CN104414892A - Lotus leaf extract, extraction method and applications thereof - Google Patents
Lotus leaf extract, extraction method and applications thereof Download PDFInfo
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- CN104414892A CN104414892A CN201310370802.7A CN201310370802A CN104414892A CN 104414892 A CN104414892 A CN 104414892A CN 201310370802 A CN201310370802 A CN 201310370802A CN 104414892 A CN104414892 A CN 104414892A
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- folium nelumbinis
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Abstract
The present invention provides a lotus leaf extract extraction method, which comprises: extracting lotus leaf in an extractant to obtain an extraction solution, wherein the extractant comprises glycerol, propylene glycol and water; and sequentially carrying out treatments such as filtration, desalting, decolorization and sterilization on the extraction solution to obtain the lotus leaf extract. According to the present invention, the lotus leaf is extracted in the extractant comprising the glycerol, the propylene glycol and the water to obtain the extraction solution, and then the extraction solution is sequentially subjected to the treatments such as filtration, desalting, decolorization and sterilization to obtain the lotus leaf extract; with the lotus leaf extract obtained by using the extraction method of the present invention, particle pollutants such as dust and the like in air can be effectively isolated, and the lotus leaf extract can be used for cosmetics and particularly used as creams, lotions, toner, foundation liquid and the like; and experiment results show that the particle pollutant barrier capacity of the cream containing 10% of the prepared lotus leaf extract can be increased by 192%.
Description
Technical field
The present invention relates to technical field of plant extraction, be specifically related to a kind of Folium Nelumbinis extract, its extracting method and application thereof.
Background technology
Along with improving constantly and scientific and technical continuous progress of living standards of the people, people more and more select natural safe articles for daily use.Therefore, the cosmetic products of natural origin obtain and develop fast.Plant extract technology have also been obtained sufficient exploitation as the main acquisition means of natural skin care product raw material.Current people can extract from positions such as the leaf of plant, stem, flower, roots, obtain the extracting solution containing special component.Common plant extract comprises: Aloe extraction solution, Cortex Mori extracting solution, Radix Ginseng extractive solution etc.
Folium Nelumbinis has self-cleaning function, and water and dust etc. all cannot be adsorbed onto Folium Nelumbinis surface, and its principle is the waxiness nanostructured that Folium Nelumbinis has one deck self assembly to get up on the surface, and this one deck waxiness can effectively stop pollutant to the invasion and attack of plant.Therefore, the present inventor considers the effective ingredient that can extract in Folium Nelumbinis, and prepares functional material.
Summary of the invention
The technical problem that the present invention solves is to provide a kind of Folium Nelumbinis extract, its extracting method and application thereof, and Folium Nelumbinis extract provided by the invention effectively can completely cut off particulate pollutant.
The invention provides a kind of extracting method of Folium Nelumbinis extract, comprise the following steps:
Extracted in extractant by Folium Nelumbinis, be extracted liquid, described extractant comprises glycerol, propylene glycol and water;
By described extract successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.
Preferably, in described extractant, the mass ratio of described glycerol, propylene glycol and water is 1 ~ 10:1 ~ 10:70 ~ 98.
Preferably, the mass ratio of described Folium Nelumbinis and described extractant is 1:3 ~ 5.
Preferably, the temperature of described extraction is 25 DEG C ~ 50 DEG C, and the time of described extraction is 10min ~ 120min.
Preferably, described Folium Nelumbinis is prepared in accordance with the following methods:
Pluck Folium Nelumbinis, shear after pretreatment.
Preferably, the time of described harvesting Folium Nelumbinis is point ~ 7 point in early morning 4 that Flos Nelumbinis blooms season; During described harvesting Folium Nelumbinis, the blade diameter of Folium Nelumbinis is 30cm ~ 60cm.
Preferably, described pretreatment is specially:
The stem of removing Folium Nelumbinis and petiole, obtain blade;
Described blade is cleaned.
Preferably, described shearing is specially:
Adopt cross cutting method to shear the Folium Nelumbinis obtained after pretreatment, obtaining area is 1cm
2~ 10cm
2fritter Folium Nelumbinis.
Preferably, described in be filtered into classified filtering, the aperture of the filter plant of employing is 0.2 micron ~ 500 microns.
