acetic acid bacteria.
A kind of manufacture method of yellow rose flowers and fruits vinegar, comprises the following steps:
Step 1: raw material selection, washing:Select the ninety percent ripe above, no disease and pests harm, without go mouldy and mechanical damage yellow rose Fresh fruit or frozen fruit, impurities removing, using rotary drum washer or rinse pouring formula cleaning machine rinse fruit surface dirt and debris, Because not easy to maintain under yellow rose fruit normal temperature, therefore can not such as process in time, can first by its it is quick-frozen store for future use, select yellow rose Luxuriant or just open yellow rose, because yellow rose and yellow rose be not really in same season, therefore can also be by yellow rose It is quick-frozen to store for future use, it is demonstrated experimentally that after yellow rose fruit and yellow rose are chilled, its nutrition and functional component are not influenceed.
Step 2: broken, mashing:Yellow rose fruit is used into roll crushing crusher machine, can be sprayed before crushing in fruit surface dense Spend the vitamin c solution for 0.1 ‰, to prevent its oxidizing brown stain, then again with roll crushing crusher machine (due to rose hip seed and Pulp be difficult separation, its seed again it is very hard, it is non-breakable, seed oil be difficult leach, do not influence fermentation, therefore, it can without point Separating fruit meat and seed), yellow rose is added when crushing, flowers and fruits slurry is finally obtained.
Step 3: alcohol extracting pigment:The pigment of yellow rose fruit and flower is extracted with 70% ethanol water, according to ethanol solution With flowers and fruits slurry 5:1 ratio, extracts 2h, filters to obtain alcohol extract, reclaims ethanol by rotary film evaporator and is concentrated to give Huang The pigment of rose hip and flower extracts concentrate, refrigerates standby.
Step 4: heat treatment, ferment treatment:A small amount of pure water is added in the flowers and fruits slurry of alcohol extracted, no more than flowers and fruits slurry The 10% of weight, is then kept for 3-5 minutes in 80-90 DEG C of water-bath, and is rapidly cooled to 45-55 DEG C, with the dissolving of a small amount of water Pectase, then adds flowers and fruits slurry by enzyme liquid, is incubated and is stirred continuously, enzyme action time is 1h.
Step 5: sterilizing:Add SO2Or potassium metabisulfite is to suppress harmful microbe vigor and polyphenol oxidase Activity, suppresses the activity of other yeast, and addition is pressed adds liquid SO per in 1Kg flowers and fruits slurry250mg or by every 1Kg flowers and fruits starch in Potassium metabisulfite 120mg is added, is stirred, sealing is placed about 2 hours.
Step 6: activated yeast, composition adjustment, by pure water:Flowers and fruits slurry=10:1 ratio calculates the gross weight of zymotic fluid Amount, dosage of sucrose (accounting for 30%) is determined according to zymotic fluid total amount, then, first takes appropriate amount of purified water, is added 20% sucrose, is warming up to 35-40 DEG C, then yeast (accounting for zymotic fluid total amount 10%) is added in syrup and constitutes yeast soln 1~2h of activation, then will be surplus Remaining pure water is added in flowers and fruits slurry, while adding sucrose in flowers and fruits slurry, the sugared content that flowers and fruits are starched is reached 20% and is stirred, The yeast soln activated is added afterwards and is well mixed in the flowers and fruits slurry stirred, finally, 0.1%~0.15% is added Citric acid starts fermentation to Ph3.5-4.0.
Step 7: alcoholic fermentation:Remaining sucrose is separately added into for three parts according to total amount point in earlier fermentation, mid-term and later stage.
(1) primary fermentation:After zymotic fluid fermentation is vigorous (pol drops to 7%~9%), the sucrose for adding 1/3 continues Fermentation, 22-25 DEG C of fermentation temperature ferments 10-12 days or so.
(2) fermented in:Primary fermentation terminates, that is, after primary fermentation zymotic fluid adds sucrose, ferment again it is vigorous after (pol drops to 7%~9%), add 1/3 sucrose, carry out second fermentation (middle fermentation), 22-25 DEG C of fermentation temperature, Fermentation 10-12 days or so.
(3) after fermentation:After middle fermentation ends, that is, (pol drops to 7% after zymotic fluid fermentation is vigorous for middle fermentation ~9%), remaining 1/3 sucrose is added, after fermentation is carried out, 13-15 DEG C of fermentation temperature ferments one month.
After three phases fermentation ends, original wine (raw wine) is filtered to obtain, alcoholic strength is up to 20 degree or so.
Each sugaring is it is desirable that total sugar amount of zymotic fluid controls that, more than 15% and no more than 30%, ferment otherwise can be influenceed Female fermentation.