The extracting method that present invention also offers described in a kind of technique scheme extracts the Folium Nelumbinis extract obtained.
The extracting method that present invention also offers described in a kind of technique scheme extracts the application of Folium Nelumbinis extract in cosmetics obtained.
Compared with prior art, Folium Nelumbinis extracts by the present invention in the extractant comprising glycerol, propylene glycol and water, is extracted liquid, then by described extract successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.The Folium Nelumbinis extract adopting extracting method provided by the invention to obtain effectively can completely cut off the particulate pollutant in air, as dust etc., may be used for cosmetics, is particularly suited for being used as facial cream, emulsion, cosmetic water, foundation emulsion etc.Experimental result shows, the ability that the facial cream of the Folium Nelumbinis extract prepared containing 10% the present invention intercepts particulate pollutant can improve 192%.
Detailed description of the invention
In order to understand the present invention further, below in conjunction with embodiment, the preferred embodiment of the invention is described, but should be appreciated that these describe just for further illustrating the features and advantages of the present invention, instead of limiting to the claimed invention.
The invention provides a kind of extracting method of Folium Nelumbinis extract, comprise the following steps:
Extracted in extractant by Folium Nelumbinis, be extracted liquid, described extractant comprises glycerol, propylene glycol and water;
By described extract successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.
The present invention take Folium Nelumbinis as raw material.It extracts after plucking fresh Folium Nelumbinis by the present invention in extractant.
The present invention before extraction, carries out shear treatment after preferably the Folium Nelumbinis of harvesting being carried out pretreatment, to improve the extraction efficiency of Folium Nelumbinis.Point ~ 7 point in early morning 4 in season is preferably bloomed in the present invention at Flos Nelumbinis, before namely the sun rises, pluck the complete mature Folium Nelumbinis that blade diameter is 30cm ~ 60cm.When the sun rise after, temperature is higher, can cause the rapid dehydration of Folium Nelumbinis wither, be unfavorable for subsequent extracted work, therefore need the harvesting carrying out Folium Nelumbinis time temperature is lower in the morning, all harvesting job demand in the morning 7 completed in the past.Described Folium Nelumbinis preferably only includes blade, does not comprise stem.After harvesting, by Folium Nelumbinis fresh-keeping preservation below 5 DEG C.
After harvesting obtains Folium Nelumbinis, before extracting, carry out pretreatment to it, described pretreatment is specially:
The stem of removing Folium Nelumbinis and petiole, obtain blade;
Described blade is cleaned.
After harvesting obtains Folium Nelumbinis, first remove its stem and petiole, retain blade; Then described blade is cleaned, preferably use clean water more than 3 times until the water after cleaning is in clarification shape.Carry out draining process after Folium Nelumbinis cleaning, as process can be left standstill at web plate, fall until Folium Nelumbinis no longer includes water droplet.After wiping out stem and petiole, before cleaning, damaged Folium Nelumbinis is preferably had on surface to sort out.
Folium Nelumbinis after draining is cut into fritter Folium Nelumbinis, is specially:
Adopt cross cutting method to shear the Folium Nelumbinis obtained after pretreatment, obtaining area is 1cm
2~ 10cm
2fritter Folium Nelumbinis.
After obtaining fritter Folium Nelumbinis, can extract it.In the present invention, Folium Nelumbinis stops from when harvesting when extraction, preferably 5 DEG C of fresh-keeping preservations, preferably within 48h, completes extraction work.
Before extracting, the present invention preferably cleans fritter Folium Nelumbinis, first uses clean water, then uses washed with de-ionized water 3 times.
Then fritter Folium Nelumbinis is mixed with extractant and extract, be extracted liquid.In the present invention, described extractant comprises glycerol, propylene glycol and water, and the mass ratio of described glycerol, propylene glycol and water is preferably 1 ~ 10:1 ~ 10:70 ~ 98, is more preferably 3 ~ 7:3 ~ 7:76 ~ 94.The present invention preferably extracts under the condition stirred, and namely Folium Nelumbinis and extractant can be added in agitated kettle and stir, realize the extraction of Folium Nelumbinis effective ingredient while stirring.In the present invention, the mass ratio of described Folium Nelumbinis and described extractant is preferably 1:3 ~ 5; The temperature of described extraction is preferably 25 DEG C ~ 50 DEG C, and be more preferably 30 DEG C ~ 45 DEG C, the time of described extraction is preferably 10min ~ 120min, is more preferably 30min ~ 100min.
Extract complete after, by the extract that obtains successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.The present invention preferably adopts the method for classified filtering to filter described extract, and the aperture of the filter plant of employing is preferably 0.2 micron ~ 500 microns.Extract preferably tentatively filters through 200 mesh filter screens by the present invention, isolates Large stone Folium Nelumbinis residue; Then use filter element adding pressure type filter, progressively reduce filter element aperture, after eventually passing through the candle filter filtration of 0.2 micron pore size, obtain filtrate.In the present invention, the object progressively reducing filter element aperture is to improve filter effect, and reduce blocking, those skilled in the art can determine suitable filtering times and filter the filter element aperture adopted at every turn.
Filter complete after, desalination well known to those skilled in the art, desolventing technology are carried out to the filtrate obtained, eventually pass biofilter sterilization after, Folium Nelumbinis extract can be obtained.
This Folium Nelumbinis extract can be used for cosmetic field, and described cosmetics comprise cosmetic, skincare product etc., as facial cream, emulsion, cosmetic water and foundation emulsion etc.When this Folium Nelumbinis extract is used for cosmetic field, its addition is preferably 5wt% ~ 10wt%.As, it can be configured to facial cream with deionized water, glycerol, carbomer-980, Fancol ID, tween, triethanolamine etc., can effective air pollution isolation thing.
In addition, Folium Nelumbinis extract provided by the invention for the preparation of health product, can also comprise health food etc., and as being prepared into oral liquid according to the addition of 95wt%, product is comparatively stable.
Folium Nelumbinis extracts by the present invention in the extractant comprising glycerol, propylene glycol and water, is extracted liquid, then by described extract successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.The Folium Nelumbinis extract adopting extracting method provided by the invention to obtain effectively can completely cut off the particulate pollutant in air, as dust etc., may be used for cosmetics, is particularly suited for being used as facial cream, emulsion, cosmetic water, foundation emulsion etc.
In order to understand the present invention further, be described Folium Nelumbinis extract provided by the invention, its preparation method and application thereof below in conjunction with embodiment, protection scope of the present invention is not limited by the following examples.
Embodiment 1
The ripe Folium Nelumbinis 3 kilograms of blade face diameter 30 ~ 60 centimetres is plucked early morning 5, Folium Nelumbinis is put into the pond that 20 kilograms of tap waters are housed to clean 5 times, be placed on web plate and leave standstill 10 minutes, then the square mold cutter of 5 centimeter sides is used Folium Nelumbinis to be cut into the square of 5 centimeter sides, finally use sealing bag to be installed by Folium Nelumbinis, put into 5 degrees Celsius of Refrigerator stores.
After 24 hours, from refrigerator, take out Folium Nelumbinis, put into the pond that 20 kilograms of tap waters are housed and clean 2 times, then Folium Nelumbinis is put into the bucket that 10 kilograms of deionized waters are housed, stirring and washing, then Folium Nelumbinis is pulled out, change 10 kilograms of deionized waters stirring and washing again, clean 3 times altogether with deionized water.After having cleaned, Folium Nelumbinis is placed on web plate and leaves standstill 10 minutes, after not having water droplet to drip, Folium Nelumbinis is weighed, obtain Folium Nelumbinis 2.8 kilograms.
By Folium Nelumbinis and extract in mass ratio 1:3 ratio put into 20L capacity oar blade type agitated kettle and stir 60 minutes, extract ratio is: glycerol 1wt%, propylene glycol 1wt%, water 98wt%.
First the extraction mixture obtained tentatively is filtered by 200 mesh filter screens, isolates Large stone Folium Nelumbinis residue; Then filter through the filter element adding pressure type filter of 100 microns, 10 microns and 0.2 micron pore size successively, then through decolouring, desalting processing, then through biofilter sterilization, obtain water white transparency Folium Nelumbinis extract.
This water white transparency Folium Nelumbinis extract is added in day creams, emulsion and cosmetic water according to 5wt% addition respectively, constant product quality.