Step 8: acetic fermentation:Acetic acid bacteria activation medium is prepared, the slant tube of inoculation is put into incubator, with 30 DEG C are incubated 3 days, and the alcohol of 2-3 drops 95% is added dropwise in culture dish, reinjecting acetic acid bacteria isolation medium in sterile working, After well mixed, flat board is settled into, the strain that culture is dipped with oese carries out line separation, with 30 DEG C of cultures, from culture medium In transfer single bacterium kind, again on acetic acid bacteria isolation medium carry out line separation, with 30 DEG C culture 3 days after transfer single bacterium Drop into row microscopy;When alcoholic strength reaches 8 or so in yellow rose fruit wine, it is 3% to adjust its pol, is added in 10% ratio through expanding Big cultured acetic acid bacteria, at 30-33 DEG C, the 150r/min enterprising row of shaking table carries out acetic fermentation 4 days, determines acetic acid content and reaches During to 6% or so, show that acetic fermentation terminates.Or (enlightening is dealt out the cards makes vinegar acetic acid bacteria, Shanghai enlightening to the acetic acid seed fermentation of access 10% Hair brewages the production of biological products Co., Ltd).
Step 9: plus salt after-ripening:After acetic fermentation terminates, to avoid acetic acid from being oxidized to CO2And H2O should add food in time Salt after-ripening, salt adding amount is the 1.5-2.2% of acetic acid, mixes placement 2 days thoroughly.
Step 10: new vinegar allotment, ageing:Flowers and fruits vinegar is obtained after fermentation ends, concentrate is extracted according to pigment:Flowers and fruits vinegar= 1:4 ratio is allocated, and the purpose of allotment is to make that the fruit flavor of vinegar body is stronger, and color and luster is more gorgeous, then ageing, essence Filter.
Step 11: finished product allotment, it is filling:According to final physical and chemical index, yellow rose flowers and fruits vinegar is added by a certain percentage pure Water purification dilutes, sugar addition, acidity, after mixing clarifying treatment, you can filling.
Step 12: once sterilizing:Once sterilize, using high-temperature instantaneous sterilization (120 DEG C, 3s).
Step 13: sealing and re-pasteurization:Yellow rose flowers and fruits vinegar after once sterilizing is bottled sealing in time, notes packing The sterilizing of bottle, re-pasteurization:(90 DEG C, 10min) are sterilized using bar formula, cooling:Less than 40 DEG C are rapidly cooled to after re-pasteurization.
Step 14: inspection, labeling:The abnormalities such as breakage, foreign matter are checked for, after qualified products are labelled i.e. Into finished product.
The standard that product quality reaches:
First, organoleptic indicator:
(1) color and luster:Red, glossy, the uniformity in rose hip.
(2) structural state:Clear, no precipitation and suspension, free from admixture.
(3) flavour and smell:With fragrant fragrant, sour-sweet tasty and refreshing, the pleasant impression long with vinegar of strong rose hip.
2nd, physical and chemical index:
(1) alcohol content (20 DEG C, volume fraction) (%):<2.
(2) total pol (with glucose meter) (g/L):80-120.
(3) total acidity (in terms of lemon juice) (g/L):2.5-3.5.
(4) soluble solid content (abbe's refractometer) %:≥8.0.
Yellow rose flowers and fruits vinegar is that advanced row alcoholic fermentation is obtained using pure natural wild yellow rose fruit and yellow rose as raw material Flower and fruit wine zymotic fluid, then by acetic fermentation, ageing, a kind of flowers and fruits vinegar beverage of allotment.With beautiful in colour (in rose Claret), nutritious, unique flavor, it is sour-sweet tasty and refreshing the characteristics of, be to integrate nutrition, the low hair of one kind of healthcare function Ferment flowers and fruits vinegar beverage.
Due in yellow rose fruit rich in flavonoids, anthocyanidin, multivitamin, 17 kinds of amino acid (wherein threonine, figured silk fabrics Seven kinds of propylhomoserin, isoleucine, leucine, methionine, phenylalanine and lysine etc. and must be unable to itself for human body The amino acid of synthesis), trace element (28 kinds altogether, wherein there is the necessary micro member of 14 kinds of human bodies such as zinc, iron, selenium Element), organic acid, carbohydrate, Coumarins, sterol, triterpenes, polyene hydrocarbons, saponin, protein, carbohydrate, fat oil, volatile oil, Etc. a variety of nutritive effect compositions.Contain the nutritive effect compositions such as volatile oil, triterpenes, polyene hydrocarbons in yellow rose.Therefore, with A variety of nutrition and health care functional components have been dissolved in yellow rose fruit and the yellow rose flowers and fruits vinegar that yellow rose is fermenting raw materials.Separately Outside, yellow rose flowers and fruits vinegar can also form acetate, several amino acids and multivitamin during the fermentation, meanwhile, pass through production Fragrant bacterium produces fragrance.As can be seen here, there are yellow rose flowers and fruits vinegar a variety of nutrition and health cares to act on.Drink for a long time, to hypertension, hat The disease such as worry, cerebral thrombus, artery sclerosis and hyperlipemia, hypovitaminosis card, cancer has prevention and auxiliary treatment well Effect.With body-building and tonifying yang, brain tonic and intelligence development and it can promote longevity.