Embodiment 2
The ripe Folium Nelumbinis 30 kilograms of blade face diameter 30 ~ 60 centimetres is plucked early morning 4, Folium Nelumbinis is put into the pond that 200 kilograms of tap waters are housed to clean 5 times, be placed on web plate and leave standstill 10 minutes, then the square mold cutter of 1 centimeter sides is used Folium Nelumbinis to be cut into the square of 1 centimeter sides, the Folium Nelumbinis cut is weighed, obtains Folium Nelumbinis 29.7 kilograms.
Folium Nelumbinis is put into the bucket that 200 kilograms of deionized waters are housed, stirring and washing; Then Folium Nelumbinis is pulled out, change 200 kilograms of deionized waters stirring and washing again, clean 3 times altogether with deionized water.
By Folium Nelumbinis and extract in mass ratio 1:5 ratio put into 250L capacity oar blade type agitated kettle and stir 120 minutes, extract ratio is: glycerol 10wt%, propylene glycol 10wt%, water 80wt%.
First the extraction mixture obtained tentatively is filtered by 200 mesh filter screens, isolates Large stone Folium Nelumbinis residue; Then filter through the filter element adding pressure type filter of 100 microns, 10 microns and 0.2 micron pore size successively, then through decolouring, desalting processing, then through biofilter sterilization, obtain water white transparency Folium Nelumbinis extract.
This water white transparency Folium Nelumbinis extract is added in foundation emulsion according to 5wt% addition, constant product quality.
Embodiment 3
The ripe Folium Nelumbinis 3 kilograms of blade face diameter 30 ~ 60 centimetres is plucked early morning 5, Folium Nelumbinis is put into the pond that 20 kilograms of tap waters are housed to clean 3 times, be placed on web plate and leave standstill 10 minutes, then the square mold cutter of 5 centimeter sides is used Folium Nelumbinis to be cut into the square of 5 centimeter sides, finally use sealing bag to be installed by Folium Nelumbinis, put into 5 degrees Celsius of Refrigerator stores.
After 40 hours, from refrigerator, take out Folium Nelumbinis, put into the pond that 20 kilograms of tap waters are housed and clean 2 times, then Folium Nelumbinis is put into the bucket that 10 kilograms of deionized waters are housed, stirring and washing, then Folium Nelumbinis is pulled out, change 10 kilograms of deionized waters stirring and washing again, share washed with de-ionized water 3 times, after having cleaned, Folium Nelumbinis is placed on web plate and leaves standstill 10 minutes, after not having water droplet to drip, Folium Nelumbinis is weighed, obtain Folium Nelumbinis 2.7 kilograms.
By Folium Nelumbinis and extract in mass ratio 1:5 ratio put into 30L capacity oar blade type agitated kettle and stir 100 minutes, extract ratio is: glycerol 5wt%, propylene glycol 5wt%, water 90wt%.
First the extraction mixture obtained tentatively is filtered by 200 mesh filter screens, isolate Large stone Folium Nelumbinis residue, then filter through the filter element adding pressure type filter of 100 microns, 10 microns and 0.2 micron pore size successively, then through decolouring, desalting processing, again through biofilter sterilization, obtain water white transparency Folium Nelumbinis extract.
This water white transparency Folium Nelumbinis extract is made oral liquid according to 95wt% addition, constant product quality.
Embodiment 4:
Formula shown in use table 1 prepares protective skin cream:
The formula of protective skin cream prepared by table 1 embodiment of the present invention 1
Raw material | Ratio |
A phase: | |
Deionized water | 76.4wt% |
Glycerol | 5wt% |
Carbomer-980(polyacrylic acid) | 0.8wt% |
B phase | |
Different 12 alkane | 5wt% |
Tween 20 | 2wt% |
C phase | |
Triethanolamine | 0.8wt% |
D phase | |
Folium Nelumbinis extract prepared by embodiment 1 | 10wt% |
By A phase with B phase mix and blend after 2 minutes, homogenizing 3 minutes.Slowly add C phase after homogenizing completes, continue stirring 3 minutes.Then add D phase, stir after 3 minutes and stop stirring, obtain the protective skin cream containing 10% Folium Nelumbinis extract.
Use 10% deionized water to replace 10% Folium Nelumbinis extract, prepare blank sample protective skin cream.
To be uniformly coated on 2 cm diameter circular hospital gauzes respectively containing the protective skin cream 0.2 gram of 10% Folium Nelumbinis extract and blank sample protective skin cream 0.2 gram, room temperature is dried in the air system 10 minutes.Cover on the hose of 2 cm diameters by the gauze of the gauze and the blank sample protective skin cream of coating that are coated with Folium Nelumbinis extract protective skin cream respectively, the hose other end connects dust collection.The local clay of getting in grinding Beijing, uses ball mill grinding to obtain the clay particle that particle diameter concentrates on 0.1-50um after dry.Use aerator respectively to the gauze air blast of the gauze and the blank sample protective skin cream of coating that are coated with Folium Nelumbinis extract protective skin cream, continue to add clay particle to blower inlet with the speed of 0.1 gram/minute, continue interpolation 30 minutes.Then, weigh the dust weight in dust collection respectively, result is see table 2, and the dust that table 2 provides for the embodiment of the present invention and comparative example completely cuts off result.
The dust that table 2 embodiment of the present invention and comparative example provide completely cuts off result
Sample | Dust weight |
10% Folium Nelumbinis extract protective skin cream | 6.5g |
Blank sample protective skin cream | 8.8g |
Test result shows, the skin-protection product containing 10% Folium Nelumbinis extract can better air pollution isolation thing, can the particulate matter of obstruct 192% more than blank sample.
The explanation of above embodiment just understands method of the present invention and core concept thereof for helping.It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, can also carry out some improvement and modification to the present invention, these improve and modify and also fall in the protection domain of the claims in the present invention.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (10)
1. an extracting method for Folium Nelumbinis extract, comprises the following steps:
Extracted in extractant by Folium Nelumbinis, be extracted liquid, described extractant comprises glycerol, propylene glycol and water;
By described extract successively after filtration, desalination, decolouring and sterilization treatment, obtain Folium Nelumbinis extract.
2. extracting method according to claim 1, is characterized in that, in described extractant, the mass ratio of described glycerol, propylene glycol and water is 1 ~ 10:1 ~ 10:70 ~ 98;
The mass ratio of described Folium Nelumbinis and described extractant is 1:3 ~ 5.
3. extracting method according to claim 1, is characterized in that, the temperature of described extraction is 25 DEG C ~ 50 DEG C, and the time of described extraction is 10min ~ 120min.
4. extracting method according to claim 1, is characterized in that, described Folium Nelumbinis is prepared in accordance with the following methods:
Pluck Folium Nelumbinis, shear after pretreatment.
5. extracting method according to claim 4, is characterized in that, the time of described harvesting Folium Nelumbinis is point ~ 7 point in early morning 4 that Flos Nelumbinis blooms season; During described harvesting Folium Nelumbinis, the blade diameter of Folium Nelumbinis is 30cm ~ 60cm.
6. extracting method according to claim 4, is characterized in that, described pretreatment is specially:
The stem of removing Folium Nelumbinis and petiole, obtain blade;
Described blade is cleaned.
7. extracting method according to claim 4, is characterized in that, described shearing is specially:
Adopt cross cutting method to shear the Folium Nelumbinis obtained after pretreatment, obtaining area is 1cm
2~ 10cm
2fritter Folium Nelumbinis.
8. extracting method according to claim 1, is characterized in that, described in be filtered into classified filtering, the aperture of the filter plant of employing is 0.2 micron ~ 500 microns.
9. the extracting method described in claim 1 ~ 8 any one extracts the Folium Nelumbinis extract obtained.
10. the extracting method described in claim 1 ~ 8 any one extracts the application of Folium Nelumbinis extract in cosmetics obtained.
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CN105687266A (en) * | 2016-02-05 | 2016-06-22 | 海南医学院 | Bruguiera sexangula leaf extract and extraction method and application thereof |
CN113116778A (en) * | 2021-04-16 | 2021-07-16 | 广州中草世家化妆品有限公司 | Ginseng extracting solution and preparation method and application thereof |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105687266A (en) * | 2016-02-05 | 2016-06-22 | 海南医学院 | Bruguiera sexangula leaf extract and extraction method and application thereof |
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CN113116778A (en) * | 2021-04-16 | 2021-07-16 | 广州中草世家化妆品有限公司 | Ginseng extracting solution and preparation method and application thereof |
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Application publication date: 20150318 |