The invention of this reality is produced there is provided a kind of yellow rose flowers and fruits vinegar and its manufacture method there is provided a kind of flowers and fruits vinegar of new varieties Product, sense organ is good, aromatic flavour, while being still belonged to the first time using yellow rose and yellow rose fruit come the flowers and fruits vinegar that ferments, stimulates emerging production The rise of industry, can bring tangible economic interests to the local common people.
The present invention is described in detail according to embodiment and comparative example above, but the present invention is not limited to above-mentioned reality Example and comparative example are applied, in the knowledge that those skilled in the art possess, the premise of present inventive concept can also not departed from Under make a variety of changes.

Claims (6)

1. a kind of yellow rose flowers and fruits vinegar, it is characterised in that include following raw material:Yellow rose fruit, yellow rose, sugar, yeast, lemon Acid, acetic acid bacteria, pure water.
2. yellow rose flowers and fruits vinegar according to claim 1, it is characterised in that:Described yellow rose fruit is that fresh fruit or jelly are fresh Really, described yellow rose is fresh flower or freezes fresh flower, and described sugar is sucrose, maltose or xylitol, and described yeast is peace Fine jade Active Dry Yeast, described acetic acid bacteria is dealt out the cards for enlightening makes vinegar acetic acid bacteria.
3. a kind of manufacture method of yellow rose flowers and fruits vinegar according to claim 1 or 2, it is characterised in that including following step Suddenly:Raw material selection, washing, broken, mashing, alcohol extracting pigment, heat treatment, ferment treatment, sterilizing, activated yeast, composition adjustment, alcohol Fermentation, acetic fermentation plus salt after-ripening, the allotment of new vinegar, ageing, finished product allotment, filling, once sterilization, sealing, re-pasteurization, inspection Test, labeling.
4. the manufacture method of yellow rose flowers and fruits vinegar according to claim 3, it is characterised in that comprise the following steps:
Step 1: raw material selection, washing:Select the ninety percent ripe above, no disease and pests harm, without go mouldy and mechanical damage yellow rose fruit, Impurities removing, rinses the dirt and debris of fruit surface, selection yellow rose petal or just open yellow rose;
Step 2: broken and mashing:Yellow rose fruit is used into roll crushing crusher machine, yellow rose is added when crushing, is finally obtained Flowers and fruits are starched;
Step 3: alcohol extracting pigment:The pigment of yellow rose fruit and flower is extracted with 70% ethanol water, according to ethanol solution and flower Pulp 5:1 ratio, extracts 2h, filters to obtain alcohol extract, reclaims ethanol by rotary film evaporator and is concentrated to give yellow rose The pigment of fruit and flower extracts concentrate, refrigerates standby;
Step 4: heat treatment and ferment treatment:A small amount of pure water is added in the flowers and fruits slurry of alcohol extracted, weight is starched no more than flowers and fruits 10%, then kept for 3-5 minutes in 80-90 DEG C of water-bath, and be rapidly cooled to 45-55 DEG C, with a small amount of water dissolving pectin Enzyme, then adds flowers and fruits slurry by enzyme liquid, is incubated and is stirred continuously, enzyme action time is 1h;
Step 5: sterilizing:Add SO2Or potassium metabisulfite is to suppress the activity of harmful microbe vigor and polyphenol oxidase, Suppress the activity of other yeast, addition is pressed adds liquid SO per in 1Kg flowers and fruits slurry250mg or by every 1Kg flowers and fruits starch in add Potassium metabisulfite 120mg, is stirred, and sealing is placed about 2 hours;
Step 6: activated yeast and composition adjustment, by pure water:Flowers and fruits slurry=10:1 ratio calculates the gross weight of zymotic fluid, Sugar and yeast consumption are determined according to zymotic fluid gross weight, sugar accounts for zymotic fluid gross weight 30%, then, first takes appropriate amount of purified water, plus Enter 20% sugar, be warming up to 35-40 DEG C, then yeast is added in syrup and constitutes yeast soln 1~2h of activation, yeast accounts for zymotic fluid Gross weight 10%, then adds purified water remainder in flowers and fruits slurry, while adding sugar in flowers and fruits slurry, reaches the sugared content that flowers and fruits are starched To 20% and stir, the yeast soln activated is added be well mixed in the flowers and fruits slurry stirred afterwards, finally, plus Enter 0.1%~0.15% citric acid to Ph3.5-4.0, start fermentation;
Step 7: alcoholic fermentation:Remaining sugar is separately added into for three parts according to total amount point in earlier fermentation, mid-term and later stage;
(1) primary fermentation:After the fermentation of step 6 zymotic fluid is vigorous (pol drops to 7%~9%), 1/3 sugar continuation is added Fermentation, 22-25 DEG C of fermentation temperature ferments 10-12 days or so;
(2) fermented in:Primary fermentation terminates, that is, after primary fermentation zymotic fluid adds sugar, ferment again it is vigorous after (under pol It is down to 7%~9%), 1/3 sugar is added, second of fermentation (middle fermentation), 22-25 DEG C of fermentation temperature, fermentation 10-12 is carried out It or so;
(3) after fermentation:After middle fermentation ends, that is, middle fermentation after zymotic fluid fermentation is vigorous (pol drops to 7%~ 9%) remaining 1/3 sugar, is added, after fermentation is carried out, 13-15 DEG C of fermentation temperature ferments one month;
After three phases fermentation ends, original wine is filtered to obtain, alcoholic strength reaches 18--25 degree;
Step 8: acetic fermentation:Acetic acid bacteria activation medium is prepared, the slant tube of inoculation is put into incubator, with 30 DEG C Incubated 3 days, the alcohol of 2-3 drops 95% was added dropwise in culture dish, reinjecting acetic acid bacteria isolation medium in sterile working, mixes After uniform, flat board is settled into, the strain that culture is dipped with oese carries out line separation, with 30 DEG C of cultures, is adjusted from culture medium Single bacterium kind is taken, line separation is carried out on acetic acid bacteria isolation medium again, single bacterium colony is transferred after being cultivated 3 days with 30 DEG C and enters Row microscopy;When alcoholic strength reaches 8 degree or so in yellow rose fruit wine, it is 3% to adjust its pol, is added in 10% ratio through expanding Cultured acetic acid bacteria, at 30-33 DEG C, the 150r/min enterprising row of shaking table carries out acetic fermentation 4 days, determines acetic acid content and reaches When 6% or so, show that acetic fermentation terminates;
Step 9: plus salt after-ripening:After acetic fermentation terminates, to avoid acetic acid from being oxidized to CO2And H2O should be added after salt in time Ripe, salt adding amount is the 1.5-2.2% of acetic acid weight, mixes placement 2 days thoroughly;
Step 10: new vinegar allotment, ageing:Flowers and fruits vinegar is obtained after fermentation ends, concentrate is extracted according to pigment:Flowers and fruits vinegar=1:4 Ratio allocated, then ageing, refined filtration;
Step 11: finished product allotment, it is filling:According to final physical and chemical index, yellow rose flowers and fruits vinegar is added into pure water by a certain percentage After dilution, sugar addition, acidity, mixing clarifying treatment, you can filling;
Step 12: once sterilizing:Once sterilize, using high-temperature instantaneous sterilization, 120 DEG C, 3s;
Step 13: sealing and re-pasteurization:Yellow rose flowers and fruits vinegar after once sterilizing is bottled sealing in time, notes Packaging Bottle Sterilizing, re-pasteurization:Sterilized using bar formula, 90 DEG C, 10min, cooling:Less than 40 DEG C are rapidly cooled to after re-pasteurization;
Step 14: inspection, labeling:Check for the abnormalities such as breakage, foreign matter, after qualified products are labelled into Product.
5. the manufacture method of yellow rose flowers and fruits vinegar according to claim 4, it is characterised in that:In the step 7, every time Sugaring makes the pol of zymotic fluid control in 15%-30%.
6. the manufacture method of yellow rose flowers and fruits vinegar according to claim 4, it is characterised in that:In the step 2, crush It is preceding fruit surface spray concentration be 0.1 ‰ vitamin c solution, to prevent its oxidizing brown stain.
CN201710082436.3A 2017-02-16 2017-02-16 Rosa xanthina fruit vinegar and preparation method thereof Expired - Fee Related CN107058042B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107354081A (en) * 2017-08-29 2017-11-17 广西仙珠食品有限公司 A kind of preparation method of sweet osmanthus mulberries fruit vinegar
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CN108504537A (en) * 2018-06-28 2018-09-07 唐山师范学院 A kind of anli pear rose vinegar brewage process

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